The role of metal–support interaction in Ag/CeO2 catalysts for CO and soot oxidation
[Display omitted] •Method of preparation of Ag/CeO2 catalysts determines the features of the MSI.•Redox reaction between Ce3+ and Ag+ during catalyst synthesis lead to MSI.•Epitaxial growth of Ag NPs (d111 = 2.35 Å) occurs on CeO2 surface (d111 = 3.1 Å).•Enhanced interfacial Ag–CeO2 interaction incr...
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| Vydané v: | Applied catalysis. B, Environmental Ročník 260; s. 118148 |
|---|---|
| Hlavní autori: | , , , , , |
| Médium: | Journal Article |
| Jazyk: | English |
| Vydavateľské údaje: |
Amsterdam
Elsevier B.V
01.01.2020
Elsevier BV |
| Predmet: | |
| ISSN: | 0926-3373, 1873-3883 |
| On-line prístup: | Získať plný text |
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| Abstract | [Display omitted]
•Method of preparation of Ag/CeO2 catalysts determines the features of the MSI.•Redox reaction between Ce3+ and Ag+ during catalyst synthesis lead to MSI.•Epitaxial growth of Ag NPs (d111 = 2.35 Å) occurs on CeO2 surface (d111 = 3.1 Å).•Enhanced interfacial Ag–CeO2 interaction increases the amount of active oxygen species.•MSI in Ag/CeO2 catalysts enhances their activity in CO and soot oxidation.
Ag/CeO2 catalysts with a silver loading of 10 wt.% have been prepared by three different techniques: impregnation, Ag/CeO2 (imp), impregnation of prereduced CeO2, Ag/CeO2 (red-imp), and co-deposition precipitation, Ag-CeO2 (co-DP). The features of the prepared composites have been studied by low-temperature N2 sorption, TGA, XRF, TPR-H2, TEM HR, XPS and Raman spectroscopy. The Raman and XPS results show that the addition of silver to CeO2 significantly increases the defectiveness of CeO2 particles, and such an effect is a function of the preparation method. The Ag-CeO2 (co-DP) and Ag/CeO2 (red-imp) catalysts show enhanced interfacial Ag–CeO2 interaction caused by the epitaxial growth of silver particles (d111 = 2.35 Å) on the CeO2 surface (d111 = 3.1 Å) as well as high amount of oxygen vacancies. A morphology-dependent interplay between the oxygen vacancies and the strength of the Ag–CeO2 interaction has been revealed. Strengthening of the metal–support interaction enhances the catalytic activity of the composites in both CO oxidation and soot combustion. |
|---|---|
| AbstractList | Ag/CeO2 catalysts with a silver loading of 10 wt.% have been prepared by three different techniques: impregnation, Ag/CeO2 (imp), impregnation of prereduced CeO2, Ag/CeO2 (red-imp), and co-deposition precipitation, Ag-CeO2 (co-DP). The features of the prepared composites have been studied by low-temperature N2 sorption, TGA, XRF, TPR-H2, TEM HR, XPS and Raman spectroscopy. The Raman and XPS results show that the addition of silver to CeO2 significantly increases the defectiveness of CeO2 particles, and such an effect is a function of the preparation method. The Ag-CeO2 (co-DP) and Ag/CeO2 (red-imp) catalysts show enhanced interfacial Ag–CeO2 interaction caused by the epitaxial growth of silver particles (d111 = 2.35 Å) on the CeO2 surface (d111 = 3.1 Å) as well as high amount of oxygen vacancies. A morphology-dependent interplay between the oxygen vacancies and the strength of the Ag–CeO2 interaction has been revealed. Strengthening of the metal–support interaction enhances the catalytic activity of the composites in both CO oxidation and soot combustion. [Display omitted] •Method of preparation of Ag/CeO2 catalysts determines the features of the MSI.•Redox reaction between Ce3+ and Ag+ during catalyst synthesis lead to MSI.•Epitaxial growth of Ag NPs (d111 = 2.35 Å) occurs on CeO2 surface (d111 = 3.1 Å).•Enhanced interfacial Ag–CeO2 interaction increases the amount of active oxygen species.•MSI in Ag/CeO2 catalysts enhances their activity in CO and soot oxidation. Ag/CeO2 catalysts with a silver loading of 10 wt.% have been prepared by three different techniques: impregnation, Ag/CeO2 (imp), impregnation of prereduced CeO2, Ag/CeO2 (red-imp), and co-deposition precipitation, Ag-CeO2 (co-DP). The features of the prepared composites have been studied by low-temperature N2 sorption, TGA, XRF, TPR-H2, TEM HR, XPS and Raman spectroscopy. The Raman and XPS results show that the addition of silver to CeO2 significantly increases the defectiveness of CeO2 particles, and such an effect is a function of the preparation method. The Ag-CeO2 (co-DP) and Ag/CeO2 (red-imp) catalysts show enhanced interfacial Ag–CeO2 interaction caused by the epitaxial growth of silver particles (d111 = 2.35 Å) on the CeO2 surface (d111 = 3.1 Å) as well as high amount of oxygen vacancies. A morphology-dependent interplay between the oxygen vacancies and the strength of the Ag–CeO2 interaction has been revealed. Strengthening of the metal–support interaction enhances the catalytic activity of the composites in both CO oxidation and soot combustion. |
| ArticleNumber | 118148 |
| Author | Zaikovskii, V.I. Vodyankina, O.V. Liotta, L.F. Mamontov, G.V. Grabchenko, M.V. La Parola, V. |
| Author_xml | – sequence: 1 givenname: M.V. surname: Grabchenko fullname: Grabchenko, M.V. organization: Tomsk State University, 36, Lenin ave., 634050, Tomsk, Russia – sequence: 2 givenname: G.V. orcidid: 0000-0001-7007-8389 surname: Mamontov fullname: Mamontov, G.V. organization: Tomsk State University, 36, Lenin ave., 634050, Tomsk, Russia – sequence: 3 givenname: V.I. surname: Zaikovskii fullname: Zaikovskii, V.I. organization: Boreskov Institute of Catalysis, 5, Lavrentiev ave., 630090, Novosibirsk, Russia – sequence: 4 givenname: V. surname: La Parola fullname: La Parola, V. organization: Istituto per lo Studio dei Materiali Nanostrutturati (ISMN)-CNR, 153, via Ugo La Malfa, 90146, Palermo, Italy – sequence: 5 givenname: L.F. surname: Liotta fullname: Liotta, L.F. email: leonardafrancesca.liotta@cnr.it organization: Istituto per lo Studio dei Materiali Nanostrutturati (ISMN)-CNR, 153, via Ugo La Malfa, 90146, Palermo, Italy – sequence: 6 givenname: O.V. orcidid: 0000-0003-1221-8851 surname: Vodyankina fullname: Vodyankina, O.V. email: vodyankina_o@mail.ru organization: Tomsk State University, 36, Lenin ave., 634050, Tomsk, Russia |
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| Keywords | Ag/CeO2 Metal–support interaction Soot combustion Epitaxial growth of silver particles CO oxidation |
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•Method of preparation of Ag/CeO2 catalysts determines the features of the MSI.•Redox reaction between Ce3+ and Ag+ during catalyst synthesis... Ag/CeO2 catalysts with a silver loading of 10 wt.% have been prepared by three different techniques: impregnation, Ag/CeO2 (imp), impregnation of prereduced... |
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| SubjectTerms | Ag/CeO2 Catalysts Catalytic activity Cerium oxides CO oxidation Composite materials Epitaxial growth Epitaxial growth of silver particles Impregnation Lattice vacancies Low temperature Metal–support interaction Morphology Oxidation Oxygen Raman spectroscopy Silver Soot Soot combustion Vacancies X ray photoelectron spectroscopy |
| Title | The role of metal–support interaction in Ag/CeO2 catalysts for CO and soot oxidation |
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