Reversible SC‐SC Transformation involving [4+4] Cycloaddition of Anthracene: A Single‐Ion to Single‐Molecule Magnet and Yellow‐Green to Blue‐White Emission

In search of magneto‐optic materials, the mononuclear compounds LnIII(depma)(NO3)3(hmpa)2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single‐ion to a single‐molecule magnet w...

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Vydáno v:	Angewandte Chemie International Edition Ročník 57; číslo 28; s. 8577 - 8581
Hlavní autoři:	Huang, Xin‐Da, Xu, Yan, Fan, Kun, Bao, Song‐Song, Kurmoo, Mohamedally, Zheng, Li‐Min
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Germany Wiley Subscription Services, Inc 09.07.2018
Vydání:	International ed. in English
Témata:	Anthracene Clean energy Cycloaddition Dimerization dysprosium Dysprosium compounds Emission Emissions Gadolinium Magnetic properties Molecular chains Optical materials Phosphonates photocycloaddition single-molecule magnets Smart materials Switches white light anthracene photocycloaddition dysprosium white light single-molecule magnets
ISSN:	1433-7851, 1521-3773
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Abstract	In search of magneto‐optic materials, the mononuclear compounds LnIII(depma)(NO3)3(hmpa)2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single‐ion to a single‐molecule magnet with doubling of the spin reversal barrier energy and from yellow‐green to blue‐white emission. The dimerization is reversed by heating at 100 °C or partially on light irradiating at 254 nm. The results suggest that lanthanide phosphonates with anthracene are promising smart materials displaying synergistic magneto‐optic property. Pairing up: The mononuclear compound DyIII(depma)(NO3)3(hmpa)2 (depma= 9‐diethylphosphono‐methylanthracene, hmpa=hexamethylphosphoramide) undergoes reversible [4+4] photodimerization in a single‐crystal‐to‐single‐crystal manner. This process is accompanied by a change from a single‐ion to a single‐molecule magnet and from yellow‐green to blue‐white emission.
AbstractList	In search of magneto‐optic materials, the mononuclear compounds LnIII(depma)(NO3)3(hmpa)2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single‐ion to a single‐molecule magnet with doubling of the spin reversal barrier energy and from yellow‐green to blue‐white emission. The dimerization is reversed by heating at 100 °C or partially on light irradiating at 254 nm. The results suggest that lanthanide phosphonates with anthracene are promising smart materials displaying synergistic magneto‐optic property. Pairing up: The mononuclear compound DyIII(depma)(NO3)3(hmpa)2 (depma= 9‐diethylphosphono‐methylanthracene, hmpa=hexamethylphosphoramide) undergoes reversible [4+4] photodimerization in a single‐crystal‐to‐single‐crystal manner. This process is accompanied by a change from a single‐ion to a single‐molecule magnet and from yellow‐green to blue‐white emission. In search of magneto-optic materials, the mononuclear compounds Ln (depma)(NO ) (hmpa) (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single-ion to a single-molecule magnet with doubling of the spin reversal barrier energy and from yellow-green to blue-white emission. The dimerization is reversed by heating at 100 °C or partially on light irradiating at 254 nm. The results suggest that lanthanide phosphonates with anthracene are promising smart materials displaying synergistic magneto-optic property. In search of magneto‐optic materials, the mononuclear compounds Ln III (depma)(NO 3 ) 3 (hmpa) 2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single‐ion to a single‐molecule magnet with doubling of the spin reversal barrier energy and from yellow‐green to blue‐white emission. The dimerization is reversed by heating at 100 °C or partially on light irradiating at 254 nm. The results suggest that lanthanide phosphonates with anthracene are promising smart materials displaying synergistic magneto‐optic property. In search of magneto‐optic materials, the mononuclear compounds LnIII(depma)(NO3)3(hmpa)2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4] dimerization when irradiated at 365 nm without loss of crystallinity. The Dy compound switches from a single‐ion to a single‐molecule magnet with doubling of the spin reversal barrier energy and from yellow‐green to blue‐white emission. The dimerization is reversed by heating at 100 °C or partially on light irradiating at 254 nm. The results suggest that lanthanide phosphonates with anthracene are promising smart materials displaying synergistic magneto‐optic property.
Author	Huang, Xin‐Da Xu, Yan Fan, Kun Zheng, Li‐Min Bao, Song‐Song Kurmoo, Mohamedally
Author_xml	– sequence: 1 givenname: Xin‐Da surname: Huang fullname: Huang, Xin‐Da organization: Nanjing University – sequence: 2 givenname: Yan surname: Xu fullname: Xu, Yan organization: Nanjing University – sequence: 3 givenname: Kun surname: Fan fullname: Fan, Kun organization: Nanjing University – sequence: 4 givenname: Song‐Song surname: Bao fullname: Bao, Song‐Song organization: Nanjing University – sequence: 5 givenname: Mohamedally surname: Kurmoo fullname: Kurmoo, Mohamedally organization: Universite de Strasbourg, CNRS-UMR7177 – sequence: 6 givenname: Li‐Min orcidid: 0000-0003-4437-1105 surname: Zheng fullname: Zheng, Li‐Min email: lmzheng@nju.edu.cn organization: Nanjing University
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Snippet	In search of magneto‐optic materials, the mononuclear compounds LnIII(depma)(NO3)3(hmpa)2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4]... In search of magneto‐optic materials, the mononuclear compounds Ln III (depma)(NO 3 ) 3 (hmpa) 2 (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo... In search of magneto-optic materials, the mononuclear compounds Ln (depma)(NO ) (hmpa) (Ln=Dy, Gd) were synthesized. The anthracene moieties undergo [4+4]...
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SubjectTerms	Anthracene Clean energy Cycloaddition Dimerization dysprosium Dysprosium compounds Emission Emissions Gadolinium Magnetic properties Molecular chains Optical materials Phosphonates photocycloaddition single-molecule magnets Smart materials Switches white light
Title	Reversible SC‐SC Transformation involving [4+4] Cycloaddition of Anthracene: A Single‐Ion to Single‐Molecule Magnet and Yellow‐Green to Blue‐White Emission
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