Siloxene‐Functionalized Laser‐Induced Graphene via COSi Bonding for High‐Performance Heavy Metal Sensing Patch Applications
Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG...
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| Vydáno v: | Small (Weinheim an der Bergstrasse, Germany) Ročník 18; číslo 25; s. e2201247 - n/a |
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| Abstract | Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene‐CNT/LIG‐based Cu‐ion sensor shows linear response within a wide range of 10–500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu‐ion sensor. The polyaniline‐deposited pH sensor demonstrates a good sensitivity of −64.81 mV pH−1 over the pH range of 3–10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C−1 (correlation coefficient of 0.139% °C−1). The flexible hybrid sensor is promising in applications of noninvasive heavy‐metal ion detection and prediction of related diseases.
A flexible hybrid sensor based on Siloxene/LIG is newly developed for the noninvasive and accurate detection of Cu ions, pH, and temperature simultaneously. The laser‐induced graphene/polydimethylsiloxane is decorated with Siloxene‐based materials via a newly generated COSi bond to ultimately functionalize the electrodes into different sensors for multiple analyses of human perspiration. |
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| AbstractList | Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser-induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene-CNT/LIG-based Cu-ion sensor shows linear response within a wide range of 10-500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu-ion sensor. The polyaniline-deposited pH sensor demonstrates a good sensitivity of -64.81 mV pH
over the pH range of 3-10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C
(correlation coefficient of 0.139% °C
). The flexible hybrid sensor is promising in applications of noninvasive heavy-metal ion detection and prediction of related diseases. Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser-induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene-CNT/LIG-based Cu-ion sensor shows linear response within a wide range of 10-500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu-ion sensor. The polyaniline-deposited pH sensor demonstrates a good sensitivity of -64.81 mV pH-1 over the pH range of 3-10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C-1 (correlation coefficient of 0.139% °C-1 ). The flexible hybrid sensor is promising in applications of noninvasive heavy-metal ion detection and prediction of related diseases.Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser-induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene-CNT/LIG-based Cu-ion sensor shows linear response within a wide range of 10-500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu-ion sensor. The polyaniline-deposited pH sensor demonstrates a good sensitivity of -64.81 mV pH-1 over the pH range of 3-10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C-1 (correlation coefficient of 0.139% °C-1 ). The flexible hybrid sensor is promising in applications of noninvasive heavy-metal ion detection and prediction of related diseases. Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene‐CNT/LIG‐based Cu‐ion sensor shows linear response within a wide range of 10–500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu‐ion sensor. The polyaniline‐deposited pH sensor demonstrates a good sensitivity of −64.81 mV pH−1 over the pH range of 3–10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C−1 (correlation coefficient of 0.139% °C−1). The flexible hybrid sensor is promising in applications of noninvasive heavy‐metal ion detection and prediction of related diseases. A flexible hybrid sensor based on Siloxene/LIG is newly developed for the noninvasive and accurate detection of Cu ions, pH, and temperature simultaneously. The laser‐induced graphene/polydimethylsiloxane is decorated with Siloxene‐based materials via a newly generated COSi bond to ultimately functionalize the electrodes into different sensors for multiple analyses of human perspiration. Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene‐CNT/LIG‐based Cu‐ion sensor shows linear response within a wide range of 10–500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu‐ion sensor. The polyaniline‐deposited pH sensor demonstrates a good sensitivity of −64.81 mV pH−1 over the pH range of 3–10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C−1 (correlation coefficient of 0.139% °C−1). The flexible hybrid sensor is promising in applications of noninvasive heavy‐metal ion detection and prediction of related diseases. Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical properties of LIG, and improve the heterogeneous electron transfer rate. Meanwhile, the newly generated COSi crosslink boosts the binding of LIG and Siloxene. Thus, the Siloxene/LIG composite is used as the basic electrode material for the multifunctional detection of copper (Cu) ions, pH, and temperature in human perspiration. Moreover, to enhance the sensing performance of Cu ions, Siloxene/LIG is further modified by carbon nanotubes (CNTs). The fabricated Siloxene‐CNT/LIG‐based Cu‐ion sensor shows linear response within a wide range of 10–500 ppb and a low detection limit of 1.55 ppb. In addition, a pH sensor is integrated to calibrate for determining the accurate concentration of Cu ions due to pH dependency of the Cu‐ion sensor. The polyaniline‐deposited pH sensor demonstrates a good sensitivity of −64.81 mV pH −1 over the pH range of 3–10. Furthermore, a temperature sensor for accurate skin temperature monitoring is also integrated and exhibits a stable linear resistance response with an excellent sensitivity of 9.147 Ω °C −1 (correlation coefficient of 0.139% °C −1 ). The flexible hybrid sensor is promising in applications of noninvasive heavy‐metal ion detection and prediction of related diseases. |
| Author | Sharifuzzaman, Md Zahed, Md Abu Shin, Young Do Sharma, Sudeep Park, Jae Yeong Hui, Xue Seonu, Soo Kyeong Song, Hye Su |
| Author_xml | – sequence: 1 givenname: Xue surname: Hui fullname: Hui, Xue organization: Kwangwoon University – sequence: 2 givenname: Sudeep surname: Sharma fullname: Sharma, Sudeep organization: Kwangwoon University – sequence: 3 givenname: Md surname: Sharifuzzaman fullname: Sharifuzzaman, Md organization: Kwangwoon University – sequence: 4 givenname: Md Abu surname: Zahed fullname: Zahed, Md Abu organization: Kwangwoon University – sequence: 5 givenname: Young Do surname: Shin fullname: Shin, Young Do organization: Kwangwoon University – sequence: 6 givenname: Soo Kyeong surname: Seonu fullname: Seonu, Soo Kyeong organization: Kwangwoon University – sequence: 7 givenname: Hye Su surname: Song fullname: Song, Hye Su organization: Kwangwoon University – sequence: 8 givenname: Jae Yeong orcidid: 0000-0002-2056-5151 surname: Park fullname: Park, Jae Yeong email: jaepark@kw.ac.kr organization: Kwangwoon University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/35595710$$D View this record in MEDLINE/PubMed |
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| Keywords | flexible hybrid perspiration sensors noninvasive Cu ions detection Siloxene-functionalized laser-induced graphene pH calibration C O Si bonds |
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| Snippet | Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser‐induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical... Here, 2D Siloxene nanosheets are newly applied to functionalize porous laser-induced graphene (LIG) on polydimethylsiloxane, modify the surface chemical... |
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| SubjectTerms | C O Si bonds Carbon nanotubes Chemical properties Copper Correlation coefficients Electrode materials Electron transfer flexible hybrid perspiration sensors Graphene Heavy metals Ion detectors Nanotechnology noninvasive Cu ions detection Perspiration pH calibration Polyanilines Polydimethylsiloxane Sensitivity Sensors Siloxene‐functionalized laser‐induced graphene Skin temperature Temperature sensors |
| Title | Siloxene‐Functionalized Laser‐Induced Graphene via COSi Bonding for High‐Performance Heavy Metal Sensing Patch Applications |
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