Effects of incorporating nanosized calcium phosphate particles on properties of whisker-reinforced dental composites
Clinical data indicate that secondary caries and restoration fracture are the most common problems facing tooth restorations. Our ultimate goal was to develop mechanically‐strong and caries‐inhibiting dental composites. The specific goal of this pilot study was to understand the relationships betwee...
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| Vydáno v: | Journal of biomedical materials research. Part B, Applied biomaterials Ročník 81B; číslo 1; s. 116 - 125 |
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| Hlavní autoři: | , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
| Vydáno: |
Hoboken
Wiley Subscription Services, Inc., A Wiley Company
01.04.2007
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| Témata: | |
| ISSN: | 1552-4973, 1552-4981 |
| On-line přístup: | Získat plný text |
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| Shrnutí: | Clinical data indicate that secondary caries and restoration fracture are the most common problems facing tooth restorations. Our ultimate goal was to develop mechanically‐strong and caries‐inhibiting dental composites. The specific goal of this pilot study was to understand the relationships between composite properties and the ratio of reinforcement filler/releasing filler. Nanoparticles of monocalcium phosphate monohydrate (MCPM) were synthesized and incorporated into a dental resin for the first time. Silicon carbide whiskers were fused with silica nanoparticles and mixed with the MCPM particles at MCPM/whisker mass ratios of 1:0, 2:1, 1:1, 1:2, and 0:1. The composites were immersed for 1–56 days to measure Ca and PO4 release. When the MCPM/whisker ratio was changed from 0:1 to 1:2, the composite flexural strength (mean ± SD; n = 5) decreased from 174 ± 26 MPa to 138 ± 9 MPa (p < 0.05). A commercial nonreleasing composite had a strength of 112 ± 14 MPa. When the MCPM/whisker ratio was changed from 1:2 to 1:1, the Ca concentration at 56 days increased from 0.77 ± 0.04 mmol/L to 1.74 ± 0.06 mmol/L (p < 0.05). The corresponding PO4 concentration increased from 3.88 ± 0.21 mmol/L to 9.95 ± 0.69 mmol/L (p < 0.05). Relationships were established between the amount of release and the MCPM volume fraction vMCPM in the resin: [Ca]= 42.9 v MCPM2.7, and [PO4] = 48.7 v MCPM1.4. In summary, the method of combining nanosized releasing fillers with reinforcing fillers yielded Ca‐ and PO4‐releasing composites with mechanical properties matching or exceeding a commercial stress‐bearing, nonreleasing composite. This method may be applicable to the use of other Ca–PO4 fillers in developing composites with high stress‐bearing and caries‐preventing capabilities, a combination not yet available in any dental materials. © 2006 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2006 |
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| Bibliografie: | ArticleID:JBM30644 ADAF NIST istex:430F246962C63FA0EB480F360F70ED23CC4E4AC8 This article is a US Government work and, as such, is in the public domain in the United States of America. ark:/67375/WNG-FXRXFFLS-W Certain commercial materials and equipment are identified to specify the experimental procedure. This does not imply recommendation or endorsement by NIST or ADAF or that the material or equipment identified is necessarily the best available for the purpose. One standard deviation was used as the estimated standard uncertainty of the measurements. These values should not be compared with data obtained in other laboratories under different conditions. This is an official contribution of the National Institute of Standards and Technology and is not subjected to copyright in the United States. NIH/NIDCR - No. R01 DE14190 ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 ObjectType-Article-1 ObjectType-Feature-2 |
| ISSN: | 1552-4973 1552-4981 |
| DOI: | 10.1002/jbm.b.30644 |