Experimental design in pesticide extraction methods: A review

•A first of its kind review on the use of experimental design in pesticide extraction methods.•Discussed in detail the applications of experimental designs in pesticide extraction methods.•This paper is a guide to help the food scientists working on pesticide extraction in the statistical evaluation...

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Veröffentlicht in:Food chemistry Jg. 289; S. 384 - 395
Hauptverfasser: Narenderan, S.T., Meyyanathan, S.N., Karri, Veera Venkata Satyanarayana Reddy
Format: Journal Article
Sprache:Englisch
Veröffentlicht: England Elsevier Ltd 15.08.2019
Schlagworte:
Design of experiment
experimental design
Extraction methods
Optimization
Pesticide residue
pesticide residues
Pesticide Residues - analysis
pesticides
Pesticides - analysis
Pesticides - isolation & purification
Research Design
Response surface methodology
screening
Screening designs
Software
P-B design
Extraction methods
BBD
FFD
SPE
FrFD
Response surface methodology
SDME
−
SPME
MIP-NPs
Design of experiment
DSLLME
PSA
RSD
IL
+
RSM
SC-CO2
α
MgSO4
MISPE
HS-SPME
LLE-dSPE
NaCl
LLME
Screening designs
DLLME
MSPD
F-value
USA-TFME
LLE
SBSE
PLE
Optimization
OA
ASE
OCPs
SFE
ANOVA
DNSUAME
QuEChERS
MSB
OPPs
p-value
CCD
GCB
rpm
Pesticide residue
USL-SPE
ISSN:0308-8146, 1873-7072, 1873-7072
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Zusammenfassung:•A first of its kind review on the use of experimental design in pesticide extraction methods.•Discussed in detail the applications of experimental designs in pesticide extraction methods.•This paper is a guide to help the food scientists working on pesticide extraction in the statistical evaluation of factors.•Discussed the systemic approach of experimental design in pesticide extraction.•The extraction process in combination with experimental design is far more efficient. The sample extraction process is considered as the essential step in the pesticide residue analysis, as it provides the base for the detection of the pesticides in trace level. Various factors need to be optimized during the extraction of pesticides due to the complexity of the matrix which is time-consuming and tedious. Therefore, the use of experimental design in the optimization process proves to be effective with minimum experiments and cost. This paper is aimed to overview the experimental designs that are frequently used for screening (full factorial, fractional factorial, Plackett-Burman Design) and optimizing (central composite design, Box-Behnken design, Taguchi design, Doehlert design, D-optimal design) the most influential factors to provide a sequential understanding of the linear and complex interactions in the pesticide extraction methods. Further, a systematic approach has been discussed about the use of experimental designs in pesticide extraction and also the softwares used for application-oriented readers.
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SourceType-Scholarly Journals-1
ObjectType-Feature-2
ObjectType-Review-3
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ISSN:0308-8146
1873-7072
1873-7072
DOI:10.1016/j.foodchem.2019.03.045