Chemically stable polyarylether-based covalent organic frameworks
The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including tow...
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| Published in: | Nature chemistry Vol. 11; no. 6; pp. 587 - 594 |
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| Main Authors: | , , , , , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
London
Nature Publishing Group UK
01.06.2019
Nature Publishing Group |
| Subjects: | |
| ISSN: | 1755-4330, 1755-4349, 1755-4349 |
| Online Access: | Get full text |
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| Abstract | The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between
ortho
-difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal–organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range.
The development of porous, crystalline materials with high chemical stability is crucial for their practical uses. Now, polyarylether-based covalent organic frameworks (PAE-COFs) have been synthesized that show high crystallinity and porosity, as well as good stability against harsh chemical environments including boiling water and strong acids and bases. |
|---|---|
| AbstractList | The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between ortho-difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal–organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range.The development of porous, crystalline materials with high chemical stability is crucial for their practical uses. Now, polyarylether-based covalent organic frameworks (PAE-COFs) have been synthesized that show high crystallinity and porosity, as well as good stability against harsh chemical environments including boiling water and strong acids and bases. The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between ortho-difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal-organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range. The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between ortho -difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal–organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range. The development of porous, crystalline materials with high chemical stability is crucial for their practical uses. Now, polyarylether-based covalent organic frameworks (PAE-COFs) have been synthesized that show high crystallinity and porosity, as well as good stability against harsh chemical environments including boiling water and strong acids and bases. The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between ortho-difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal-organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range.The development of crystalline porous materials with high chemical stability is of paramount importance for their practical application. Here, we report the synthesis of polyarylether-based covalent organic frameworks (PAE-COFs) with high crystallinity, porosity and chemical stability, including towards water, owing to the inert nature of their polyarylether-based building blocks. The PAE-COFs are synthesized through nucleophilic aromatic substitution reactions between ortho-difluoro benzene and catechol building units, which form ether linkages. The resulting materials are shown to be stable against harsh chemical environments including boiling water, strong acids and bases, and oxidation and reduction conditions. Their stability surpasses the performance of other known crystalline porous materials such as zeolites, metal-organic frameworks and covalent organic frameworks. We also demonstrate the post-synthetic functionalization of these materials with carboxyl or amino functional groups. The functionalized PAE-COFs combine porosity, high stability and recyclability. A preliminary application of these materials is demonstrated with the removal of antibiotics from water over a wide pH range. |
| Author | Xue, Ming Yan, Yushan Qiu, Shilun Li, Hui Ma, Yunchao Fang, Qianrong Guan, Xinyu Valtchev, Valentin |
| Author_xml | – sequence: 1 givenname: Xinyu surname: Guan fullname: Guan, Xinyu organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University – sequence: 2 givenname: Hui surname: Li fullname: Li, Hui organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University – sequence: 3 givenname: Yunchao surname: Ma fullname: Ma, Yunchao organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University – sequence: 4 givenname: Ming surname: Xue fullname: Xue, Ming organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University – sequence: 5 givenname: Qianrong orcidid: 0000-0003-3365-5508 surname: Fang fullname: Fang, Qianrong email: qrfang@jlu.edu.cn organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University – sequence: 6 givenname: Yushan orcidid: 0000-0001-6616-4575 surname: Yan fullname: Yan, Yushan email: yanys@udel.edu organization: Department of Chemical and Biomolecular Engineering, Center for Catalytic Science and Technology, University of Delaware – sequence: 7 givenname: Valentin orcidid: 0000-0002-2341-6397 surname: Valtchev fullname: Valtchev, Valentin email: valentin.valtchev@ensicaen.fr organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Normandie Université, ENSICAEN, UNICAEN, CNRS – sequence: 8 givenname: Shilun surname: Qiu fullname: Qiu, Shilun organization: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30962609$$D View this record in MEDLINE/PubMed https://normandie-univ.hal.science/hal-03035133$$DView record in HAL |
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| Title | Chemically stable polyarylether-based covalent organic frameworks |
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