Selective Patterning of Gold Surfaces by Core/Shell, Semisoft Hybrid Nanoparticles

The generation of patterned surfaces with well‐defined nano‐ and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold‐coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition‐fragmenta...

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Published in:	Small Vol. 11; no. 4; pp. 482 - 488
Main Authors:	Moraes, John, Ohno, Kohji, Maschmeyer, Thomas, Perrier, Sébastien
Format:	Journal Article
Language:	English
Published:	Germany Blackwell Publishing Ltd 2015 Wiley Wiley Subscription Services, Inc
Subjects:	Addition polymerization core/shell nanoparticles Gold gold surfaces nanopatterning Nanoparticles Nanotechnology Polystyrene resins QD Shells silica particles Silicon Silicon dioxide Silicon wafers Wafers silica particles core/shell nanoparticles gold surfaces nanopatterning
ISSN:	1613-6810, 1613-6829, 1613-6829
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Abstract	The generation of patterned surfaces with well‐defined nano‐ and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold‐coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition‐fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as‐prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol‐terminated nanoparticles. When gold‐coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations. The preparation of monodisperse particles with a silica core and a polystyrene shell is described using reversible addition‐fragmentation chain transfer (RAFT) polymerization. The particles prepared this way display either trithiocarbonate or thiolate end groups. The thiolated particles are shown to selectively deposit onto gold domains of a patterned silicon wafer while trithiocarbonate‐functionalize particles deposited onto both gold and silicon domains with an aggregation‐free coverage.
AbstractList	The generation of patterned surfaces with well-defined nano- and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold-coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition-fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as-prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol-terminated nanoparticles. When gold-coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations. The preparation of monodisperse particles with a silica core and a polystyrene shell is described using reversible addition-fragmentation chain transfer (RAFT) polymerization. The particles prepared this way display either trithiocarbonate or thiolate end groups. The thiolated particles are shown to selectively deposit onto gold domains of a patterned silicon wafer while trithiocarbonate-functionalize particles deposited onto both gold and silicon domains with an aggregation-free coverage. The generation of patterned surfaces with well-defined nano- and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold-coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition-fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as-prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol-terminated nanoparticles. When gold-coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations. The generation of patterned surfaces with well-defined nano- and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold-coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition-fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as-prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol-terminated nanoparticles. When gold-coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations.The generation of patterned surfaces with well-defined nano- and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold-coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition-fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as-prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol-terminated nanoparticles. When gold-coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations. The generation of patterned surfaces with well‐defined nano‐ and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size distribution to microdomains of a gold‐coated silicon wafer. Near monodisperse nanoparticles are prepared using reversible addition‐fragmentation chain transfer (RAFT) polymerization, initiated from a silica surface, to prepare a polystyrene shell around a silica core. The particles are then used as‐prepared, or after aminolysis of the terminal thiocarbonyl group of the polystyrene shell, to give thiol‐terminated nanoparticles. When gold‐coated silicon wafers are immersed into very dilute suspensions of these particles (as low as 0.004 wt%), both types of particles are shown to adhere to the gold domains. The thiolated particles adhere selectively to the gold microdomains, allowing for microdomain patterning, while particles that contain the trithiocarbonate functionality lead to a much more even coverage of the gold surface with fewer particle aggregations. The preparation of monodisperse particles with a silica core and a polystyrene shell is described using reversible addition‐fragmentation chain transfer (RAFT) polymerization. The particles prepared this way display either trithiocarbonate or thiolate end groups. The thiolated particles are shown to selectively deposit onto gold domains of a patterned silicon wafer while trithiocarbonate‐functionalize particles deposited onto both gold and silicon domains with an aggregation‐free coverage.
Author	Ohno, Kohji Perrier, Sébastien Maschmeyer, Thomas Moraes, John
Author_xml	– sequence: 1 givenname: John surname: Moraes fullname: Moraes, John organization: Key Centre for Polymers & Colloids, School of Chemistry, The University of Sydney, NSW, 2006, Australia – sequence: 2 givenname: Kohji surname: Ohno fullname: Ohno, Kohji organization: Institute for Chemical Research, Kyoto University, Kyoto, 611-0011, Uji, Japan – sequence: 3 givenname: Thomas surname: Maschmeyer fullname: Maschmeyer, Thomas organization: Laboratory of Advanced Catalysis for Sustainability, School of Chemistry, The University of Sydney, NSW, 2006, Australia – sequence: 4 givenname: Sébastien surname: Perrier fullname: Perrier, Sébastien email: s.perrier@warwick.ac.uk organization: Key Centre for Polymers & Colloids, School of Chemistry, The University of Sydney, NSW, 2006, Australia
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Snippet	The generation of patterned surfaces with well‐defined nano‐ and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size... The generation of patterned surfaces with well-defined nano- and microdomains is demonstrated by attaching core/shell, semisoft nanoparticles with narrow size...
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SubjectTerms	Addition polymerization core/shell nanoparticles Gold gold surfaces nanopatterning Nanoparticles Nanotechnology Polystyrene resins QD Shells silica particles Silicon Silicon dioxide Silicon wafers Wafers
Title	Selective Patterning of Gold Surfaces by Core/Shell, Semisoft Hybrid Nanoparticles
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