Effect of polyethylene glycol on pore structure and separation efficiency of silica-based monolithic capillary columns

•We investigated the effect of PEGs on the structure of monolithic silica capillary columns.•Columns with smaller domain size than previous 2nd generation monoliths were developed.•Improved kinetic performance in the region of N≤40,000 plates is obtained.•Performance improvement is due to smaller do...

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Vydáno v:	Journal of Chromatography A Ročník 1442; s. 42 - 52
Hlavní autoři:	Hara, Takeshi, Desmet, Gert, Baron, Gino V., Minakuchi, Hiroyoshi, Eeltink, Sebastiaan
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Netherlands Elsevier B.V 15.04.2016
Témata:	argon (noble gases) Capillarity Capillary column Chemistry Techniques, Analytical - instrumentation Chemistry Techniques, Analytical - standards chromatography Column efficiency Columns (structural) Core-shell particles Kinetic performance Kinetics mercury Molecular Weight Permeability Polyethylene glycol Polyethylene Glycols - chemistry Porosity Reproducibility of Results Rods silica Silica monolith Silicon dioxide Silicon Dioxide - chemistry Small domain size Tuning Capillary column Kinetic performance Column efficiency Small domain size Silica monolith
ISSN:	0021-9673, 1873-3778, 1873-3778
On-line přístup:	Získat plný text
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