Independent tuning of size and coverage of supported Pt nanoparticles using atomic layer deposition

Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility...

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Vydáno v:	Nature communications Ročník 8; číslo 1; s. 1074 - 12
Hlavní autoři:	Dendooven, Jolien, Ramachandran, Ranjith K., Solano, Eduardo, Kurttepeli, Mert, Geerts, Lisa, Heremans, Gino, Rongé, Jan, Minjauw, Matthias M., Dobbelaere, Thomas, Devloo-Casier, Kilian, Martens, Johan A., Vantomme, André, Bals, Sara, Portale, Giuseppe, Coati, Alessandro, Detavernier, Christophe
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	London Nature Publishing Group UK 20.10.2017 Nature Publishing Group Nature Portfolio
Témata:	639/301/299 639/301/357/354 639/301/930/1032 Atomic layer epitaxy Catalysis Catalysts Grazing incidence Humanities and Social Sciences multidisciplinary Nanoparticles Nitrogen plasma Particle size Physics Platinum Science Science (multidisciplinary) Small angle X ray scattering Tuning X-ray fluorescence X-ray scattering
ISSN:	2041-1723, 2041-1723
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Abstract	Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance. The performance of supported nanoparticle catalysts is closely related to their size, shape and interparticle distance. Here, the authors introduce an atomic layer deposition-based strategy to independently tune the size and coverage of platinum nanoparticles with atomic-level precision.
AbstractList	Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance. The performance of supported nanoparticle catalysts is closely related to their size, shape and interparticle distance. Here, the authors introduce an atomic layer deposition-based strategy to independently tune the size and coverage of platinum nanoparticles with atomic-level precision. Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl) platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance. The performance of supported nanoparticle catalysts is closely related to their size, shape and interparticle distance. Here, the authors introduce an atomic layer deposition-based strategy to independently tune the size and coverage of platinum nanoparticles with atomic-level precision. Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance.Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance. Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work, we propose a strategy that allows precise and independent control of the Pt particle size and coverage. Our approach exploits the versatility of the atomic layer deposition (ALD) technique by combining two ALD processes for Pt using different reactants. The particle areal density is controlled by tailoring the number of ALD cycles using trimethyl(methylcyclopentadienyl)platinum and oxygen, while subsequent growth using the same Pt precursor in combination with nitrogen plasma allows for tuning of the particle size at the atomic level. The excellent control over the particle morphology is clearly demonstrated by means of in situ and ex situ X-ray fluorescence and grazing incidence small angle X-ray scattering experiments, providing information about the Pt loading, average particle dimensions, and mean center-to-center particle distance. The performance of supported nanoparticle catalysts is closely related to their size, shape and interparticle distance. Here, the authors introduce an atomic layer deposition-based strategy to independently tune the size and coverage of platinum nanoparticles with atomic-level precision.
ArticleNumber	1074
Author	Heremans, Gino Dobbelaere, Thomas Devloo-Casier, Kilian Ramachandran, Ranjith K. Minjauw, Matthias M. Martens, Johan A. Geerts, Lisa Dendooven, Jolien Detavernier, Christophe Solano, Eduardo Kurttepeli, Mert Portale, Giuseppe Rongé, Jan Coati, Alessandro Vantomme, André Bals, Sara
Author_xml	– sequence: 1 givenname: Jolien orcidid: 0000-0002-2385-3693 surname: Dendooven fullname: Dendooven, Jolien organization: Department of Solid State Sciences, COCOON, Ghent University – sequence: 2 givenname: Ranjith K. orcidid: 0000-0002-9423-219X surname: Ramachandran fullname: Ramachandran, Ranjith K. organization: Department of Solid State Sciences, COCOON, Ghent University – sequence: 3 givenname: Eduardo surname: Solano fullname: Solano, Eduardo organization: Department of Solid State Sciences, COCOON, Ghent University, ALBA Synchrotron Light Source, NCD beamline – sequence: 4 givenname: Mert surname: Kurttepeli fullname: Kurttepeli, Mert organization: Electron Microscopy for Materials Science (EMAT), University of Antwerp – sequence: 5 givenname: Lisa orcidid: 0000-0003-0188-3039 surname: Geerts fullname: Geerts, Lisa organization: Center for Surface Chemistry and Catalysis, KU Leuven – sequence: 6 givenname: Gino orcidid: 0000-0001-6489-8188 surname: Heremans fullname: Heremans, Gino organization: Center for Surface Chemistry and Catalysis, KU Leuven – sequence: 7 givenname: Jan orcidid: 0000-0003-0315-5676 surname: Rongé fullname: Rongé, Jan organization: Center for Surface Chemistry and Catalysis, KU Leuven – sequence: 8 givenname: Matthias M. orcidid: 0000-0003-3620-8949 surname: Minjauw fullname: Minjauw, Matthias M. organization: Department of Solid State Sciences, COCOON, Ghent University – sequence: 9 givenname: Thomas surname: Dobbelaere fullname: Dobbelaere, Thomas organization: Department of Solid State Sciences, COCOON, Ghent University – sequence: 10 givenname: Kilian surname: Devloo-Casier fullname: Devloo-Casier, Kilian organization: Department of Solid State Sciences, COCOON, Ghent University – sequence: 11 givenname: Johan A. surname: Martens fullname: Martens, Johan A. organization: Center for Surface Chemistry and Catalysis, KU Leuven – sequence: 12 givenname: André surname: Vantomme fullname: Vantomme, André organization: Instituut voor Kern- en Stralingsfysica, KU Leuven – sequence: 13 givenname: Sara surname: Bals fullname: Bals, Sara organization: Electron Microscopy for Materials Science (EMAT), University of Antwerp – sequence: 14 givenname: Giuseppe orcidid: 0000-0002-4903-3159 surname: Portale fullname: Portale, Giuseppe organization: ESRF European Synchrotron, DUBBLE Beamline BM26, Macromolecular Chemistry & New Polymeric Materials, University of Groningen – sequence: 15 givenname: Alessandro surname: Coati fullname: Coati, Alessandro organization: Synchrotron SOLEIL, SixS Beamline, L′Orme des Merisiers – sequence: 16 givenname: Christophe orcidid: 0000-0001-7653-0858 surname: Detavernier fullname: Detavernier, Christophe email: Christophe.Detavernier@UGent.be organization: Department of Solid State Sciences, COCOON, Ghent University
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Snippet	Synthetic methods that allow for the controlled design of well-defined Pt nanoparticles are highly desirable for fundamental catalysis research. In this work,... The performance of supported nanoparticle catalysts is closely related to their size, shape and interparticle distance. Here, the authors introduce an atomic...
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SubjectTerms	639/301/299 639/301/357/354 639/301/930/1032 Atomic layer epitaxy Catalysis Catalysts Grazing incidence Humanities and Social Sciences multidisciplinary Nanoparticles Nitrogen plasma Particle size Physics Platinum Science Science (multidisciplinary) Small angle X ray scattering Tuning X-ray fluorescence X-ray scattering
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Title	Independent tuning of size and coverage of supported Pt nanoparticles using atomic layer deposition
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