Synthesis of pure nano Cr2O3 from chromite ore by a novel method and investigation of its composites with bentonite for their photocatalytic properties
In the present study, nano Cr 2 O 3 was prepared with a novel method from chromite ore. In this method, K 2 Cr 2 O 7 was prepared by alkaline melting of chromite ore. Then, the precursor complex K 3 [Cr(C 2 O 4 ) 3 ] was prepared using potassium dichromate obtained from chromite ore and Merck Co. fo...
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| Published in: | Journal of the Iranian Chemical Society Vol. 20; no. 11; pp. 2805 - 2819 |
|---|---|
| Main Authors: | , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
Berlin/Heidelberg
Springer Berlin Heidelberg
01.11.2023
Springer Nature B.V |
| Subjects: | |
| ISSN: | 1735-207X, 1735-2428 |
| Online Access: | Get full text |
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| Abstract | In the present study, nano Cr
2
O
3
was prepared with a novel method from chromite ore. In this method, K
2
Cr
2
O
7
was prepared by alkaline melting of chromite ore. Then, the precursor complex K
3
[Cr(C
2
O
4
)
3
] was prepared using potassium dichromate obtained from chromite ore and Merck Co. for comparing their purity. Therefore, two types of nano (Cr
2
O
3
)
M or ch
(M = Merck, ch = chromite ore) were prepared by destructing the gel contained K
3
[Cr(C
2
O
4
)
3
] and starch as an eco-friendly material for controlling the size and morphology of the nanoparticles. So, these nanoparticles were characterized by XRD, FESEM, and EDX. The ball-milled bentonite (B) was used for the preparation of (Cr
2
O
3
(n% = 30, 50, and 70%)/B)
ch
and (Cr
2
O
3
(n% = 30, 50%)/B)
M
nanocomposites. The XRD and FESEM of (Cr
2
O
3
(n%)/B)
ch
and (Cr
2
O
3
(n%)/B)
M
are the same. So, the (Cr
2
O
3
(n%)/B)
ch
nanocomposites were just used for further investigations, such as photocatalytic properties, and analysed by other techniques, including FTIR and DRS. The (Cr
2
O
3
(30%)/B)
ch
showed the highest degradation property, 69% after 240 min, among other prepared nanocomposites to destroy methylene blue with 10 ppm concentration at pH = 10 under UV irradiation. Also, the (Cr
2
O
3
(30%)/B)
ch
could degrade methyl orange with 10 ppm concentration at pH = 7 up to 74% after 240 min. Nano Cr
2
O
3
and bare bentonite efficiency for methylene blue and methyl orange degradation were lower (< 30%) under the same conditions. |
|---|---|
| AbstractList | In the present study, nano Cr
2
O
3
was prepared with a novel method from chromite ore. In this method, K
2
Cr
2
O
7
was prepared by alkaline melting of chromite ore. Then, the precursor complex K
3
[Cr(C
2
O
4
)
3
] was prepared using potassium dichromate obtained from chromite ore and Merck Co. for comparing their purity. Therefore, two types of nano (Cr
2
O
3
)
M or ch
(M = Merck, ch = chromite ore) were prepared by destructing the gel contained K
3
[Cr(C
2
O
4
)
3
] and starch as an eco-friendly material for controlling the size and morphology of the nanoparticles. So, these nanoparticles were characterized by XRD, FESEM, and EDX. The ball-milled bentonite (B) was used for the preparation of (Cr
2
O
3
(n% = 30, 50, and 70%)/B)
ch
and (Cr
2
O
3
(n% = 30, 50%)/B)
M
nanocomposites. The XRD and FESEM of (Cr
2
O
3
(n%)/B)
ch
and (Cr
2
O
3
(n%)/B)
M
are the same. So, the (Cr
2
O
3
(n%)/B)
ch
nanocomposites were just used for further investigations, such as photocatalytic properties, and analysed by other techniques, including FTIR and DRS. The (Cr
2
O
3
(30%)/B)
ch
showed the highest degradation property, 69% after 240 min, among other prepared nanocomposites to destroy methylene blue with 10 ppm concentration at pH = 10 under UV irradiation. Also, the (Cr
2
O
3
(30%)/B)
ch
could degrade methyl orange with 10 ppm concentration at pH = 7 up to 74% after 240 min. Nano Cr
2
O
3
and bare bentonite efficiency for methylene blue and methyl orange degradation were lower (< 30%) under the same conditions. In the present study, nano Cr2O3 was prepared with a novel method from chromite ore. In this method, K2Cr2O7 was prepared by alkaline melting of chromite ore. Then, the precursor complex K3[Cr(C2O4)3] was prepared using potassium dichromate obtained from chromite ore and Merck Co. for comparing their purity. Therefore, two types of nano (Cr2O3)M or ch (M = Merck, ch = chromite ore) were prepared by destructing the gel contained K3[Cr(C2O4)3] and starch as an eco-friendly material for controlling the size and morphology of the nanoparticles. So, these nanoparticles were characterized by XRD, FESEM, and EDX. The ball-milled bentonite (B) was used for the preparation of (Cr2O3(n% = 30, 50, and 70%)/B)ch and (Cr2O3(n% = 30, 50%)/B)M nanocomposites. The XRD and FESEM of (Cr2O3(n%)/B)ch and (Cr2O3(n%)/B)M are the same. So, the (Cr2O3(n%)/B)ch nanocomposites were just used for further investigations, such as photocatalytic properties, and analysed by other techniques, including FTIR and DRS. The (Cr2O3(30%)/B)ch showed the highest degradation property, 69% after 240 min, among other prepared nanocomposites to destroy methylene blue with 10 ppm concentration at pH = 10 under UV irradiation. Also, the (Cr2O3(30%)/B)ch could degrade methyl orange with 10 ppm concentration at pH = 7 up to 74% after 240 min. Nano Cr2O3 and bare bentonite efficiency for methylene blue and methyl orange degradation were lower (< 30%) under the same conditions. |
| Author | Fazli-Shokouhi, Sara Khatamian, Maasoumeh Dastar, Elham Hosseini Nami, Shamin |
| Author_xml | – sequence: 1 givenname: Maasoumeh orcidid: 0000-0002-4405-1294 surname: Khatamian fullname: Khatamian, Maasoumeh email: khatamian@tabrizu.ac.ir organization: Department of Inorganic Chemistry, Faculty of Chemistry, University of Tabriz – sequence: 2 givenname: Elham surname: Dastar fullname: Dastar, Elham organization: Department of Inorganic Chemistry, Faculty of Chemistry, University of Tabriz – sequence: 3 givenname: Sara surname: Fazli-Shokouhi fullname: Fazli-Shokouhi, Sara organization: Faculty of Materials Engineering, Sahand University of Technology – sequence: 4 givenname: Shamin surname: Hosseini Nami fullname: Hosseini Nami, Shamin organization: Faculty of Chemical and Petroleum Engineering, University of Tabriz |
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| ContentType | Journal Article |
| Copyright | Iranian Chemical Society 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Iranian Chemical Society 2023. |
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| Keywords | Bentonite Chromium oxide/bentonite nanocomposite Photocatalyst Nano chromium oxide Chromite ore |
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| Snippet | In the present study, nano Cr
2
O
3
was prepared with a novel method from chromite ore. In this method, K
2
Cr
2
O
7
was prepared by alkaline melting of... In the present study, nano Cr2O3 was prepared with a novel method from chromite ore. In this method, K2Cr2O7 was prepared by alkaline melting of chromite ore.... |
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| SubjectTerms | Analytical Chemistry Bentonite Biochemistry Chemistry Chemistry and Materials Science Chromite Chromium oxides Degradation Dyes Electron microscopes Fourier transforms Inorganic Chemistry Investigations Methods Methylene blue Nanocomposites Nanoparticles Organic Chemistry Original Paper Particle size Photocatalysis Physical Chemistry Pollutants Potassium Potassium dichromate Scanning electron microscopy Semiconductors Ultraviolet radiation Water Water pollution |
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| Title | Synthesis of pure nano Cr2O3 from chromite ore by a novel method and investigation of its composites with bentonite for their photocatalytic properties |
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