Investigation of the effect of titanium and zirconium oxides on the strength characteristics of nanoscale hydroxyapatite
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| Názov: | Investigation of the effect of titanium and zirconium oxides on the strength characteristics of nanoscale hydroxyapatite |
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| Autori: | K.I. Sabanin, V.M. Skachkov, I.S. Medyankina, E.A. Bogdanova, N.A. Sabirzyanov |
| Zdroj: | Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов, Vol 16, Pp 981-1003 (2024) |
| Informácie o vydavateľovi: | Tver State University, 2024. |
| Rok vydania: | 2024 |
| Zbierka: | LCC:Physical and theoretical chemistry |
| Predmety: | hydroxyapatite, titanium oxide, zirconium oxide, sintering, composite biomaterials, microhardness, Physical and theoretical chemistry, QD450-801 |
| Popis: | The article discusses the possibility of dispersion strengthening of nanostructured hydroxyapatite synthesized by precipitation from solution introducing reinforcing additives of non-stoichiometric titanium oxide and zirconium dioxide. The reinforced composite material: hydroxyapatite – non-stoichiometric titanium oxide – zirconium dioxide was obtained by mechanochemical synthesis of hydroxyapatite with doping components followed by annealing at 1000°C. The initial components and synthesized samples were certified using modern physicochemical methods of analysis: X-ray phase analysis, differential thermal analysis, scanning electron microscopy, surface area and porosity analysis, dispersion analysis. The influence of the qualitative and quantitative composition of the composite on the sintering processes and strength characteristics of the studied samples in a wide temperature range of 25-1200°C is shown. It has been experimentally established that the most promising system for developing biocomposites based on it ishydroxyapatite – 15% non-stoichiometric titanium oxide – 5% zirconium dioxide. Composite materials of this composition have a dense, uniform, strong structure with a high degree of crystallinity and a developed surface. They seem to be promising materials for further research with the aim of introducing it into medical practice. |
| Druh dokumentu: | article |
| Popis súboru: | electronic resource |
| Jazyk: | Russian |
| ISSN: | 2226-4442 2658-4360 |
| Relation: | https://physchemaspects.ru/2024/doi-10-26456-pcascnn-2024-16-981/?lang=en; https://doaj.org/toc/2226-4442; https://doaj.org/toc/2658-4360 |
| DOI: | 10.26456/pcascnn/2024.16.981 |
| Prístupová URL adresa: | https://doaj.org/article/547b1b4b3c9d4fdcb1a40d519f64935e |
| Prístupové číslo: | edsdoj.547b1b4b3c9d4fdcb1a40d519f64935e |
| Databáza: | Directory of Open Access Journals |
Nájsť tento článok vo Web of Science | Abstrakt: | The article discusses the possibility of dispersion strengthening of nanostructured hydroxyapatite synthesized by precipitation from solution introducing reinforcing additives of non-stoichiometric titanium oxide and zirconium dioxide. The reinforced composite material: hydroxyapatite – non-stoichiometric titanium oxide – zirconium dioxide was obtained by mechanochemical synthesis of hydroxyapatite with doping components followed by annealing at 1000°C. The initial components and synthesized samples were certified using modern physicochemical methods of analysis: X-ray phase analysis, differential thermal analysis, scanning electron microscopy, surface area and porosity analysis, dispersion analysis. The influence of the qualitative and quantitative composition of the composite on the sintering processes and strength characteristics of the studied samples in a wide temperature range of 25-1200°C is shown. It has been experimentally established that the most promising system for developing biocomposites based on it ishydroxyapatite – 15% non-stoichiometric titanium oxide – 5% zirconium dioxide. Composite materials of this composition have a dense, uniform, strong structure with a high degree of crystallinity and a developed surface. They seem to be promising materials for further research with the aim of introducing it into medical practice. |
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| ISSN: | 22264442 26584360 |
| DOI: | 10.26456/pcascnn/2024.16.981 |