M2(H2O)[μ10-C6H2(COO)4] (M = Ba2+, Pb2+) - Two Isotypic Three-Dimensional Coordination Polymers with a Layer-like Separation between Anions and Cations
Monoclinic single crystals of Ba2(H2O)[μ10‐C6H2(COO)4] (1) and Pb2(H2O)[μ10‐C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no. 15), Z = 4; 1: a = 780.89(4), b = 1756.19(8), c = 914.80(5) pm, β = 114.512(5)°; 2: a = 756.70(10), b = 1772.8(2), c = 890.2(2) pm, β = 113.590...
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| Veröffentlicht in: | Zeitschrift für anorganische und allgemeine Chemie (1950) Jg. 641; H. 6; S. 1150 - 1155 |
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Weinheim
WILEY-VCH Verlag
01.05.2015
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| Abstract | Monoclinic single crystals of Ba2(H2O)[μ10‐C6H2(COO)4] (1) and Pb2(H2O)[μ10‐C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no. 15), Z = 4; 1: a = 780.89(4), b = 1756.19(8), c = 914.80(5) pm, β = 114.512(5)°; 2: a = 756.70(10), b = 1772.8(2), c = 890.2(2) pm, β = 113.590(10)°]. There are two crystallographically independent M2+ ions (M = Ba, Pb). M(1) is surrounded by eight carboxylate oxygen atoms and one water molecule forming a tricapped trigonal prism. M(2) is coordinated by ten carboxylate oxygen atoms in the shape of a tetracapped octahedron. The connection between the M(1) and M(2) polyhedra leads to infinite layers parallel to (010), which are linked by [C6H2(COO)4]4– anions to form a three‐dimensional framework. The [C6H2(COO)4]4– anion adopts a μ10 coordination mode. Compound 1 reveals short Ba–Ba contacts of 426.46(2) pm, whereas the Pb–Pb distance of 411.01(6) pm in 2 is larger than twice the van der Waals radius. |
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| AbstractList | Monoclinic single crystals of Ba2(H2O)[μ10‐C6H2(COO)4] (1) and Pb2(H2O)[μ10‐C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no. 15), Z = 4; 1: a = 780.89(4), b = 1756.19(8), c = 914.80(5) pm, β = 114.512(5)°; 2: a = 756.70(10), b = 1772.8(2), c = 890.2(2) pm, β = 113.590(10)°]. There are two crystallographically independent M2+ ions (M = Ba, Pb). M(1) is surrounded by eight carboxylate oxygen atoms and one water molecule forming a tricapped trigonal prism. M(2) is coordinated by ten carboxylate oxygen atoms in the shape of a tetracapped octahedron. The connection between the M(1) and M(2) polyhedra leads to infinite layers parallel to (010), which are linked by [C6H2(COO)4]4– anions to form a three‐dimensional framework. The [C6H2(COO)4]4– anion adopts a μ10 coordination mode. Compound 1 reveals short Ba–Ba contacts of 426.46(2) pm, whereas the Pb–Pb distance of 411.01(6) pm in 2 is larger than twice the van der Waals radius. Monoclinic single crystals of Ba2(H2O)[μ10-C6H2(COO)4] (1) and Pb2(H2O)[μ10-C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no. 15), Z = 4; 1: a = 780.89(4), b = 1756.19(8), c = 914.80(5) pm, β = 114.512(5)°; 2: a = 756.70(10), b = 1772.8(2), c = 890.2(2) pm, β = 113.590(10)°]. There are two crystallographically independent M 2+ ions (M = Ba, Pb). M(1) is surrounded by eight carboxylate oxygen atoms and one water molecule forming a tricapped trigonal prism. M(2) is coordinated by ten carboxylate oxygen atoms in the shape of a tetracapped octahedron. The connection between the M(1) and M(2) polyhedra leads to infinite layers parallel to (010), which are linked by [C6H2(COO)4] 4-anions to form a three-dimensional framework. The [C6H2(COO)4] 4-anion adopts a μ 10 coordination mode. Compound 1 reveals short Ba-Ba contacts of 426.46(2) pm, whereas the Pb-Pb distance of 411.01(6) pm in 2 is larger than twice the van der Waals radius. Monoclinic single crystals of Ba2(H2O)[µ10-C6H2(COO)4] (1) and Pb2(H2O)[µ10-C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no. 15), Z = 4; 1: a = 780.89(4), b = 1756.19(8), c = 914.80(5) pm, [beta] = 114.512(5)°; 2: a = 756.70(10), b = 1772.8(2), c = 890.2(2) pm, [beta] = 113.590(10)°]. There are two crystallographically independent M2+ ions (M = Ba, Pb). M(1) is surrounded by eight carboxylate oxygen atoms and one water molecule forming a tricapped trigonal prism. M(2) is coordinated by ten carboxylate oxygen atoms in the shape of a tetracapped octahedron. The connection between the M(1) and M(2) polyhedra leads to infinite layers parallel to (010), which are linked by [C6H2(COO)4]4- anions to form a three-dimensional framework. The [C6H2(COO)4]4- anion adopts a µ10 coordination mode. Compound 1 reveals short Ba-Ba contacts of 426.46(2) pm, whereas the Pb-Pb distance of 411.01(6) pm in 2 is larger than twice the van der Waals radius. |
| Author | Robl, Christian Köferstein, Roberto |
| Author_xml | – sequence: 1 givenname: Roberto surname: Köferstein fullname: Köferstein, Roberto organization: Institute of Inorganic and Analytical Chemistry, Friedrich-Schiller-University Jena, Humboldtstrasse 8, 07743 Jena, Germany – sequence: 2 givenname: Christian surname: Robl fullname: Robl, Christian email: crr@uni-jena.de organization: Institute of Inorganic and Analytical Chemistry, Friedrich-Schiller-University Jena, Humboldtstrasse 8, 07743 Jena, Germany |
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| Keywords | Coordination polymers Metal-organic frameworks IR Spectroscopy infrared sprectroscopy benzene carboxylate complexes |
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| Snippet | Monoclinic single crystals of Ba2(H2O)[μ10‐C6H2(COO)4] (1) and Pb2(H2O)[μ10‐C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no.... Monoclinic single crystals of Ba2(H2O)[µ10-C6H2(COO)4] (1) and Pb2(H2O)[µ10-C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no.... Monoclinic single crystals of Ba2(H2O)[μ10-C6H2(COO)4] (1) and Pb2(H2O)[μ10-C6H2(COO)4] (2) were obtained using the silica gel method [space group C2/c (no.... |
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| SubjectTerms | 5-tetracarboxylate Barium Benzene-1 Benzene‐1, 2, 4, 5‐tetracarboxylate Chemical Sciences Coordination chemistry Cristallography Crystal structure Lead Metal-organic-frameworks Polymers Pyromellitate |
| Title | M2(H2O)[μ10-C6H2(COO)4] (M = Ba2+, Pb2+) - Two Isotypic Three-Dimensional Coordination Polymers with a Layer-like Separation between Anions and Cations |
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