Experimental design in pesticide extraction methods: A review
•A first of its kind review on the use of experimental design in pesticide extraction methods.•Discussed in detail the applications of experimental designs in pesticide extraction methods.•This paper is a guide to help the food scientists working on pesticide extraction in the statistical evaluation...
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| Veröffentlicht in: | Food chemistry Jg. 289; S. 384 - 395 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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England
Elsevier Ltd
15.08.2019
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| ISSN: | 0308-8146, 1873-7072, 1873-7072 |
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| Abstract | •A first of its kind review on the use of experimental design in pesticide extraction methods.•Discussed in detail the applications of experimental designs in pesticide extraction methods.•This paper is a guide to help the food scientists working on pesticide extraction in the statistical evaluation of factors.•Discussed the systemic approach of experimental design in pesticide extraction.•The extraction process in combination with experimental design is far more efficient.
The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers. |
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| AbstractList | The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers. •A first of its kind review on the use of experimental design in pesticide extraction methods.•Discussed in detail the applications of experimental designs in pesticide extraction methods.•This paper is a guide to help the food scientists working on pesticide extraction in the statistical evaluation of factors.•Discussed the systemic approach of experimental design in pesticide extraction.•The extraction process in combination with experimental design is far more efficient. The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers. The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers.The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers. |
| Author | Karri, Veera Venkata Satyanarayana Reddy Narenderan, S.T. Meyyanathan, S.N. |
| Author_xml | – sequence: 1 givenname: S.T. surname: Narenderan fullname: Narenderan, S.T. email: mail2narenderan@gmail.com organization: Department of Pharmaceutical Analysis, JSS College of Pharmacy, Udhagamandalam, JSS Academy of Higher Education & Research, Tamil Nadu, India – sequence: 2 givenname: S.N. surname: Meyyanathan fullname: Meyyanathan, S.N. organization: Department of Pharmaceutical Analysis, JSS College of Pharmacy, Udhagamandalam, JSS Academy of Higher Education & Research, Tamil Nadu, India – sequence: 3 givenname: Veera Venkata Satyanarayana Reddy surname: Karri fullname: Karri, Veera Venkata Satyanarayana Reddy organization: Department of Pharmaceutics, JSS College of Pharmacy, Udhagamandalam, JSS Academy of Higher Education & Research, Tamil Nadu, India |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30955627$$D View this record in MEDLINE/PubMed |
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| Keywords | P-B design Extraction methods BBD FFD SPE FrFD Response surface methodology SDME − SPME MIP-NPs Design of experiment DSLLME PSA RSD IL + RSM SC-CO2 α MgSO4 MISPE HS-SPME LLE-dSPE NaCl LLME Screening designs DLLME MSPD F-value USA-TFME LLE SBSE PLE Optimization OA ASE OCPs SFE ANOVA DNSUAME QuEChERS MSB OPPs p-value CCD GCB rpm Pesticide residue USL-SPE |
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| SubjectTerms | Design of experiment experimental design Extraction methods Optimization Pesticide residue pesticide residues Pesticide Residues - analysis pesticides Pesticides - analysis Pesticides - isolation & purification Research Design Response surface methodology screening Screening designs Software |
| Title | Experimental design in pesticide extraction methods: A review |
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