Countercurrent gas-solid trickle flow reactor with structured packing: Hydrodynamics and CaO-CO2 reaction

The sorption reaction CaO–CO2 was examined in a countercurrent gas–solid trickle flow reactor with regularly stacked packing at T = 500–600°C, pCO2 = 40–50 kPa, solid‐phase fluxes S = 0.3–0.5 kg m−2 s−1, and CaO particles of 500–710 μm in size. Sorption kinetics was evaluated by thermogravimetric (T...

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Published in:	AIChE journal Vol. 61; no. 5; pp. 1601 - 1612
Main Authors:	Obradović, Ana, Levec, Janez
Format:	Journal Article
Language:	English
Published:	New York Blackwell Publishing Ltd 01.05.2015 American Institute of Chemical Engineers
Subjects:	CaO-CO2 reaction Carbon dioxide countercurrent gas-solid trickle flow Hydrodynamics Plug flow plug flow model Reactors Sorption structured packing
ISSN:	0001-1541, 1547-5905
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Abstract	The sorption reaction CaO–CO2 was examined in a countercurrent gas–solid trickle flow reactor with regularly stacked packing at T = 500–600°C, pCO2 = 40–50 kPa, solid‐phase fluxes S = 0.3–0.5 kg m−2 s−1, and CaO particles of 500–710 μm in size. Sorption kinetics was evaluated by thermogravimetric (TG) technique. The random pore model was used for the description of the carbonization reaction. Hydrodynamic characteristics of gas–solid trickle flow were estimated at room temperature and ambient pressure. Plug flow model of both gas and solid‐phase, with the parameters obtained from TG and hydrodynamics experiments, satisfactorily described the sorption process in countercurrent gas–solid trickle flow reactor. © 2015 American Institute of Chemical Engineers AIChE J, 61: 1601–1612, 2015
AbstractList	The sorption reaction CaO–CO2 was examined in a countercurrent gas–solid trickle flow reactor with regularly stacked packing at T = 500–600°C, pCO2 = 40–50 kPa, solid‐phase fluxes S = 0.3–0.5 kg m−2 s−1, and CaO particles of 500–710 μm in size. Sorption kinetics was evaluated by thermogravimetric (TG) technique. The random pore model was used for the description of the carbonization reaction. Hydrodynamic characteristics of gas–solid trickle flow were estimated at room temperature and ambient pressure. Plug flow model of both gas and solid‐phase, with the parameters obtained from TG and hydrodynamics experiments, satisfactorily described the sorption process in countercurrent gas–solid trickle flow reactor. © 2015 American Institute of Chemical Engineers AIChE J, 61: 1601–1612, 2015 The sorption reaction CaO-CO2 was examined in a countercurrent gas-solid trickle flow reactor with regularly stacked packing at T=500-600°C, pCO2=40-50 kPa, solid-phase fluxes S=0.3-0.5 kg m-2 s-1, and CaO particles of 500-710 µm in size. Sorption kinetics was evaluated by thermogravimetric (TG) technique. The random pore model was used for the description of the carbonization reaction. Hydrodynamic characteristics of gas-solid trickle flow were estimated at room temperature and ambient pressure. Plug flow model of both gas and solid-phase, with the parameters obtained from TG and hydrodynamics experiments, satisfactorily described the sorption process in countercurrent gas-solid trickle flow reactor. © 2015 American Institute of Chemical Engineers AIChE J, 61: 1601-1612, 2015
Author	Obradović, Ana Levec, Janez
Author_xml	– sequence: 1 givenname: Ana surname: Obradović fullname: Obradović, Ana organization: Laboratory for Catalysis and Chemical Reaction Engineering, National Institute of Chemistry, Hajdrihova 19, 1000, Ljubljana, Slovenia – sequence: 2 givenname: Janez surname: Levec fullname: Levec, Janez email: janez.levec@ki.si organization: Laboratory for Catalysis and Chemical Reaction Engineering, National Institute of Chemistry, Hajdrihova 19, 1000, Ljubljana, Slovenia
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The effect of CO2 on the kinetics and extent of calcination of limestone and dolomite particles in fluidised beds. Chem Eng Sci. 1987;42:2361-2372. – reference: Obradović A, Likozar B, Levec J. Catalytic surface development of novel nickel plate catalyst with combined thermally annealed platinum and alumina coatings for steam methane reforming, Int J Hydrogen Energy. 2013;38:1419-1429. – reference: Harrison DP. Sorption-enhanced hydrogen production: a review. Ind Eng Chem Res. 2008;47:6486-6501. – reference: Verver AB, van Swaaij WPM. The hydrodynamic behaviour of gas-solid trickle flow over a regularly stacked packing. Powder Technol. 1986;45:119-132. – reference: Lee DK. An apparent kinetic model for the carbonation of calcium oxide by carbon dioxide. Chem Eng J. 2004;100:71-77. – reference: Bhatia SK, Perlmutter DD. Effect of the product layer on the kinetics of the CO2-lime reaction. AIChE J. 1983;29:79-86. – reference: Ranz WE, Marshall WR. Evaporation from drops. Chem Eng Prog. 1952;48:141-146;173-180. – reference: Verver AB, van Swaaij WPM. The gas-solid trickle-flow reactor for the catalytic oxidation of hydrogen sulphide: a trickle-phase model. Chem Eng Sci. 1987;42:435-445. – reference: Bhatia SK, Perlmutter DD. A random pore model for fluid-solid reactions: I. Isothermal, kinetic control. AIChE J. 1980;26:379-386. – reference: Finlayson B. The Method of Weighted Residuals and Variational Principles. London: Academic Press, 1972. – reference: Alvarez D, Abanades JC. Determination of the critical product layer thickness in the reaction of CaO with CO2. Ind Eng Chem Res. 2005;44:5608-5615. – reference: Westerterp KR, Kuczynski M. Gas-solid trickle flow hydrodynamics in a packed column. Chem Eng Sci. 1987;42:1539-1551. – reference: Kiel JHA, Prins W, van Swaaij WPM. Modelling of non-catalytic reactions in a gas-solid trickle flow reactor: dry, regenerative flue gas desulphurisation using a silica-supported copper oxide sorbent. Chem Eng Sci. 1992;47:4271-4286. – reference: Grasa GS, Murillo R, Alonso M, Abanades JC. Application of the random pore model to the carbonation cyclic reaction. AIChE J. 2009;55(5):1246-1255. – reference: Heesink ABM, Prins W, van Swaaij WPM. A grain size distribution model for non-catalytic gas-solid reactions. Chem Eng J. 1993;53:25-37. – reference: Nikačević NM, Duduković AP. Solids residence time distribution in gas-flowing solids-fixed bed contactors. Ind Eng Chem Res. 2005;44:6509-6517. – reference: Obradović A, Likozar B, Levec J. Steam methane reforming over Ni-based pellet-type and Pt/Ni/Al2O3 plate-type catalyst: intrinsic kinetics study. Ind Eng Chem Res. 2013;52:13597-13606. – reference: Reid RC, Prausnitz JM, Poling BE. The Properties of Gases and Liquids, 4th ed. McGraw-Hill, Inc., New York, 1987. – reference: Zhiming Z, Xu P, Xie M, Cheng Z, Yuan W. Modeling of the carbonation kinetics of a synthetic CaO-based sorbent. Chem Eng Sci. 2013;95:283-290. – reference: Grasa GS, Abanades JC. CO2 capture capacity of CaO in long series of carbonation/calcination cycles. Ind Eng Chem Res. 2006;45:8846-8851. – reference: Johnsen K, Grace JR, Elnashaie SSEH, Kolbeinsen L, Eriksen D. Modeling of sorption-enhanced steam reforming in a dual fluidized bubbling bed reactor. Ind Eng Chem Res. 2006;45:4133-4144. – reference: Wakao N, Smith JM. Diffusion in catalyst pellets. Chem Eng Sci. 1962;17:825-834. – reference: Bird RB, Stewart WE, Lightfoot, EN. Transport Phenomena. Wiley International Edition, Wiley, New York, 1960. – reference: Bhatia SK, Perlmutter DD. A random pore model for fluid-solid reactions: II. Diffusion and transport effects. AIChE J. 1981;27:247-254. – volume: 100 start-page: 71 year: 2004 end-page: 77 article-title: An apparent kinetic model for the carbonation of calcium oxide by carbon dioxide publication-title: Chem Eng J. – volume: 44 start-page: 6509 year: 2005 end-page: 6517 article-title: Solids residence time distribution in gas‐flowing solids‐fixed bed contactors publication-title: Ind Eng Chem Res. – volume: 53 start-page: 25–37 year: 1993 article-title: A grain size distribution model for non‐catalytic gas–solid reactions publication-title: Chem Eng J. – year: 1960 – year: 1987 – volume: 45 start-page: 8846 year: 2006 end-page: 8851 article-title: CO capture capacity of CaO in long series of carbonation/calcination cycles publication-title: Ind Eng Chem Res. – volume: 17 start-page: 825 year: 1962 end-page: 834 article-title: Diffusion in catalyst pellets publication-title: Chem Eng Sci. – volume: 47 start-page: 4271 year: 1992 end-page: 4286 article-title: Modelling of non‐catalytic reactions in a gas–solid trickle flow reactor: dry, regenerative flue gas desulphurisation using a silica‐supported copper oxide sorbent publication-title: Chem Eng Sci. – volume: 42 start-page: 435 year: 1987 end-page: 445 article-title: The gas–solid trickle‐flow reactor for the catalytic oxidation of hydrogen sulphide: a trickle‐phase model publication-title: Chem Eng Sci. – volume: 81 start-page: 787 year: 2003 end-page: 826 article-title: Static mixers in the process industries—a review publication-title: Trans IchemE. – volume: 137 start-page: 561 year: 2008 end-page: 567 article-title: Reactivity of highly cycled particles of CaO in a carbonation/calcination loop publication-title: Chem Eng J. – volume: 42 start-page: 1539 year: 1987 end-page: 1551 article-title: Gas–solid trickle flow hydrodynamics in a packed column publication-title: Chem Eng Sci. – volume: 48 start-page: 141 year: 1952 end-page: 146;173–180 article-title: Evaporation from drops publication-title: Chem Eng Prog. – volume: 44 start-page: 5608 year: 2005 end-page: 5615 article-title: Determination of the critical product layer thickness in the reaction of CaO with CO publication-title: Ind Eng Chem Res. – volume: 27 start-page: 247 year: 1981 end-page: 254 article-title: A random pore model for fluid–solid reactions: II. Diffusion and transport effects publication-title: AIChE J. – volume: 64 start-page: 3536 year: 2009 end-page: 3543 article-title: CO capture from syngas via cyclic carbonation/calcination for a naturally occurring limestone: modelling and bench‐scale testing publication-title: Chem Eng Sci. – volume: 55 start-page: 1246 issue: 5 year: 2009 end-page: 1255 article-title: Application of the random pore model to the carbonation cyclic reaction publication-title: AIChE J. – volume: 42 start-page: 2361 year: 1987 end-page: 2372 article-title: The effect of CO on the kinetics and extent of calcination of limestone and dolomite particles in fluidised beds publication-title: Chem Eng Sci. – volume: 26 start-page: 379 year: 1980 end-page: 386 article-title: A random pore model for fluid–solid reactions: I. Isothermal, kinetic control publication-title: AIChE J. – volume: 95 start-page: 283 year: 2013 end-page: 290 article-title: Modeling of the carbonation kinetics of a synthetic CaO‐based sorbent publication-title: Chem Eng Sci. – year: 1972 – volume: 52 start-page: 13597 year: 2013 end-page: 13606 article-title: Steam methane reforming over Ni‐based pellet‐type and Pt/Ni/Al O plate‐type catalyst: intrinsic kinetics study publication-title: Ind Eng Chem Res. – volume: 17 start-page: 81 year: 1979 end-page: 89 article-title: Hydrodynamic behaviour of a gas–solid counter‐current packed column at trickle flow publication-title: Chem Eng J. – volume: 38 start-page: 1419 year: 2013 end-page: 1429 article-title: Catalytic surface development of novel nickel plate catalyst with combined thermally annealed platinum and alumina coatings for steam methane reforming publication-title: Int J Hydrogen Energy – volume: 45 start-page: 4133 year: 2006 end-page: 4144 article-title: Modeling of sorption‐enhanced steam reforming in a dual fluidized bubbling bed reactor publication-title: Ind Eng Chem Res. – volume: 47 start-page: 6486 year: 2008 end-page: 6501 article-title: Sorption‐enhanced hydrogen production: a review publication-title: Ind Eng Chem Res. – volume: 29 start-page: 79 year: 1983 end-page: 86 article-title: Effect of the product layer on the kinetics of the CO –lime reaction publication-title: AIChE J. – volume: 45 start-page: 119 year: 1986 end-page: 132 article-title: The hydrodynamic behaviour of gas–solid trickle flow over a regularly stacked packing publication-title: Powder Technol. – volume: 77 start-page: 62 year: 1999 end-page: 68 article-title: A twin fluid‐bed reactor for removal of CO from combustion processes publication-title: Chem Eng Res Des.
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Snippet	The sorption reaction CaO–CO2 was examined in a countercurrent gas–solid trickle flow reactor with regularly stacked packing at T = 500–600°C, pCO2 = 40–50... The sorption reaction CaO-CO2 was examined in a countercurrent gas-solid trickle flow reactor with regularly stacked packing at T=500-600°C, pCO2=40-50 kPa,...
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SubjectTerms	CaO-CO2 reaction Carbon dioxide countercurrent gas-solid trickle flow Hydrodynamics Plug flow plug flow model Reactors Sorption structured packing
Title	Countercurrent gas-solid trickle flow reactor with structured packing: Hydrodynamics and CaO-CO2 reaction
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