Enabling hydrate-based methane storage under mild operating conditions by periodic mesoporous organosilica nanotubes
Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodi...
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| Vydáno v: | Heliyon Ročník 9; číslo 7; s. e17662 |
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| Hlavní autoři: | , , , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
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England
Elsevier Ltd
01.07.2023
Elsevier |
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| ISSN: | 2405-8440, 2405-8440 |
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| Abstract | Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material’s excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates.
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| AbstractList | Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material’s excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates.
Image 1 Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material's excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates.Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material's excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates. Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material's excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates. Biomethane is a renewable natural gas substitute produced from biogas. Storage of this sustainable energy vector in confined clathrate hydrates, encapsulated in the pores of a host material, is a highly promising avenue to improve storage capacity and energy efficiency. Herein, a new type of periodic mesoporous organosilica (PMO) nanotubes, referred to as hollow ring PMO (HR-PMO), capable of promoting methane clathrate hydrate formation under mild working conditions (273 K, 3.5 MPa) and at high water loading (5.1 g water/g HR-PMO) is reported. Gravimetric uptake measurements reveal a steep single-stepped isotherm and a noticeably high methane storage capacity (0.55 g methane/g HR-PMO; 0.11 g methane/g water at 3.5 MPa). The large working capacity throughout consecutive pressure-induced clathrate hydrate formation-dissociation cycles demonstrates the material’s excellent recyclability (97% preservation of capacity). Supported by ex situ cryo-electron tomography and x-ray diffraction, HR-PMO nanotubes are hypothesized to promote clathrate hydrate nucleation and growth by distribution and confinement of water in the mesopores of their outer wall, along the central channels of the nanotubes and on the external nanotube surface. These findings showcase the potential for application of organosilica materials with hierarchical and interconnected pore systems for pressure-based storage of biomethane in confined clathrate hydrates. [Display omitted] |
| ArticleNumber | e17662 |
| Author | Beckwée, Emile Jules Breynaert, Eric Watson, Geert Baron, Gino V. Van Der Voort, Pascal Arenas Esteban, Daniel Martens, Johan Denayer, Joeri F.M. Houlleberghs, Maarten Bals, Sara |
| Author_xml | – sequence: 1 givenname: Emile Jules orcidid: 0000-0002-4135-4249 surname: Beckwée fullname: Beckwée, Emile Jules organization: Department of Chemical Engineering, Vrije Universiteit Brussel, Pleinlaan 2, 1050, Brussel, Belgium – sequence: 2 givenname: Geert orcidid: 0000-0002-2324-4521 surname: Watson fullname: Watson, Geert organization: Center for Ordered Materials, Organometallics and Catalysis, Department of Chemistry, Ghent University, Krijgslaan 281, B-9000, Ghent, Belgium – sequence: 3 givenname: Maarten orcidid: 0000-0002-8456-0886 surname: Houlleberghs fullname: Houlleberghs, Maarten organization: Centre for Surface Chemistry and Catalysis, NMRCoRe - NMR - XRAY - EM Platform for Convergence Research, Department of Microbial and Molecular Systems (M2S), KU Leuven, Celestijnenlaan 200F, 3001, Leuven, Belgium – sequence: 4 givenname: Daniel orcidid: 0000-0002-5626-9848 surname: Arenas Esteban fullname: Arenas Esteban, Daniel organization: Electron Microscopy for Materials Science, Department of Physics, University of Antwerp, Groenenborgerlaan 171, 2020, Antwerp, Belgium – sequence: 5 givenname: Sara surname: Bals fullname: Bals, Sara organization: Electron Microscopy for Materials Science, Department of Physics, University of Antwerp, Groenenborgerlaan 171, 2020, Antwerp, Belgium – sequence: 6 givenname: Pascal orcidid: 0000-0002-1248-479X surname: Van Der Voort fullname: Van Der Voort, Pascal organization: Center for Ordered Materials, Organometallics and Catalysis, Department of Chemistry, Ghent University, Krijgslaan 281, B-9000, Ghent, Belgium – sequence: 7 givenname: Eric orcidid: 0000-0003-3499-0455 surname: Breynaert fullname: Breynaert, Eric organization: Centre for Surface Chemistry and Catalysis, NMRCoRe - NMR - XRAY - EM Platform for Convergence Research, Department of Microbial and Molecular Systems (M2S), KU Leuven, Celestijnenlaan 200F, 3001, Leuven, Belgium – sequence: 8 givenname: Johan surname: Martens fullname: Martens, Johan organization: Centre for Surface Chemistry and Catalysis, NMRCoRe - NMR - XRAY - EM Platform for Convergence Research, Department of Microbial and Molecular Systems (M2S), KU Leuven, Celestijnenlaan 200F, 3001, Leuven, Belgium – sequence: 9 givenname: Gino V. orcidid: 0000-0003-4483-2434 surname: Baron fullname: Baron, Gino V. organization: Department of Chemical Engineering, Vrije Universiteit Brussel, Pleinlaan 2, 1050, Brussel, Belgium – sequence: 10 givenname: Joeri F.M. orcidid: 0000-0001-5587-5136 surname: Denayer fullname: Denayer, Joeri F.M. email: joeri.denayer@vub.be organization: Department of Chemical Engineering, Vrije Universiteit Brussel, Pleinlaan 2, 1050, Brussel, Belgium |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/37449178$$D View this record in MEDLINE/PubMed |
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| Issue | 7 |
| Keywords | Methane hydrate Periodic mesoporous organosilica Biomethane Clathrate hydrate Pressure-swing (un)loading |
| Language | English |
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| Title | Enabling hydrate-based methane storage under mild operating conditions by periodic mesoporous organosilica nanotubes |
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