Three-Dimensional Visualization of Defects Formed during the Synthesis of Metal-Organic Frameworks: A Fluorescence Microscopy Study

Imperfections in the spotlight: Fluorescence microscopy was used to detect defects in metal–organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three‐dimensional imaging at the single‐crystal level combin...

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Published in:	Angewandte Chemie International Edition Vol. 52; no. 1; pp. 401 - 405
Main Authors:	Ameloot, Rob, Vermoortele, Frederik, Hofkens, Johan, De Schryver, Frans C., De Vos, Dirk E., Roeffaers, Maarten B. J.
Format:	Journal Article
Language:	English
Published:	Weinheim WILEY-VCH Verlag 02.01.2013 WILEY‐VCH Verlag Wiley Subscription Services, Inc
Edition:	International ed. in English
Subjects:	Communications Confocal crystal growth Defects Fluorescence Fluorescence microscopy Formations Metal-organic frameworks microporous materials Microscopy Synthesis Three dimensional Visualization
ISSN:	1433-7851, 1521-3773, 1521-3773
Online Access:	Get full text
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Abstract	Imperfections in the spotlight: Fluorescence microscopy was used to detect defects in metal–organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three‐dimensional imaging at the single‐crystal level combined with the sensitivity required to study the start of defect formation.
AbstractList	Imperfections in the spotlight: fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three-dimensional imaging at the single-crystal level combined with the sensitivity required to study the start of defect formation.Imperfections in the spotlight: fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three-dimensional imaging at the single-crystal level combined with the sensitivity required to study the start of defect formation. Imperfections in the spotlight: fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three-dimensional imaging at the single-crystal level combined with the sensitivity required to study the start of defect formation.
Author	De Vos, Dirk E. Roeffaers, Maarten B. J. Vermoortele, Frederik De Schryver, Frans C. Hofkens, Johan Ameloot, Rob
Author_xml	– sequence: 1 givenname: Rob surname: Ameloot fullname: Ameloot, Rob organization: Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium) – sequence: 2 givenname: Frederik surname: Vermoortele fullname: Vermoortele, Frederik organization: Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium) – sequence: 3 givenname: Johan surname: Hofkens fullname: Hofkens, Johan organization: Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium) – sequence: 4 givenname: Frans C. surname: De Schryver fullname: De Schryver, Frans C. organization: Department of Chemistry, Katholieke Universiteit Leuven, Celestijnenlaan 200F, 3001 Leuven (Belgium) – sequence: 5 givenname: Dirk E. surname: De Vos fullname: De Vos, Dirk E. organization: Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium) – sequence: 6 givenname: Maarten B. J. surname: Roeffaers fullname: Roeffaers, Maarten B. J. email: maarten.roeffaers@biw.kuleuven.be organization: Center for Surface Chemistry and Catalysis, Katholieke Universiteit Leuven, Kasteelpark Arenberg 23, 3001 Leuven (Belgium)
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/23143805$$D View this record in MEDLINE/PubMed
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Copyright	2013 The Authors. Published by Wiley‐VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution Non‐Commercial License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim 2013 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. 2013
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Notes	istex:34C1E37E84E0219245F14C04E0D9D1BBBC9047DD Funded Access ArticleID:ANIE201205627 This research was supported financially by Belspo (IAP 7), the Flemish government (long-term structural funding-Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.). European Research Council - No. 307523 Belspo Flemish government - No. METH/08/04 ark:/67375/WNG-LFR937K8-M This research was supported financially by Belspo (IAP 7), the Flemish government (long‐term structural funding—Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.). ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23 This research was supported financially by Belspo (IAP 7), the Flemish government (long-term structural funding—Methusalem funding CASAS METH/08/04), FWO Vlaanderen (postdoctoral research fellowship to R.A.), and the European Research Council (ERC Starting Grant 307523 to M.B.J.R.).
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SSID	ssj0028806
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Snippet	Imperfections in the spotlight: Fluorescence microscopy was used to detect defects in metal–organic frameworks formed during synthesis. In contrast to... Imperfections in the spotlight: fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to... Imperfections in the spotlight: Fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to...
SourceID	pubmedcentral proquest pubmed crossref wiley istex
SourceType	Open Access Repository Aggregation Database Index Database Enrichment Source Publisher
StartPage	401
SubjectTerms	Communications Confocal crystal growth Defects Fluorescence Fluorescence microscopy Formations Metal-organic frameworks microporous materials Microscopy Synthesis Three dimensional Visualization
Title	Three-Dimensional Visualization of Defects Formed during the Synthesis of Metal-Organic Frameworks: A Fluorescence Microscopy Study
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Volume	52
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