Recovery of cathode copper and ternary precursors from CuS slag derived by waste lithium-ion batteries: Process analysis and evaluation

The efficient and environmentally friendly recycling technology of waste residue that including abundant heavy metal produced during the recovery of lithium batteries has become a research hotspot. Herein, a novelty process of acid leaching-selective electrodeposition-deep impurity removal-regenerat...

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Vydáno v:Chinese chemical letters Ročník 35; číslo 7; s. 109172 - 182
Hlavní autoři: Wei, Yun, Zhou, Lei, Hu, Wenbin, Yang, Liming, Yang, Guang, Wang, Chaoqiang, Shi, Hui, Han, Fei, Feng, Yufa, Ding, Xuan, Shao, Penghui, Luo, Xubiao
Médium: Journal Article
Jazyk:angličtina
Vydáno: Elsevier B.V 01.07.2024
National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China%CAS Key Laboratory of Green Process and Engineering,National Engineering Research Center of Green Recycling for Strategic Metal Resources,Institute of Process Engineering,Chinese Academy of Sciences,Beijing 100190,China%Biomass Molecular Engineering Center and Anhui Provincial Key Laboratory of Microbial Pest Control,Anhui Agricultural University,Hefei 230036,China%Jiangxi Ganfeng Recycling Technology Co.LTD.,Xinyu 338004,China%National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China
School of Life Science,Jinggangshan University,Ji'an 343009,China
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ISSN:1001-8417, 1878-5964
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Abstract The efficient and environmentally friendly recycling technology of waste residue that including abundant heavy metal produced during the recovery of lithium batteries has become a research hotspot. Herein, a novelty process of acid leaching-selective electrodeposition-deep impurity removal-regeneration was proposed to recovery of the CuS slag, which has been efficient transferred to high purity cathode copper and commercially available ternary precursors. Copper cathode with a purity of 99.67% was prepared under electrochemical reaction conditions at −0.55 V for 2 h. A novel impurity remover-Mn powder, which was used to remove the residual impurities and as a feedstock for the ternary precursor. Finally, NCM523 was regenerated by co-precipitation. The process is superior to the traditional process in economy, energy consumption, CO2 emissions, product purity and process duration. This study provides a new approach for solid waste recovery and precious metal enrichment. For the resourceful recovery of secondary waste from retired lithium-ion batteries, a novel process of acid leaching-selective electrodeposition-deep decontamination-regeneration was proposed to recover CuS slag, and regenerate it efficiently with high-purity cathode copper and commercially available ternary precursors. A new pathway for solid waste recovery and precious metal enrichment is provided. [Display omitted]
AbstractList The efficient and environmentally friendly recycling technology of waste residue that including abundant heavy metal produced during the recovery of lithium batteries has become a research hotspot. Herein, a novelty process of acid leaching-selective electrodeposition-deep impurity removal-regeneration was proposed to recovery of the CuS slag, which has been efficient transferred to high purity cathode copper and commercially available ternary precursors. Copper cathode with a purity of 99.67% was prepared under electrochemical reaction conditions at −0.55 V for 2 h. A novel impurity remover-Mn powder, which was used to remove the residual impurities and as a feedstock for the ternary precursor. Finally, NCM523 was regenerated by co-precipitation. The process is superior to the traditional process in economy, energy consumption, CO2 emissions, product purity and process duration. This study provides a new approach for solid waste recovery and precious metal enrichment. For the resourceful recovery of secondary waste from retired lithium-ion batteries, a novel process of acid leaching-selective electrodeposition-deep decontamination-regeneration was proposed to recover CuS slag, and regenerate it efficiently with high-purity cathode copper and commercially available ternary precursors. A new pathway for solid waste recovery and precious metal enrichment is provided. [Display omitted]
The efficient and environmentally friendly recycling technology of waste residue that including abundant heavy metal produced during the recovery of lithium batteries has become a research hotspot.Herein,a novelty process of acid leaching-selective electrodeposition-deep impurity removal-regeneration was pro-posed to recovery of the CuS slag,which has been efficient transferred to high purity cathode copper and commercially available ternary precursors.Copper cathode with a purity of 99.67% was prepared under electrochemical reaction conditions at-0.55 V for 2h.A novel impurity remover-Mn powder,which was used to remove the residual impurities and as a feedstock for the ternary precursor.Finally,NCM523 was regenerated by co-precipitation.The process is superior to the traditional process in economy,energy consumption,CO2 emissions,product purity and process duration.This study provides a new approach for solid waste recovery and precious metal enrichment.
ArticleNumber 109172
Author Yang, Liming
Han, Fei
Yang, Guang
Ding, Xuan
Shi, Hui
Wei, Yun
Zhou, Lei
Wang, Chaoqiang
Feng, Yufa
Hu, Wenbin
Luo, Xubiao
Shao, Penghui
AuthorAffiliation National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China%CAS Key Laboratory of Green Process and Engineering,National Engineering Research Center of Green Recycling for Strategic Metal Resources,Institute of Process Engineering,Chinese Academy of Sciences,Beijing 100190,China%Biomass Molecular Engineering Center and Anhui Provincial Key Laboratory of Microbial Pest Control,Anhui Agricultural University,Hefei 230036,China%Jiangxi Ganfeng Recycling Technology Co.LTD.,Xinyu 338004,China%National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China;School of Life Science,Jinggangshan University,Ji'an 343009,China
AuthorAffiliation_xml – name: National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China%CAS Key Laboratory of Green Process and Engineering,National Engineering Research Center of Green Recycling for Strategic Metal Resources,Institute of Process Engineering,Chinese Academy of Sciences,Beijing 100190,China%Biomass Molecular Engineering Center and Anhui Provincial Key Laboratory of Microbial Pest Control,Anhui Agricultural University,Hefei 230036,China%Jiangxi Ganfeng Recycling Technology Co.LTD.,Xinyu 338004,China%National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China;School of Life Science,Jinggangshan University,Ji'an 343009,China
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Issue 7
Keywords Cathode copper
Ternary precursor
Electrodeposition
Solid waste recovery
CuS slag
Language English
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National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China%CAS Key Laboratory of Green Process and Engineering,National Engineering Research Center of Green Recycling for Strategic Metal Resources,Institute of Process Engineering,Chinese Academy of Sciences,Beijing 100190,China%Biomass Molecular Engineering Center and Anhui Provincial Key Laboratory of Microbial Pest Control,Anhui Agricultural University,Hefei 230036,China%Jiangxi Ganfeng Recycling Technology Co.LTD.,Xinyu 338004,China%National-Local Joint Engineering Research Center of Heavy Metals Pollutants Control and Resource Utilization,Nanchang Hangkong University,Nanchang 330063,China
School of Life Science,Jinggangshan University,Ji'an 343009,China
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Snippet The efficient and environmentally friendly recycling technology of waste residue that including abundant heavy metal produced during the recovery of lithium...
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StartPage 109172
SubjectTerms Cathode copper
CuS slag
Electrodeposition
Solid waste recovery
Ternary precursor
Title Recovery of cathode copper and ternary precursors from CuS slag derived by waste lithium-ion batteries: Process analysis and evaluation
URI https://dx.doi.org/10.1016/j.cclet.2023.109172
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