Imaging the facet surface strain state of supported multi-faceted Pt nanoparticles during reaction
Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographi...
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| Vydáno v: | Nature communications Ročník 13; číslo 1; s. 3003 - 10 |
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| Hlavní autoři: | , , , , , , , , , , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
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London
Nature Publishing Group UK
30.05.2022
Nature Publishing Group Nature Portfolio |
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| ISSN: | 2041-1723, 2041-1723 |
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| Abstract | Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical {
hkl
} facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O
2
adsorption or desorption during O
2
exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields.
Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here the authors demonstrate how the 3D lattice displacement and strain evolution depend on the crystallographic facets of Pt nanoparticles during CO oxidation reaction, providing new insights in the relationship between facet-related surface strain and chemistry. |
|---|---|
| AbstractList | Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical {hkl} facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O2 adsorption or desorption during O2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here the authors demonstrate how the 3D lattice displacement and strain evolution depend on the crystallographic facets of Pt nanoparticles during CO oxidation reaction, providing new insights in the relationship between facet-related surface strain and chemistry. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here the authors demonstrate how the 3D lattice displacement and strain evolution depend on the crystallographic facets of Pt nanoparticles during CO oxidation reaction, providing new insights in the relationship between facet-related surface strain and chemistry. Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical { hkl } facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O 2 adsorption or desorption during O 2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here the authors demonstrate how the 3D lattice displacement and strain evolution depend on the crystallographic facets of Pt nanoparticles during CO oxidation reaction, providing new insights in the relationship between facet-related surface strain and chemistry. Abstract Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical { hkl } facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O 2 adsorption or desorption during O 2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical {hkl} facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O adsorption or desorption during O exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical { hkl } facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O 2 adsorption or desorption during O 2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical {hkl} facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O2 adsorption or desorption during O2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields.Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in widespread applications in catalysis, energy conversion or sensing. Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here, we reveal in situ, in three-dimensions and at the nanoscale, the volume, surface and interface strain evolution of single supported platinum nanocrystals during reaction using coherent x-ray diffractive imaging. Interestingly, identical {hkl} facets show equivalent catalytic response during non-stoichiometric cycles. Periodic strain variations are rationalised in terms of O2 adsorption or desorption during O2 exposure or CO oxidation under reducing conditions, respectively. During stoichiometric CO oxidation, the strain evolution is, however, no longer facet dependent. Large strain variations are observed in localised areas, in particular in the vicinity of the substrate/particle interface, suggesting a significant influence of the substrate on the reactivity. These findings will improve the understanding of dynamic properties in catalysis and related fields. |
| ArticleNumber | 3003 |
| Author | Li, Ni Westermeier, Fabian Richard, Marie-Ingrid Thomas, Olivier Sprung, Michael Dupraz, Maxime van de Poll, Rim Rabkin, Eugen Wu, Longfei Carnis, Jérôme Chatelier, Corentin Hensen, Emiel J. M. Almog, Ehud Hofmann, Jan P. Watier, Yves Labat, Stéphane Leake, Steven J. Lazarev, Sergey |
| Author_xml | – sequence: 1 givenname: Maxime orcidid: 0000-0003-3213-6255 surname: Dupraz fullname: Dupraz, Maxime email: maxime.dupraz@esrf.fr organization: Univ. Grenoble Alpes, CEA Grenoble, IRIG, MEM, NRS, ESRF - The European Synchrotron – sequence: 2 givenname: Ni surname: Li fullname: Li, Ni organization: Univ. Grenoble Alpes, CEA Grenoble, IRIG, MEM, NRS, ESRF - The European Synchrotron – sequence: 3 givenname: Jérôme orcidid: 0000-0001-7270-6211 surname: Carnis fullname: Carnis, Jérôme organization: ESRF - The European Synchrotron, Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334 – sequence: 4 givenname: Longfei surname: Wu fullname: Wu, Longfei organization: ESRF - The European Synchrotron, Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334 – sequence: 5 givenname: Stéphane surname: Labat fullname: Labat, Stéphane organization: Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334 – sequence: 6 givenname: Corentin surname: Chatelier fullname: Chatelier, Corentin organization: Univ. Grenoble Alpes, CEA Grenoble, IRIG, MEM, NRS, ESRF - The European Synchrotron – sequence: 7 givenname: Rim surname: van de Poll fullname: van de Poll, Rim organization: Laboratory for Inorganic Materials and Catalysis, Department of Chemical Engineering and Chemistry, Eindhoven University of Technology – sequence: 8 givenname: Jan P. orcidid: 0000-0002-5765-1096 surname: Hofmann fullname: Hofmann, Jan P. organization: Laboratory for Inorganic Materials and Catalysis, Department of Chemical Engineering and Chemistry, Eindhoven University of Technology, Surface Science Laboratory, Department of Materials and Earth Sciences, Technical University of Darmstadt – sequence: 9 givenname: Ehud surname: Almog fullname: Almog, Ehud organization: Department of Materials Science and Engineering, Technion-Israel Institute of Technology – sequence: 10 givenname: Steven J. orcidid: 0000-0003-1640-0386 surname: Leake fullname: Leake, Steven J. organization: ESRF - The European Synchrotron – sequence: 11 givenname: Yves surname: Watier fullname: Watier, Yves organization: ESRF - The European Synchrotron – sequence: 12 givenname: Sergey surname: Lazarev fullname: Lazarev, Sergey organization: Deutsches Elektronen-Synchrotron (DESY) – sequence: 13 givenname: Fabian orcidid: 0000-0003-0696-206X surname: Westermeier fullname: Westermeier, Fabian organization: Deutsches Elektronen-Synchrotron (DESY) – sequence: 14 givenname: Michael surname: Sprung fullname: Sprung, Michael organization: Deutsches Elektronen-Synchrotron (DESY) – sequence: 15 givenname: Emiel J. M. orcidid: 0000-0002-9754-2417 surname: Hensen fullname: Hensen, Emiel J. M. organization: Laboratory for Inorganic Materials and Catalysis, Department of Chemical Engineering and Chemistry, Eindhoven University of Technology – sequence: 16 givenname: Olivier orcidid: 0000-0002-0583-9257 surname: Thomas fullname: Thomas, Olivier organization: Aix Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334 – sequence: 17 givenname: Eugen orcidid: 0000-0001-5545-1261 surname: Rabkin fullname: Rabkin, Eugen organization: Department of Materials Science and Engineering, Technion-Israel Institute of Technology – sequence: 18 givenname: Marie-Ingrid orcidid: 0000-0002-8172-3141 surname: Richard fullname: Richard, Marie-Ingrid email: mrichard@esrf.fr organization: Univ. Grenoble Alpes, CEA Grenoble, IRIG, MEM, NRS, ESRF - The European Synchrotron |
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| DOI | 10.1038/s41467-022-30592-1 |
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| Snippet | Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements, resulting in... Abstract Nanostructures with specific crystallographic planes display distinctive physico-chemical properties because of their unique atomic arrangements,... Understanding strain dynamics and their relationship with crystallographic facets have been largely unexplored. Here the authors demonstrate how the 3D lattice... |
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| Title | Imaging the facet surface strain state of supported multi-faceted Pt nanoparticles during reaction |
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