Surface Modified Nanocellulose Fibers Yield Conducting Polymer-Based Flexible Supercapacitors with Enhanced Capacitances

We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full electrode-normalized gravimetric (127 F g–1) and volumetric (122 F cm–3) capacitances at high current densities (300 mA cm–2 ≈ 33 A g–1) until date...

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Published in:ACS nano Vol. 9; no. 7; pp. 7563 - 7571
Main Authors: Wang, Zhaohui, Carlsson, Daniel O, Tammela, Petter, Hua, Kai, Zhang, Peng, Nyholm, Leif, Strømme, Maria
Format: Journal Article
Language:English
Published: United States American Chemical Society 28.07.2015
Subjects:
capacitance
Conducting polymers
Density
Devices
Electrodes
energy storage devices
Engineering Science with specialization in Nanotechnology and Functional Materials
Fibers
modified nanocellulose
Nanostructure
Polymerization
porosity optimization
Surface chemistry
Teknisk fysik med inriktning mot nanoteknologi och funktionella material
porosity optimization
energy storage devices
capacitance
conducting polymers
modified nanocellulose
ISSN:1936-0851, 1936-086X, 1936-086X
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Abstract We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full electrode-normalized gravimetric (127 F g–1) and volumetric (122 F cm–3) capacitances at high current densities (300 mA cm–2 ≈ 33 A g–1) until date reported for conducting polymer-based electrodes with active mass loadings as high as 9 mg cm–2. By introducing quaternary amine groups on the surface of NCFs prior to polypyrrole (PPy) polymerization, the macropore volume of the formed PPy-NCF composites can be minimized while maintaining the volume of the micro- and mesopores at the same level as when unmodified or carboxylate groups functionalized NCFs are employed as polymerization substrates. Symmetric, aqueous electrolyte-based, devices comprising these porosity-optimized electrodes exhibit device-specific volumetric energy and power densities of 3.1 mWh cm–3 and 3 W cm–3 respectively; which are among the highest values reported for conducting polymer electrodes in aqueous electrolytes. The functionality of the devices is verified by powering a red light-emitting diode with the device in different mechanically challenging states.
AbstractList We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full electrode-normalized gravimetric (127 F g(-1)) and volumetric (122 F cm(-3)) capacitances at high current densities (300 mA cm(-2) ≈ 33 A g(-1)) until date reported for conducting polymer-based electrodes with active mass loadings as high as 9 mg cm(-2). By introducing quaternary amine groups on the surface of NCFs prior to polypyrrole (PPy) polymerization, the macropore volume of the formed PPy-NCF composites can be minimized while maintaining the volume of the micro- and mesopores at the same level as when unmodified or carboxylate groups functionalized NCFs are employed as polymerization substrates. Symmetric, aqueous electrolyte-based, devices comprising these porosity-optimized electrodes exhibit device-specific volumetric energy and power densities of 3.1 mWh cm(-3) and 3 W cm(-3) respectively; which are among the highest values reported for conducting polymer electrodes in aqueous electrolytes. The functionality of the devices is verified by powering a red light-emitting diode with the device in different mechanically challenging states.
We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full electrode-normalized gravimetric (127 F g super(-1)) and volumetric (122 F cm super(-3)) capacitances at high current densities (300 mA cm super(-2) approximately 33 A g super(-1)) until date reported for conducting polymer-based electrodes with active mass loadings as high as 9 mg cm super(-2). By introducing quaternary amine groups on the surface of NCFs prior to polypyrrole (PPy) polymerization, the macropore volume of the formed PPy-NCF composites can be minimized while maintaining the volume of the micro- and mesopores at the same level as when unmodified or carboxylate groups functionalized NCFs are employed as polymerization substrates. Symmetric, aqueous electrolyte-based, devices comprising these porosity-optimized electrodes exhibit device-specific volumetric energy and power densities of 3.1 mWh cm super(-3) and 3 W cm super(-3) respectively; which are among the highest values reported for conducting polymer electrodes in aqueous electrolytes. The functionality of the devices is verified by powering a red light-emitting diode with the device in different mechanically challenging states. Keywords: energy storage devices; conducting polymers; modified nanocellulose; porosity optimization; capacitance
We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full electrode-normalized gravimetric (127 F g(-1)) and volumetric (122 F cm(-3)) capacitances at high current densities (300 mA cm(-2) approximate to 33 A g(-1)) until date reported for conducting polymer-based electrodes with active mass loadings as high as 9 mg cm(-2). By introducing quaternary amine groups on the surface of NCFs prior to polypyrrole (PPy) polymerization, the macropore volume of the formed PPy-NCF composites can be minimized while maintaining the volume of the micro- and mesopores at the same level as when unmodified or carboxylate groups functionalized NCFs are employed as polymerization substrates. Symmetric, aqueous electrolyte-based, devices comprising these porosity-optimized electrodes exhibit device-specific volumetric energy and power densities of 3.1 mWh cm(-3) and 3 W cm(-3) respectively; which are among the highest values reported for conducting polymer electrodes in aqueous electrolytes. The functionality of the devices is verified by powering a red light-emitting diode with the device in different mechanically challenging states.
Author Nyholm, Leif
Zhang, Peng
Strømme, Maria
Hua, Kai
Carlsson, Daniel O
Wang, Zhaohui
Tammela, Petter
AuthorAffiliation Nanotechnology and Functional Materials, Department of Engineering Sciences, The Ångström Laboratory
Uppsala University
Department of Chemistry-The Ångström Laboratory
AuthorAffiliation_xml – name: Uppsala University
– name: Department of Chemistry-The Ångström Laboratory
– name: Nanotechnology and Functional Materials, Department of Engineering Sciences, The Ångström Laboratory
Author_xml – sequence: 1
  givenname: Zhaohui
  surname: Wang
  fullname: Wang, Zhaohui
  email: zhaohui.wang@kemi.uu.se, leif.nyholm@kemi.uu.se, maria.stromme@angstrom.uu.se
– sequence: 2
  givenname: Daniel O
  surname: Carlsson
  fullname: Carlsson, Daniel O
– sequence: 3
  givenname: Petter
  surname: Tammela
  fullname: Tammela, Petter
– sequence: 4
  givenname: Kai
  surname: Hua
  fullname: Hua, Kai
– sequence: 5
  givenname: Peng
  surname: Zhang
  fullname: Zhang, Peng
– sequence: 6
  givenname: Leif
  surname: Nyholm
  fullname: Nyholm, Leif
  email: zhaohui.wang@kemi.uu.se, leif.nyholm@kemi.uu.se, maria.stromme@angstrom.uu.se
– sequence: 7
  givenname: Maria
  surname: Strømme
  fullname: Strømme, Maria
  email: zhaohui.wang@kemi.uu.se, leif.nyholm@kemi.uu.se, maria.stromme@angstrom.uu.se
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https://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-261306$$DView record from Swedish Publication Index (Uppsala universitet)
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Keywords porosity optimization
energy storage devices
capacitance
conducting polymers
modified nanocellulose
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Snippet We demonstrate that surface modified nanocellulose fibers (NCFs) can be used as substrates to synthesize supercapacitor electrodes with the highest full...
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SubjectTerms capacitance
Conducting polymers
Density
Devices
Electrodes
energy storage devices
Engineering Science with specialization in Nanotechnology and Functional Materials
Fibers
modified nanocellulose
Nanostructure
Polymerization
porosity optimization
Surface chemistry
Teknisk fysik med inriktning mot nanoteknologi och funktionella material
Title Surface Modified Nanocellulose Fibers Yield Conducting Polymer-Based Flexible Supercapacitors with Enhanced Capacitances
URI http://dx.doi.org/10.1021/acsnano.5b02846
https://www.ncbi.nlm.nih.gov/pubmed/26083393
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https://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-261306
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