Particles for multiplexed analysis in solution: detection and identification of striped metallic particles using optical microscopy

In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished in an optical microscope. Accurate particle identification is discussed relative to synthesis reproducibility and the limitations of optical m...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Analytical chemistry (Washington) Jg. 74; H. 10; S. 2240
Hauptverfasser: Walton, Ian D, Norton, Scott M, Balasingham, Arjuna, He, Lin, Oviso, Jr, Dominador F, Gupta, Dimpy, Raju, Paul A, Natan, Michael J, Freeman, R Griffith
Format: Journal Article
Sprache:Englisch
Veröffentlicht: United States 15.05.2002
Schlagworte:
ISSN:0003-2700
Online-Zugang:Weitere Angaben
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Abstract In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished in an optical microscope. Accurate particle identification is discussed relative to synthesis reproducibility and the limitations of optical microscopes. Results from a library of these particles, of which over 100 different striping patterns have been produced, are presented. For these particles, made with Au and Ag stripes, more than 70 patterns may be identified with greater than 90% accuracy. The ability to chemically modify the surface of these particles, making them useful for bioanalytical measurements, is also demonstrated. Finally, we discuss improvements in our manufacturing and identification processes that will lead to both larger numbers of striping patterns and improved identification accuracy.
AbstractList In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished in an optical microscope. Accurate particle identification is discussed relative to synthesis reproducibility and the limitations of optical microscopes. Results from a library of these particles, of which over 100 different striping patterns have been produced, are presented. For these particles, made with Au and Ag stripes, more than 70 patterns may be identified with greater than 90% accuracy. The ability to chemically modify the surface of these particles, making them useful for bioanalytical measurements, is also demonstrated. Finally, we discuss improvements in our manufacturing and identification processes that will lead to both larger numbers of striping patterns and improved identification accuracy.In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished in an optical microscope. Accurate particle identification is discussed relative to synthesis reproducibility and the limitations of optical microscopes. Results from a library of these particles, of which over 100 different striping patterns have been produced, are presented. For these particles, made with Au and Ag stripes, more than 70 patterns may be identified with greater than 90% accuracy. The ability to chemically modify the surface of these particles, making them useful for bioanalytical measurements, is also demonstrated. Finally, we discuss improvements in our manufacturing and identification processes that will lead to both larger numbers of striping patterns and improved identification accuracy.
In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished in an optical microscope. Accurate particle identification is discussed relative to synthesis reproducibility and the limitations of optical microscopes. Results from a library of these particles, of which over 100 different striping patterns have been produced, are presented. For these particles, made with Au and Ag stripes, more than 70 patterns may be identified with greater than 90% accuracy. The ability to chemically modify the surface of these particles, making them useful for bioanalytical measurements, is also demonstrated. Finally, we discuss improvements in our manufacturing and identification processes that will lead to both larger numbers of striping patterns and improved identification accuracy.
Author Walton, Ian D
Norton, Scott M
Gupta, Dimpy
He, Lin
Freeman, R Griffith
Balasingham, Arjuna
Natan, Michael J
Oviso, Jr, Dominador F
Raju, Paul A
Author_xml – sequence: 1
  givenname: Ian D
  surname: Walton
  fullname: Walton, Ian D
  organization: SurroMed, Inc., Mountain View, California 94043, USA
– sequence: 2
  givenname: Scott M
  surname: Norton
  fullname: Norton, Scott M
– sequence: 3
  givenname: Arjuna
  surname: Balasingham
  fullname: Balasingham, Arjuna
– sequence: 4
  givenname: Lin
  surname: He
  fullname: He, Lin
– sequence: 5
  givenname: Dominador F
  surname: Oviso, Jr
  fullname: Oviso, Jr, Dominador F
– sequence: 6
  givenname: Dimpy
  surname: Gupta
  fullname: Gupta, Dimpy
– sequence: 7
  givenname: Paul A
  surname: Raju
  fullname: Raju, Paul A
– sequence: 8
  givenname: Michael J
  surname: Natan
  fullname: Natan, Michael J
– sequence: 9
  givenname: R Griffith
  surname: Freeman
  fullname: Freeman, R Griffith
BackLink https://www.ncbi.nlm.nih.gov/pubmed/12038747$$D View this record in MEDLINE/PubMed
BookMark eNo9ULtOxDAQdHGIe0DBDyBXdIG144sdOnTiJSFBAXW02A4ycuwQO4Kr-XECHDQ7-5iZlWZJZiEGS8gRg1MGnJ2hBg4gy_cZWQBAWXAJMCfLlF4BGANW7ZM541AqKeSCfD7gkJ32NtE2DrQbfXa9tx_WUAzot8kl6gJN0Y_ZxXBOjc1Wf7fT3VBnbMiudRp_VrGlKQ-un9Sdzei907T_fzAmF15o7KcRPe2cHmLSsd8ekL0WfbKHO1yRp6vLx81NcXd_fbu5uCtQSJ4LsQaNQinGajsV1BUyQFnVKEHUaBQvq1YpVdtKYWmYAVEJRCsqQKamcFbk5Ne3H-LbaFNuOpe09R6DjWNqJJOlWnM-EY93xPG5s6bpB9fhsG3-YuNfSolwsg
CitedBy_id crossref_primary_10_1039_b803807d
crossref_primary_10_1002_anie_200504025
crossref_primary_10_1016_j_bios_2010_12_010
crossref_primary_10_1016_j_cap_2012_02_030
crossref_primary_10_1016_j_bios_2003_08_014
crossref_primary_10_2217_17435889_2_5_695
crossref_primary_10_2116_analsci_30_89
crossref_primary_10_1002_ange_200601104
crossref_primary_10_3390_ma12233908
crossref_primary_10_1002_wnan_19
crossref_primary_10_1016_j_bios_2014_12_023
crossref_primary_10_1002_elps_200700448
crossref_primary_10_1002_adma_200390105
crossref_primary_10_1002_wnan_96
crossref_primary_10_1002_smll_200600727
crossref_primary_10_1002_adma_202004734
crossref_primary_10_1063_1_2745438
crossref_primary_10_1002_ange_200600288
crossref_primary_10_1007_s12030_007_0003_5
crossref_primary_10_1039_b501146a
crossref_primary_10_1109_LMAG_2016_2618781
crossref_primary_10_1385_NBT_1_4_327
crossref_primary_10_1002_anie_200600288
crossref_primary_10_1007_s00216_005_0225_0
crossref_primary_10_1016_j_cbpa_2008_08_027
crossref_primary_10_1021_cr0300789
crossref_primary_10_1007_s00216_008_2062_4
crossref_primary_10_1007_s10404_007_0240_x
crossref_primary_10_2116_analsci_30_319
crossref_primary_10_1073_pnas_0236044100
crossref_primary_10_1155_2010_203756
crossref_primary_10_1364_AO_44_006285
crossref_primary_10_2217_nnm_09_92
crossref_primary_10_1016_j_bios_2012_07_013
crossref_primary_10_1039_b610085f
crossref_primary_10_1016_j_actamat_2013_11_067
crossref_primary_10_1021_ja0658261
crossref_primary_10_1021_ja0637200
crossref_primary_10_1039_B814408G
crossref_primary_10_1002_adma_200390089
crossref_primary_10_1002_smll_200701047
crossref_primary_10_1016_j_nano_2006_11_008
crossref_primary_10_1039_b903728d
crossref_primary_10_1373_clinchem_2003_029850
crossref_primary_10_1002_adom_201400232
crossref_primary_10_1088_0957_4484_16_7_002
crossref_primary_10_1002_ange_200504025
crossref_primary_10_1002_cphc_200900377
crossref_primary_10_1021_ic0601384
crossref_primary_10_1002_anie_200601104
crossref_primary_10_1021_jp034139i
crossref_primary_10_1016_j_aca_2013_08_039
crossref_primary_10_1016_j_cccn_2005_03_014
crossref_primary_10_1039_C9QM00607A
crossref_primary_10_1016_j_jcis_2016_01_055
crossref_primary_10_1016_j_trac_2008_11_012
crossref_primary_10_1016_S0958_1669_02_00015_0
crossref_primary_10_1063_1_2162449
ContentType Journal Article
DBID CGR
CUY
CVF
ECM
EIF
NPM
7X8
DOI 10.1021/ac020073w
DatabaseName Medline
MEDLINE
MEDLINE (Ovid)
MEDLINE
MEDLINE
PubMed
MEDLINE - Academic
DatabaseTitle MEDLINE
Medline Complete
MEDLINE with Full Text
PubMed
MEDLINE (Ovid)
MEDLINE - Academic
DatabaseTitleList MEDLINE - Academic
MEDLINE
Database_xml – sequence: 1
  dbid: NPM
  name: PubMed
  url: http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed
  sourceTypes: Index Database
– sequence: 2
  dbid: 7X8
  name: MEDLINE - Academic
  url: https://search.proquest.com/medline
  sourceTypes: Aggregation Database
DeliveryMethod no_fulltext_linktorsrc
Discipline Engineering
Chemistry
ExternalDocumentID 12038747
Genre Research Support, U.S. Gov't, Non-P.H.S
Research Support, U.S. Gov't, P.H.S
Journal Article
GrantInformation_xml – fundername: NIDDK NIH HHS
  grantid: 1R43DK059077-01
GroupedDBID ---
-DZ
-~X
.DC
.GJ
.K2
186
23M
3EH
3O-
4.4
53G
55A
5GY
5RE
5VS
6J9
6TJ
7~N
85S
AABXI
AAHBH
AAUTI
ABDEX
ABHFT
ABHMW
ABJNI
ABMVS
ABOCM
ABPPZ
ABQRX
ABUCX
ACBEA
ACGFO
ACGFS
ACGOD
ACIWK
ACJ
ACKIV
ACKOT
ACNCT
ACPRK
ACPVT
ACRPL
ACS
ADHLV
ADNMO
AEESW
AENEX
AEYZD
AFEFF
AFFDN
AFFNX
AFRAH
AGXLV
AHGAQ
AIDAL
ALMA_UNASSIGNED_HOLDINGS
ANPPW
ANTXH
AQSVZ
BAANH
BKOMP
CGR
CS3
CUPRZ
CUY
CVF
D0L
EBS
ECM
ED~
EIF
EJD
F5P
GGK
GNL
IH9
IHE
JG~
KZ1
LG6
NHB
NPM
OHT
P2P
PQQKQ
ROL
RXW
TAE
TN5
UHB
UI2
UKR
VF5
VG9
VOH
VQA
VXZ
W1F
WH7
X6Y
XOL
XSW
YIN
YR5
YYP
YZZ
ZCA
ZCG
ZGI
~02
7X8
ABBLG
ABLBI
ADXHL
AETEA
AGQPQ
ID FETCH-LOGICAL-a472t-450ca488119e811ac6a10a769a7049ad8236f8889e68a3d1d0464aae460a18102
IEDL.DBID 7X8
ISICitedReferencesCount 105
ISICitedReferencesURI http://www.webofscience.com/api/gateway?GWVersion=2&SrcApp=Summon&SrcAuth=ProQuest&DestLinkType=CitingArticles&DestApp=WOS_CPL&KeyUT=000175662100002&url=https%3A%2F%2Fcvtisr.summon.serialssolutions.com%2F%23%21%2Fsearch%3Fho%3Df%26include.ft.matches%3Dt%26l%3Dnull%26q%3D
ISSN 0003-2700
IngestDate Fri Jul 11 07:50:09 EDT 2025
Wed Feb 19 02:36:43 EST 2025
IsPeerReviewed true
IsScholarly true
Issue 10
Language English
LinkModel DirectLink
MergedId FETCHMERGED-LOGICAL-a472t-450ca488119e811ac6a10a769a7049ad8236f8889e68a3d1d0464aae460a18102
Notes ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
PMID 12038747
PQID 71738522
PQPubID 23479
ParticipantIDs proquest_miscellaneous_71738522
pubmed_primary_12038747
PublicationCentury 2000
PublicationDate 2002-05-15
PublicationDateYYYYMMDD 2002-05-15
PublicationDate_xml – month: 05
  year: 2002
  text: 2002-05-15
  day: 15
PublicationDecade 2000
PublicationPlace United States
PublicationPlace_xml – name: United States
PublicationTitle Analytical chemistry (Washington)
PublicationTitleAlternate Anal Chem
PublicationYear 2002
SSID ssj0011016
Score 2.0551789
Snippet In this report, we present data demonstrating that cylindrical metallic particles, with various submicrometer striping patterns, may be readily distinguished...
SourceID proquest
pubmed
SourceType Aggregation Database
Index Database
StartPage 2240
SubjectTerms Diagnostic Imaging - standards
Electronic Data Processing - instrumentation
Electronic Data Processing - methods
Electronic Data Processing - standards
Metals - standards
Microscopy - methods
Nanotechnology
Particle Size
Title Particles for multiplexed analysis in solution: detection and identification of striped metallic particles using optical microscopy
URI https://www.ncbi.nlm.nih.gov/pubmed/12038747
https://www.proquest.com/docview/71738522
Volume 74
WOSCitedRecordID wos000175662100002&url=https%3A%2F%2Fcvtisr.summon.serialssolutions.com%2F%23%21%2Fsearch%3Fho%3Df%26include.ft.matches%3Dt%26l%3Dnull%26q%3D
hasFullText
inHoldings 1
isFullTextHit
isPrint
link http://cvtisr.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwpV07T8MwED4VigQMPMqrPD2wRk2cxHYQEkIVFQtVB5C6RW7soEo0CbS8Zv44PjcGFsTA4iWyEp3Pznd3n-8DOKWahUzR0BMizD2zExNPaK68SGdUqphyKn0rNsH7fTEcJoMGnLu7MEirdGeiPahVmWGOvIPVYmHAwkX16KFmFNZWawGNBWiGBsigT_Phdw0B41Knl4flVddXiAYdmfmYowtff8eV9v_SW__fl23AWo0ryeXcETahoYsWLHednFsLVn90HtyCj4FjxBGDWomjFb5pRWTdpoSMC-Ic84woPbOkrcI8V2SsapKRXVdS5gTlPyoze6INmn8YZ6T6egFS6-9JWdmsOZkgAxDvwrxvw13v6rZ77dV6DJ6MOJ15UexjD3QRBIk2g8yYDHzJWSK5iTOkQu303ETUiWZChipQWDaVUkfMlwZI-HQHFouy0HtAmIximmNreMxoxmyUm8iKjgx-0MwfibANJ87WqbETFjFkocvnaeqs3Ybd-XKl1bwtRxpQLMVHfP_PuQewYkVdsAlrfAjN3Ox0fQRL2ctsPH06tm5kxv7g5hM5VdRX
linkProvider ProQuest
openUrl ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Particles+for+multiplexed+analysis+in+solution%3A+detection+and+identification+of+striped+metallic+particles+using+optical+microscopy&rft.jtitle=Analytical+chemistry+%28Washington%29&rft.au=Walton%2C+Ian+D&rft.au=Norton%2C+Scott+M&rft.au=Balasingham%2C+Arjuna&rft.au=He%2C+Lin&rft.date=2002-05-15&rft.issn=0003-2700&rft.volume=74&rft.issue=10&rft.spage=2240&rft_id=info:doi/10.1021%2Fac020073w&rft.externalDBID=NO_FULL_TEXT
thumbnail_l http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=0003-2700&client=summon
thumbnail_m http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=0003-2700&client=summon
thumbnail_s http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=0003-2700&client=summon