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Establishing operando diffraction capability through the study of Li-ion (de) intercalation in LiFePO4

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Název:	Establishing operando diffraction capability through the study of Li-ion (de) intercalation in LiFePO4
Autoři:	Wilson, G., Zilinskaite, S., Unka, S., Boston, R., Reeves-McLaren, N.
Přispěvatelé:	Cruden, A.
Informace o vydavateli:	Elsevier
Rok vydání:	2020
Sbírka:	White Rose Research Online (Universities of Leeds, Sheffield & York)
Popis:	We have used a laboratory diffractometer to perform operando X-ray diffraction on LiFePO4 during electrochemical cycling in a coin cell fitted with a Kapton window. The results obtained are in good agreement with previous studies, verifying that extraction of Li from LiFePO4 follows dual-phase solid solution behaviour, with neither LiFePO4 nor FePO4 maintaining a static composition during deintercalation.
Druh dokumentu:	report
Popis souboru:	text
Jazyk:	English
Relation:	https://eprints.whiterose.ac.uk/161516/1/1-s2.0-S2352484720302316-main.pdf; Wilson, G., Zilinskaite, S., Unka, S. et al. (2 more authors) (2020) Establishing operando diffraction capability through the study of Li-ion (de) intercalation in LiFePO4. In: Cruden, A., (ed.) Energy Reports. 4th Annual CDT Conference in Energy Storage & Its Applications, 09-10 Jul 2019, Southampton, UK. Elsevier , pp. 174-179.
Dostupnost:	https://eprints.whiterose.ac.uk/161516/
Rights:	cc_by_nc_nd_4
Přístupové číslo:	edsbas.E52D56B6
Databáze:	BASE

Popis
Abstrakt:	We have used a laboratory diffractometer to perform operando X-ray diffraction on LiFePO4 during electrochemical cycling in a coin cell fitted with a Kapton window. The results obtained are in good agreement with previous studies, verifying that extraction of Li from LiFePO4 follows dual-phase solid solution behaviour, with neither LiFePO4 nor FePO4 maintaining a static composition during deintercalation.