Syntheses and crystal structures of lutetium(III) and dysprosium(III) coordination polymers with 2,5-dihydroxybenzene-1,4-dicarboxylate anion: Magnetic and photoluminescent properties of the dysprosium complex
[Display omitted] •Lutetium (III), 1 and dysprosium (III), 2 coordination polymers were synthesized.•Characterized by CHN analysis, IR spectroscopy, TGA-DSC and X-ray crystallography.• 3D MOF encapsulating elongated channels propagating in the [100] direction.•Magnetic susceptibility measurement sho...
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| Veröffentlicht in: | Polyhedron Jg. 189; S. 114732 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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01.10.2020
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| ISSN: | 0277-5387 |
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| Abstract | [Display omitted]
•Lutetium (III), 1 and dysprosium (III), 2 coordination polymers were synthesized.•Characterized by CHN analysis, IR spectroscopy, TGA-DSC and X-ray crystallography.• 3D MOF encapsulating elongated channels propagating in the [100] direction.•Magnetic susceptibility measurement shows compound 2 obeys the Curie Weiss law.
Lutetium(III) and dysprosium(III) coordination polymers containing the 2,5-dihydroxybenzene1,4-dicarboxylate (Dhbdc, C8H4O62−) ligand, [Lu(Dhbdc)1.5(H2O)4]n·nC2H6O·nH2O (1) and [Dy(Dhbdc)1.5(H2O)3.58(C2H6O)0.42]n·nC2H6O·0.42nH2O (2) have been prepared from a mixed solvent system and characterized by elemental analysis, infrared spectroscopy, TGA–DSC and X-ray crystallography. The crystal structural analysis reveals that 1 and 2 are almost isostructural, differing slightly in the coordination of the solvent molecules to the respective metal ions. The coordination polyhedra around the metal atoms in 1 and 2 can be described as distorted LnO8 triangular dodecahedra. The structures of the complexes are extended into three-dimensional metal-organic frameworks encapsulating elongated channels propagating in the [100] direction. In both compounds, OH…O hydrogen bonds arising from the coordinated water and solvent molecules help to consolidate the structures. Magnetic susceptibility (χm) measurements were carried out for complex 2, which was found to obey the Curie Weiss law.
Luminescent studies of complex 2 indicate that it displays enhanced ligand-centred fluorescence. |
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| AbstractList | [Display omitted]
•Lutetium (III), 1 and dysprosium (III), 2 coordination polymers were synthesized.•Characterized by CHN analysis, IR spectroscopy, TGA-DSC and X-ray crystallography.• 3D MOF encapsulating elongated channels propagating in the [100] direction.•Magnetic susceptibility measurement shows compound 2 obeys the Curie Weiss law.
Lutetium(III) and dysprosium(III) coordination polymers containing the 2,5-dihydroxybenzene1,4-dicarboxylate (Dhbdc, C8H4O62−) ligand, [Lu(Dhbdc)1.5(H2O)4]n·nC2H6O·nH2O (1) and [Dy(Dhbdc)1.5(H2O)3.58(C2H6O)0.42]n·nC2H6O·0.42nH2O (2) have been prepared from a mixed solvent system and characterized by elemental analysis, infrared spectroscopy, TGA–DSC and X-ray crystallography. The crystal structural analysis reveals that 1 and 2 are almost isostructural, differing slightly in the coordination of the solvent molecules to the respective metal ions. The coordination polyhedra around the metal atoms in 1 and 2 can be described as distorted LnO8 triangular dodecahedra. The structures of the complexes are extended into three-dimensional metal-organic frameworks encapsulating elongated channels propagating in the [100] direction. In both compounds, OH…O hydrogen bonds arising from the coordinated water and solvent molecules help to consolidate the structures. Magnetic susceptibility (χm) measurements were carried out for complex 2, which was found to obey the Curie Weiss law.
Luminescent studies of complex 2 indicate that it displays enhanced ligand-centred fluorescence. |
| ArticleNumber | 114732 |
| Author | Ahmad, Saeed Chen, Xuenian Harrison, William T.A. Sharif, Shahzad Alarfaji, Saleh S. Hussain, Sajjad |
| Author_xml | – sequence: 1 givenname: Sajjad surname: Hussain fullname: Hussain, Sajjad email: sajjaduet07@yahoo.com organization: School of Chemistry and Chemical Engineering, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Henan Normal University, Xinxiang 453007, China – sequence: 2 givenname: Saeed surname: Ahmad fullname: Ahmad, Saeed organization: Department of Chemistry, College of Sciences and Humanities, Prince Sattam Bin Abdulaziz University, Al-Kharj 11942, Saudi Arabia – sequence: 3 givenname: Shahzad surname: Sharif fullname: Sharif, Shahzad organization: Materials Chemistry Laboratory, Department of Chemistry, Government College University, Lahore 54000, Pakistan – sequence: 4 givenname: Saleh S. surname: Alarfaji fullname: Alarfaji, Saleh S. organization: Department of Chemistry, Faculty of Science, King Khalid University, P.O. Box 9004, Abha 61413, Saudi Arabia – sequence: 5 givenname: William T.A. surname: Harrison fullname: Harrison, William T.A. organization: Department of Chemistry, University of Aberdeen, Aberdeen AB24 3UE, United Kingdom – sequence: 6 givenname: Xuenian surname: Chen fullname: Chen, Xuenian email: xnchen@htu.edu.cn organization: School of Chemistry and Chemical Engineering, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Henan Normal University, Xinxiang 453007, China |
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| Keywords | magnetic properties 2,5-dihydroxybenzene-1,4-dicarboxylic acid dysprosium(III) crystal structures coordination polymer Lutetium(III) |
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•Lutetium (III), 1 and dysprosium (III), 2 coordination polymers were synthesized.•Characterized by CHN analysis, IR spectroscopy, TGA-DSC... |
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| SubjectTerms | 2,5-dihydroxybenzene-1,4-dicarboxylic acid coordination polymer crystal structures dysprosium(III) Lutetium(III) magnetic properties |
| Title | Syntheses and crystal structures of lutetium(III) and dysprosium(III) coordination polymers with 2,5-dihydroxybenzene-1,4-dicarboxylate anion: Magnetic and photoluminescent properties of the dysprosium complex |
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