Coupling Adsorbed Evolution and Lattice Oxygen Mechanism in Fe‐Co(OH)2/Fe2O3 Heterostructure for Enhanced Electrochemical Water Oxidation

Oxygen evolution reaction (OER) remains a bottleneck for electrocatalytic water‐splitting to generate hydrogen. However, the traditional adsorbed evolution mechanism (AEM) possesses sluggish reaction kinetics due to the scaling relationship, while lattice oxygen mechanism (LOM) triggers an unstable...

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Published in:Advanced functional materials Vol. 33; no. 45
Main Authors: Xin, Sisi, Tang, Yu, Jia, Baohua, Zhang, Zhengfu, Li, Chengping, Bao, Rui, Li, Caiju, Yi, Jianhong, Wang, Jinsong, Ma, Tianyi
Format: Journal Article
Language:English
Published: Hoboken Wiley Subscription Services, Inc 02.11.2023
Subjects:
adsorbed evolution mechanism
Cobalt
Coupling
Current density
Electrocatalysts
Heterostructures
Iron
lattice oxygen mechanism
Materials science
Oxidation
oxygen evolution reaction
Oxygen evolution reactions
Reaction kinetics
Stability
Water splitting
ISSN:1616-301X, 1616-3028
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Abstract Oxygen evolution reaction (OER) remains a bottleneck for electrocatalytic water‐splitting to generate hydrogen. However, the traditional adsorbed evolution mechanism (AEM) possesses sluggish reaction kinetics due to the scaling relationship, while lattice oxygen mechanism (LOM) triggers an unstable structure due to the escaping of lattice oxygen. Herein, a proof‐of‐concept Fe‐Co(OH)2/Fe2O3 heterostructure is put forward, where Fe‐Co(OH)2 following AEM can complete rapidly deprotonation process while Fe2O3 following LOM can trigger O─O coupling step. Combining the theoretical and experimental investigation confirmed that the redistributed space‐charge of Fe‐Co(OH)2/Fe2O3 junction can optimize synergistically adsorbed and lattice oxygen, the coupling mechanism of AEM and LOM can facilitate synchronously the OER activity and stability. As a result, the Fe‐Co(OH)2/Fe2O3 heterostructure shows excellent OER performance with low overpotential of only 219 and 249 mV to reach a current density of 10 and 100 mA cm−2. Specifically, the Fe‐Co(OH)2/Fe2O3 electrocatalyst maintains excellent long‐term stability for 100 h at a large current density of 100 mA cm−2. This work paves an avenue to break through the limit of the conventional OER mechanism. A proof‐of‐concept Fe‐Co(OH)2/Fe2O3 heterostructure catalyst with high activity and stability is designed and fabricated. The coupling mechanism of AEM and LOM can break through the limit of the conventional OER mechanism to facilitate the OER activity and stability. This work offers a possible coupling mechanism for designing and explaining high‐performance OER electrocatalysts.
AbstractList Oxygen evolution reaction (OER) remains a bottleneck for electrocatalytic water‐splitting to generate hydrogen. However, the traditional adsorbed evolution mechanism (AEM) possesses sluggish reaction kinetics due to the scaling relationship, while lattice oxygen mechanism (LOM) triggers an unstable structure due to the escaping of lattice oxygen. Herein, a proof‐of‐concept Fe‐Co(OH)2/Fe2O3 heterostructure is put forward, where Fe‐Co(OH)2 following AEM can complete rapidly deprotonation process while Fe2O3 following LOM can trigger O─O coupling step. Combining the theoretical and experimental investigation confirmed that the redistributed space‐charge of Fe‐Co(OH)2/Fe2O3 junction can optimize synergistically adsorbed and lattice oxygen, the coupling mechanism of AEM and LOM can facilitate synchronously the OER activity and stability. As a result, the Fe‐Co(OH)2/Fe2O3 heterostructure shows excellent OER performance with low overpotential of only 219 and 249 mV to reach a current density of 10 and 100 mA cm−2. Specifically, the Fe‐Co(OH)2/Fe2O3 electrocatalyst maintains excellent long‐term stability for 100 h at a large current density of 100 mA cm−2. This work paves an avenue to break through the limit of the conventional OER mechanism.
Oxygen evolution reaction (OER) remains a bottleneck for electrocatalytic water‐splitting to generate hydrogen. However, the traditional adsorbed evolution mechanism (AEM) possesses sluggish reaction kinetics due to the scaling relationship, while lattice oxygen mechanism (LOM) triggers an unstable structure due to the escaping of lattice oxygen. Herein, a proof‐of‐concept Fe‐Co(OH)2/Fe2O3 heterostructure is put forward, where Fe‐Co(OH)2 following AEM can complete rapidly deprotonation process while Fe2O3 following LOM can trigger O─O coupling step. Combining the theoretical and experimental investigation confirmed that the redistributed space‐charge of Fe‐Co(OH)2/Fe2O3 junction can optimize synergistically adsorbed and lattice oxygen, the coupling mechanism of AEM and LOM can facilitate synchronously the OER activity and stability. As a result, the Fe‐Co(OH)2/Fe2O3 heterostructure shows excellent OER performance with low overpotential of only 219 and 249 mV to reach a current density of 10 and 100 mA cm−2. Specifically, the Fe‐Co(OH)2/Fe2O3 electrocatalyst maintains excellent long‐term stability for 100 h at a large current density of 100 mA cm−2. This work paves an avenue to break through the limit of the conventional OER mechanism. A proof‐of‐concept Fe‐Co(OH)2/Fe2O3 heterostructure catalyst with high activity and stability is designed and fabricated. The coupling mechanism of AEM and LOM can break through the limit of the conventional OER mechanism to facilitate the OER activity and stability. This work offers a possible coupling mechanism for designing and explaining high‐performance OER electrocatalysts.
Author Tang, Yu
Li, Caiju
Xin, Sisi
Wang, Jinsong
Jia, Baohua
Ma, Tianyi
Zhang, Zhengfu
Li, Chengping
Yi, Jianhong
Bao, Rui
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  orcidid: 0000-0002-1042-8700
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  email: tianyi.ma@rmit.edu.au
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Snippet Oxygen evolution reaction (OER) remains a bottleneck for electrocatalytic water‐splitting to generate hydrogen. However, the traditional adsorbed evolution...
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SubjectTerms adsorbed evolution mechanism
Cobalt
Coupling
Current density
Electrocatalysts
Heterostructures
Iron
lattice oxygen mechanism
Materials science
Oxidation
oxygen evolution reaction
Oxygen evolution reactions
Reaction kinetics
Stability
Water splitting
Title Coupling Adsorbed Evolution and Lattice Oxygen Mechanism in Fe‐Co(OH)2/Fe2O3 Heterostructure for Enhanced Electrochemical Water Oxidation
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fadfm.202305243
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