Thermal Analysis and Thermodynamic Properties of Solids
Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an authoritative overview of theoretical knowledge and practical applications across several fields.
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| Format: | E-Book |
| Sprache: | Englisch |
| Veröffentlicht: |
Chantilly
Elsevier
2021
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| Ausgabe: | 2 |
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| ISBN: | 0323855377, 9780323855372 |
| Online-Zugang: | Volltext |
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| Abstract | Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an authoritative overview of theoretical knowledge and practical applications across several fields. |
|---|---|
| AbstractList | Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an authoritative overview of theoretical knowledge and practical applications across several fields. |
| Author | Sestak, Jaroslav |
| Author_xml | – sequence: 1 fullname: Sestak, Jaroslav |
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| ContentType | eBook |
| DEWEY | 530.4/12 |
| DOI | 10.1016/C2020-0-02847-1 |
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| Discipline | Physics |
| EISBN | 9780323858113 0323858112 |
| Edition | 2 |
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| Snippet | Thermal Analysis and Thermodynamic Properties of Solids, Second Edition covers foundational principles and recent updates in the field, presenting an... |
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| SubjectTerms | Solids-Thermal properties |
| TableOfContents | Front cover -- Half Title -- Title -- Copyright -- Contents -- Dedication -- Acknowledgment -- About the Author -- Forward -- Introduction: Anniversary of the half century development and formation of a new field of thermal analysis -- Historical prologue -- Eastern stream of thermoanalytical progression and the foundation of Journal of Thermal Analysis -- The Western course of thermal analysis advancement and foundation of Thermochimica Acta -- Word in Conclusion -- Glossary of terms, definitions and symbols -- Chapter 1 Thermophysical examinations, experimental set-ups, sample and temperature control -- 1.1 Exploring the environment and scale dimensions -- 1.2 Thermal measurements, modes of assessment and thermal methods grouping -- 1.3 Temperature control -- 1.4 Characterisation of experimental curves -- 1.5 Comments on the thermoanalytical sample -- 1.6 Particularities of further temperature modulation -- Chapter 2 Understanding of temperature, heat, gradients and related thermodynamics -- 2.1 A historical look at the development of the temperature concept -- 2.2 What is temperature, its scope and how to specify its thermodynamic description: concept of tempericity -- 2.3 Varying temperature depending on the measurement procedure used and the related new view of the phase diagram kinetics -- 2.4 Heat transfer, Newton cooling law and sample heat inertia -- 2.5 Thermal inertia values calculated for temperature measurement -- 2.6 Illustrative approach to temperature fields developed inside an inert infinite cylinder -- 2.7 Response differential curves for temperature sensor location in temperature gradients -- 2.8 Discussion on temperature and its physical and operational use -- 2.9Appendix: A generalised view on temperature from the cosmic macro-dimension to the quantum micro-world 9.4 Fundamental aspects of kinetic evaluations under non-isothermal conditions -- 9.5 Integral and differential methods of kinetic data evaluation -- 9.6 Non-integral power exponents, formal kinetic models and the role of an accommodation function -- 9.7 Practicality and peculiarity of non-isothermal approach -- 9.7.1 Apparent values of activation energies -- 9.7.2 An alternative view on the kinetics: non-parametric approach -- 9.7.3 Non-isothermal studies performed close to equilibrium -- 9.8 Optimal kinetic evaluation procedures of experimental data -- 9.8.1 Málek's master plot -- 9.8.2 Koga's approach to overlapping reactions -- 9.8.3 Evaluation based on polynomial regression: Netzsch software by Moukina -- 9.8.4 Overlapping models, including uncertainty and distort activation energy -- 9.8.5 Special cases of CRTA and temperature oscillation modes -- 9.9 Kinetic compensation effect -- Chapter 10 Thermokinetics in DTA experiments -- 10.1 On the historical outline of differential methods -- 10.2 DTA equation and its testing by rectangular heat pulse -- 10.3 What exactly is the DTA curve and what is its scope and responsibility? -- 10.4 A continuous model of phase transition and temperature profiles within a simple case of cylinder -- 10.5 Temperature profile, temperature modulation and revised DTA equation -- Chapter 11 Physical thermokinetics of reversible thermal decomposition by thermogravimetry -- 11.1 Some notes on the historical thermogravimetry -- 11.2 Specific case of TG study of calcium carbonate decomposition -- 11.3 How are thermo-gravimetric results usable in practice? -- 11.3.1 Micro-kinetics -- 11.3.2 Macro-kinetics -- 11.4 How is the thermodynamic-equilibrium temperature represented in TG curves? -- 11.5 Practical consequences -- 11.6 Yet further accompaniments Chapter 12 Exploiting fractals, tackle thermal processes and truer non-isothermal kinetics -- 12.1 Introduction to fractal analysis -- 12.2 Heat capacity by means of fractal structures -- 12.3 Nucleation-induced crystallisation within fractal scrutiny -- 12.4 Heterogeneity, fractals and solid-state reaction kinetics -- 12.5 All-purpose use of yet atypical fractal geometry -- 12.6 Mathematical instigation and impact of logistic models -- 12.7 Origin of the Šesták-Berggren (SB) equation and the impact of logistic tactic -- 12.8 How we are doing and our other prospects and effects -- Chapter 13 Constrained states of glasses, exploitation of transition temperatures, glass-forming coefficients and concepts of fragility -- 13.1 Introduction-a brief look at the glass history -- 13.2 Enthalpy temperature dependence diagrams for a better understanding of the processes taking place in the glasses -- 13.3 GFA and GS -- 13.4 Expressing the Hrubý parameter using temperature relations: r = Tc/Tg and m = Tm/Tg -- 13.5 Relative changes of GS parameters -- 13.6 Modified Angell plot of viscous flow and fragility concept -- 13.7 Reduced glass transition temperature and fragility as parameters for estimating GFA -- 13.8 Stretching exponent against configurational entropy: which factor has greater contribution to kinetic liquid fragility? -- 13.9 The function of temperature dependence of configurational entropy -- Chapter 14 Explanation of crystallisation kinetics both during glass heating and melt cooling, while the incorrectness of the Kissinger method is indicated -- 14.1 Introduction: glass crystallisation and use of DTA -- 14.2 Reminding simple kinetic method proposed by Kissinger -- 14.3 Choice of reaction mechanism, iso-thermal and non-iso-thermal degree of conversion and equilibrium background Chapter 3 Phenomenological approach to the caloric theory of heat: An alternative thermodynamics -- 3.1 Fire as a manufacturing tool and its non-matter disposition as caloric -- 3.2 Classical thermodynamics subsist in a phenomenological theory -- 3.3 Heat alike entropy: introduction of caloric theory -- 3.4 Constitutive relations and fundamental laws of thermodynamics within caloric theory -- 3.5 Resolution and determination of caloric -- 3.6 Efficiency of heat engines, dynamic and caloric theory -- Chapter 4 Textbook thermodynamics as thermostatics -- 4.1 Introduction to basic logic of textbook thermodynamics -- 4.2 Force field and measurable deformations -- 4.3 Principles of thermodynamic alternation reaching measurable quantities -- 4.4 Chemical reactions -- 4.5 Heterogeneous systems and the effect of surface energy -- 4.6 Equilibria and impact of Clapeyron equations -- 4.7 Ideal and real solid solutions, phase diagrams -- Chapter 5 Equilibrium background and its importance for temperature and particle size -- 5.1 Some historical facts about the theory of phase transformations -- 5.2 Equilibrium background as a basis for thermal analysis, type of processes and impact of heating -- 5.3 Ehrenfest equations derived for gradual transitions in binary systems -- 5.4 Equilibrium background due to the change in particle curvature -- 5.5 Appendix: A bottom-up inverse approach illustrated by the construction on the atomic level using assembled spheres in a cubic structure -- Chapter 6 Thermodynamics: processes dynamics under constant heating -- 6.1 The validity of thermodynamic laws when ensuring the effect of constant temperature changes -- 6.2 Fourier's heat transfer and the Laws of Fick and Ohm in a historical overview -- 6.3 Phase transitions, their order and concept of broadened transformations 6.4 Kinetic degree of transformation and the Holba-Sestak equation -- 6.5 Interpretation of phase diagrams using the new kinetic approach -- 6.6 T-T-T and C-T diagrams -- 6.7 Thermodynamics applied to non-equilibrium glass transition -- 6.8 Influence of fluctuations and some features of rational approach -- Chapter 7 Thermotics-theoretical thermal analysis, thermometry and calorimetry -- 7.1 Heat determination by thermometry and calorimetry -- 7.2 Some remarks on the origins of modern thermal analysis -- 7.3 Measurements of thermal diffusivity -- 7.4 Classification of thermoanalytical methods-heat balance -- 7.5 DSC and DTA as quantitative instruments -- 7.6 DTA calibration and the use of defined electrical pulses -- 7.7 Practical cases of applications -- 7.7.1 Phase diagrams -- 7.7.2 Heat capacity -- 7.7.3 Impurity measurements -- 7.8 Temperature-modulated mode -- 7.9 Fast scanning calorimetry -- Chapter 8 Rationality of creating kinetic models: How to mold a reaction path in solid-state -- 8.1 Some philosophical thoughts on a general exercise towards mathematical models -- 8.2 Portrayal roots applied in modelling solid-state reaction pathway -- 8.3 Rate constant function-Arrhenius and non-Arrhenius expressions -- 8.4 Rate constant functions two: reaction models f(α) based on simple geometrical bodies -- 8.5 Idealised models contrary to the real process mechanisms and morphologies -- Chapter 9 Facilitated reaction kinetics by thermal analysis -- 9.1 Inserted retrospective historical view of early non-isothermal kinetics from the point of view of own experience -- 9.1.1 Supplementary references valid only for the above historical section -- 9.2 Constitutive equations applied in non-isothermal chemical kinetics -- 9.3 Once discussed ill-defined kinetic concept of derivates misuse 14.4 The point of maximum temperature deviation at DTA peak is not the point of maximum reaction rate |
| Title | Thermal Analysis and Thermodynamic Properties of Solids |
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