A Novel One-Dimensional Copper Mellitate Complex Featured by {Cu(H2O)2(urea)[C6(COO)4(COOH)2]}n2n- Polyanions
Blue monoclinic single crystals of the novel one‐dimensional [H3N‐(CH2)6‐NH3][Cu(H2O)2(urea)(μ2‐C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in aqueous solution at room temperature in the presence of 1,6‐diaminohexane and urea [space group P21/n (no. 14) with a = 958.48(9), b = 1465.74(1...
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| Vydané v: | Zeitschrift für anorganische und allgemeine Chemie (1950) Ročník 641; číslo 11; s. 1886 - 1891 |
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| Hlavní autori: | , |
| Médium: | Journal Article |
| Jazyk: | English |
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Weinheim
WILEY-VCH Verlag
01.09.2015
WILEY‐VCH Verlag Wiley Subscription Services, Inc Wiley-VCH Verlag |
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| ISSN: | 0044-2313, 1521-3749 |
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| Abstract | Blue monoclinic single crystals of the novel one‐dimensional [H3N‐(CH2)6‐NH3][Cu(H2O)2(urea)(μ2‐C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in aqueous solution at room temperature in the presence of 1,6‐diaminohexane and urea [space group P21/n (no. 14) with a = 958.48(9), b = 1465.74(11), c = 1821.14(12) pm, β = 97.655(8)°]. The Cu2+ cation is coordinated in a square pyramidal manner by two oxygen atoms stemming from the dihydrogen mellitate tetraanion, one oxygen atom from the urea molecule, and two water molecules. The Cu–O distances are in the range of 193.3(2) and 229.4(2) pm. The connection between Cu2+ and [C6(COO)4(COOH)2]4– yields infinite chain‐like polyanions parallel to [1$\bar{}$01] with a composition of {Cu(H2O)2(urea)[C6(COO)4(COOH)2]}n2n–. The dihydrogen mellitate tetraanion adopts a μ2 coordination mode. The [(H3N–(CH2)6–NH3)]2+ cations are accommodated between the chains as counter cations. The hexane‐1,6‐diammonium cations adopt a partial synclinal conformation. The chains are connected by strong and weak hydrogen bonds. Magnetic measurements reveal a paramagnetic Curie‐Weiss behavior and a magnetic moment of 1.93 μB per Cu2+. Thermoanalytical investigations in air show that the complex is stable up to 135 °C, and the following decomposition processes yield CuO. |
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| AbstractList | Blue monoclinic single crystals of the novel one-dimensional [H 3 N-(CH 2) 6-NH 3 ][Cu(H 2 O) 2 (urea)(µ 2-C 6 (COO) 4 (COOH) 2)]*H 2 O coordination polymer have been prepared in aqueous solution at room temperature in the presence of 1,6-diaminohexane and urea. Space group P2 1 /n (no. 14) with a = 958.48(9), b = 1465.74(11), c = 1821.14(12) pm, beta = 97.655(8)°. The Cu 2+ cation is coordinated in a square pyramidal manner by two oxygen atoms stemming from the dihydrogen mellitate tetraanion, one oxygen atom from the urea molecule, and two water molecules. The Cu−O distances are between 193.3(2) and 229.4(2) pm. The connection between Cu 2+ and [C 6 (COO) 4 (COOH) 2 ] 4- yields infinite chain-like polyanions parallel to [-1 ̅01] with a composition of {Cu(H 2 O) 2 (urea)[C 6 (COO) 4 (COOH) 2 ]} n 2n-. The dihydrogen mellitate tetraanion adopts a µ 2 coordination mode. The [(H 3 N-(CH 2) 6-NH 3)] 2+ cations are accommodated between the chains as counter cations. The hexane-1,6-diammonium cations adopt a partial synclinal conformation. The chains are connected by strong and weak hydrogen bonds. Magnetic measurements reveal a paramagnetic Curie-Weiss behaviour and a magnetic moment of 1.93 µ B per Cu 2+. Thermoanalytical investigations in air show that the complex is stable up to 135 °C. Following decomposition processes yielding CuO. Blue monoclinic single crystals of the novel one‐dimensional [H3N‐(CH2)6‐NH3][Cu(H2O)2(urea)(μ2‐C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in aqueous solution at room temperature in the presence of 1,6‐diaminohexane and urea [space group P21/n (no. 14) with a = 958.48(9), b = 1465.74(11), c = 1821.14(12) pm, β = 97.655(8)°]. The Cu2+ cation is coordinated in a square pyramidal manner by two oxygen atoms stemming from the dihydrogen mellitate tetraanion, one oxygen atom from the urea molecule, and two water molecules. The Cu–O distances are in the range of 193.3(2) and 229.4(2) pm. The connection between Cu2+ and [C6(COO)4(COOH)2]4– yields infinite chain‐like polyanions parallel to [1$\bar{}$01] with a composition of {Cu(H2O)2(urea)[C6(COO)4(COOH)2]}n2n–. The dihydrogen mellitate tetraanion adopts a μ2 coordination mode. The [(H3N–(CH2)6–NH3)]2+ cations are accommodated between the chains as counter cations. The hexane‐1,6‐diammonium cations adopt a partial synclinal conformation. The chains are connected by strong and weak hydrogen bonds. Magnetic measurements reveal a paramagnetic Curie‐Weiss behavior and a magnetic moment of 1.93 μB per Cu2+. Thermoanalytical investigations in air show that the complex is stable up to 135 °C, and the following decomposition processes yield CuO. Blue monoclinic single crystals of the novel one-dimensional [H3N-(CH2)6-NH3][Cu(H2O)2(urea)(µ2-C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in aqueous solution at room temperature in the presence of 1,6-diaminohexane and urea [space group P21/n (no. 14) with a = 958.48(9), b = 1465.74(11), c = 1821.14(12) pm, [beta] = 97.655(8)°]. The Cu2+ cation is coordinated in a square pyramidal manner by two oxygen atoms stemming from the dihydrogen mellitate tetraanion, one oxygen atom from the urea molecule, and two water molecules. The Cu-O distances are in the range of 193.3(2) and 229.4(2) pm. The connection between Cu2+ and [C6(COO)4(COOH)2]4- yields infinite chain-like polyanions parallel to [1$\bar{}$01] with a composition of {Cu(H2O)2(urea)[C6(COO)4(COOH)2]}n2n-. The dihydrogen mellitate tetraanion adopts a µ2 coordination mode. The [(H3N-(CH2)6-NH3)]2+ cations are accommodated between the chains as counter cations. The hexane-1,6-diammonium cations adopt a partial synclinal conformation. The chains are connected by strong and weak hydrogen bonds. Magnetic measurements reveal a paramagnetic Curie-Weiss behavior and a magnetic moment of 1.93 µB per Cu2+. Thermoanalytical investigations in air show that the complex is stable up to 135 °C, and the following decomposition processes yield CuO. |
| Author | Robl, Christian Köferstein, Roberto |
| Author_xml | – sequence: 1 givenname: Roberto surname: Köferstein fullname: Köferstein, Roberto organization: Institute of Inorganic and Analytical Chemistry, Friedrich-Schiller-University Jena, Humboldtstrasse 8, 07743 Jena, Germany – sequence: 2 givenname: Christian surname: Robl fullname: Robl, Christian email: crr@uni-jena.de organization: Institute of Inorganic and Analytical Chemistry, Friedrich-Schiller-University Jena, Humboldtstrasse 8, 07743 Jena, Germany |
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| Copyright | Copyright © 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim Distributed under a Creative Commons Attribution 4.0 International License |
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| Issue | 11 |
| Keywords | Urea Infrared spectroscopy Benzene carboxylate Coordination polymer Magnetism Diaminohexane curie-weiss law mellitate Copper complexes |
| Language | English |
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| Snippet | Blue monoclinic single crystals of the novel one‐dimensional [H3N‐(CH2)6‐NH3][Cu(H2O)2(urea)(μ2‐C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in... Blue monoclinic single crystals of the novel one-dimensional [H3N-(CH2)6-NH3][Cu(H2O)2(urea)(µ2-C6(COO)4(COOH)2)]·H2O coordination polymer were prepared in... Blue monoclinic single crystals of the novel one-dimensional [H 3 N-(CH 2) 6-NH 3 ][Cu(H 2 O) 2 (urea)(µ 2-C 6 (COO) 4 (COOH) 2)]*H 2 O coordination polymer... |
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| SubjectTerms | Benzenehexacarboxylic acid Chemical Sciences Coordination chemistry Copper Diaminohexane Inorganic chemistry Polyanions Urea |
| Title | A Novel One-Dimensional Copper Mellitate Complex Featured by {Cu(H2O)2(urea)[C6(COO)4(COOH)2]}n2n- Polyanions |
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