What Can Electron Microscopy Tell Us Beyond Crystal Structures?

Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and morphology, crystal orientation, crystal defects, surface structures, superstructures, etc. However, due to the 2D nature of TEM images, it is easy to...

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Veröffentlicht in:	European journal of inorganic chemistry Jg. 2016; H. 7; S. 941 - 950
Hauptverfasser:	Zhou, Wuzong, Greer, Heather F.
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	Weinheim WILEY-VCH Verlag 01.03.2016 WILEY‐VCH Verlag Wiley Subscription Services, Inc
Schlagworte:	Crystal defects Crystal growth Crystal structure Crystals Electron diffraction Electron microscopes Electron microscopy Morphology Nanostructures Scanning electron microscopy Solid-state structures Three dimensional Transmission electron microscopy
ISSN:	1434-1948, 1099-0682
Online-Zugang:	Volltext
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Abstract	Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and morphology, crystal orientation, crystal defects, surface structures, superstructures, etc. However, due to the 2D nature of TEM images, it is easy to make mistakes when we try to recover a 3D structure from them. Scanning electron microscopy is able to provide information on the particle size, morphology and surface topography. However, obtaining information on crystallinity of particles using SEM is difficult. In this microreview article, some practical cases of transmission and scanning electron microscopy investigations of inorganic crystals are reviewed. Commonly occurring uncertainties, imperfection and misunderstandings are discussed. Some examples of conventional SEM and TEM studies of inorganic crystals are reviewed. Typical problems of misinterpretation of the images are discussed.
AbstractList	Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and morphology, crystal orientation, crystal defects, surface structures, superstructures, etc. However, due to the 2D nature of TEM images, it is easy to make mistakes when we try to recover a 3D structure from them. Scanning electron microscopy is able to provide information on the particle size, morphology and surface topography. However, obtaining information on crystallinity of particles using SEM is difficult. In this microreview article, some practical cases of transmission and scanning electron microscopy investigations of inorganic crystals are reviewed. Commonly occurring uncertainties, imperfection and misunderstandings are discussed. Some examples of conventional SEM and TEM studies of inorganic crystals are reviewed. Typical problems of misinterpretation of the images are discussed. Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and morphology, crystal orientation, crystal defects, surface structures, superstructures, etc. However, due to the 2D nature of TEM images, it is easy to make mistakes when we try to recover a 3D structure from them. Scanning electron microscopy is able to provide information on the particle size, morphology and surface topography. However, obtaining information on crystallinity of particles using SEM is difficult. In this microreview article, some practical cases of transmission and scanning electron microscopy investigations of inorganic crystals are reviewed. Commonly occurring uncertainties, imperfection and misunderstandings are discussed. Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and morphology, crystal orientation, crystal defects, surface structures, superstructures, etc. However, due to the 2D nature of TEM images, it is easy to make mistakes when we try to recover a 3D structure from them. Scanning electron microscopy is able to provide information on the particle size, morphology and surface topography. However, obtaining information on crystallinity of particles using SEM is difficult. In this microreview article, some practical cases of transmission and scanning electron microscopy investigations of inorganic crystals are reviewed. Commonly occurring uncertainties, imperfection and misunderstandings are discussed. Some examples of conventional SEM and TEM studies of inorganic crystals are reviewed. Typical problems of misinterpretation of the images are discussed.
Author	Greer, Heather F. Zhou, Wuzong
Author_xml	– sequence: 1 givenname: Wuzong surname: Zhou fullname: Zhou, Wuzong email: wzhou@st-andrews.ac.uk organization: School of Chemistry, University of St Andrews St Andrews KY16 9ST, United Kingdom, http://www.st-andrews.ac.uk/chemistry/contact/academic/#wzhou – sequence: 2 givenname: Heather F. surname: Greer fullname: Greer, Heather F. organization: School of Chemistry, University of St Andrews St Andrews KY16 9ST, United Kingdom, http://www.st-andrews.ac.uk/chemistry/contact/academic/#wzhou
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Copyright	2016 The Authors. Published by WILEY‐VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited. 2016 The Authors. Published by WILEY-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
Copyright_xml	– notice: 2016 The Authors. Published by WILEY‐VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited. – notice: 2016 The Authors. Published by WILEY-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.
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Snippet	Transmission electron microscopy is a powerful tool to directly image crystal structures. Not only that, it is often used to reveal crystal size and...
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SubjectTerms	Crystal defects Crystal growth Crystal structure Crystals Electron diffraction Electron microscopes Electron microscopy Morphology Nanostructures Scanning electron microscopy Solid-state structures Three dimensional Transmission electron microscopy
Title	What Can Electron Microscopy Tell Us Beyond Crystal Structures?
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