An electrochemical sensing platform based on ZnO nanostructure modified glassy carbon electrode for sensitive hydroxylamine detection

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Název: An electrochemical sensing platform based on ZnO nanostructure modified glassy carbon electrode for sensitive hydroxylamine detection
Autoři: Shallal, Muhammad Abdel Hasan, Mubarak, Hayfaa A.
Zdroj: Journal of Electrochemical Science and Engineering (2025)
Informace o vydavateli: International Association of Physical Chemists (IAPC), 2025.
Rok vydání: 2025
Témata: Chemistry, Electrochemical sensor, water sample, environmental pollutants, QD1-999, differential pulse voltammetry
Popis: Background and purpose: Hydroxylamine is a reducing agent widely used in pharmacology and industry. The respiratory system, skin, eyes, and other mucous membranes are all irritated. Therefore, while researching biological industrial processes, quantitative HXA detection is crucial. Experimental approach: This study uses ZnO nanostructures on the glassy carbon electrode (GCE) surface to develop a sensitive electrochemical sensor for hydroxyl­amine (HXA). The drop-casting method was used to modify the sensor. Key results: The manufactured ZnO/GCE sensor showed outstanding catalytic performance for the electro­oxidation of HXA. Using differential pulse voltammetry with a low limit of detection of 0.3 μM in the range of 0.5 to 470.0 μM, the ZnO/GCE demonstrated strong electrocatalytic perfor­mances toward HXA. Furthermore, in the detection of HXA, the ZnO/GCE demonstrated satisfactory repeatability and stability.
Druh dokumentu: Article
Popis souboru: application/pdf
Jazyk: English
ISSN: 1847-9286
DOI: 10.5599/jese.2789
Přístupová URL adresa: https://doaj.org/article/6c876197fe5941baa5084ea01cff8bc6
https://hrcak.srce.hr/335040
https://doi.org/10.5599/jese.2789
Přístupové číslo: edsair.dedup.wf.002..a1be2b0ce6feb0f61a381586daef0341
Databáze: OpenAIRE
Popis
Abstrakt:Background and purpose: Hydroxylamine is a reducing agent widely used in pharmacology and industry. The respiratory system, skin, eyes, and other mucous membranes are all irritated. Therefore, while researching biological industrial processes, quantitative HXA detection is crucial. Experimental approach: This study uses ZnO nanostructures on the glassy carbon electrode (GCE) surface to develop a sensitive electrochemical sensor for hydroxyl­amine (HXA). The drop-casting method was used to modify the sensor. Key results: The manufactured ZnO/GCE sensor showed outstanding catalytic performance for the electro­oxidation of HXA. Using differential pulse voltammetry with a low limit of detection of 0.3 μM in the range of 0.5 to 470.0 μM, the ZnO/GCE demonstrated strong electrocatalytic perfor­mances toward HXA. Furthermore, in the detection of HXA, the ZnO/GCE demonstrated satisfactory repeatability and stability.
ISSN:18479286
DOI:10.5599/jese.2789