Gallium Oxide Nanorods: Novel, Template-Free Synthesis and High Catalytic Activity in Epoxidation Reactions

Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2O2, rivaling the industrial benchmark...

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Published in:	Angewandte Chemie International Edition Vol. 53; no. 6; pp. 1585 - 1589
Main Authors:	Lueangchaichaweng, Warunee, Brooks, Neil R., Fiorilli, Sonia, Gobechiya, Elena, Lin, Kaifeng, Li, Li, Parres-Esclapez, Sonia, Javon, Elsa, Bals, Sara, Van Tendeloo, Gustaaf, Martens, Johan A., Kirschhock, Christine E. A., Jacobs, Pierre A., Pescarmona, Paolo P.
Format:	Journal Article
Language:	English
Published:	Weinheim WILEY-VCH Verlag 03.02.2014 WILEY‐VCH Verlag Wiley Subscription Services, Inc
Edition:	International ed. in English
Subjects:	Alkenes Catalysts Epoxidation Gallium gallium oxide Gallium oxides heterogeneous catalysis Hydrogen peroxide Nanorods Nanostructure Physicochemical properties R&D Research & development Specific surface Synthesis gallium oxide epoxidation heterogeneous catalysis nanorods hydrogen peroxide
ISSN:	1433-7851, 1521-3773, 1521-3773
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Abstract	Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2O2, rivaling the industrial benchmark microporous titanosilicate TS‐1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Selective epoxidation: Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. The nanorods are much superior to conventional gallium oxide both in terms of specific surface area and number of acid sites and display excellent performance as epoxidation catalyst with H2O2 as the oxidant (see picture).
AbstractList	Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H 2 O 2 , rivaling the industrial benchmark microporous titanosilicate TS‐1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Gallium oxide nanorods with unprecedented small dimensions (20-80nm length and 3-5nm width) were prepared using a novel, template-free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2O2, rivaling the industrial benchmark microporous titanosilicate TS-1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. [PUBLICATION ABSTRACT] Gallium oxide nanorods with unprecedented small dimensions (20-80nm length and 3-5nm width) were prepared using a novel, template-free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H sub(2)O sub(2), rivaling the industrial benchmark microporous titanosilicate TS-1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Selective epoxidation: Gallium oxide nanorods with unprecedented small dimensions (20-80nm length and 3-5nm width) were prepared using a novel, template-free synthesis method. The nanorods are much superior to conventional gallium oxide both in terms of specific surface area and number of acid sites and display excellent performance as epoxidation catalyst with H sub(2)O sub(2) as the oxidant (see picture). Gallium oxide nanorods with unprecedented small dimensions (20-80 nm length and 3-5 nm width) were prepared using a novel, template-free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2 O2 , rivaling the industrial benchmark microporous titanosilicate TS-1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Gallium oxide nanorods with unprecedented small dimensions (20-80 nm length and 3-5 nm width) were prepared using a novel, template-free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2 O2 , rivaling the industrial benchmark microporous titanosilicate TS-1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites.Gallium oxide nanorods with unprecedented small dimensions (20-80 nm length and 3-5 nm width) were prepared using a novel, template-free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2 O2 , rivaling the industrial benchmark microporous titanosilicate TS-1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. This nanomaterial is an excellent heterogeneous catalyst for the sustainable epoxidation of alkenes with H2O2, rivaling the industrial benchmark microporous titanosilicate TS‐1 with linear alkenes and being much superior with bulkier substrates. A thorough characterization study elucidated the correlation between the physicochemical properties of the gallium oxide nanorods and their catalytic performance, and underlined the importance of the nanorod morphology for generating a material with high specific surface area and a high number of accessible acid sites. Selective epoxidation: Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. The nanorods are much superior to conventional gallium oxide both in terms of specific surface area and number of acid sites and display excellent performance as epoxidation catalyst with H2O2 as the oxidant (see picture).
Author	Li, Li Javon, Elsa Lueangchaichaweng, Warunee Van Tendeloo, Gustaaf Fiorilli, Sonia Martens, Johan A. Jacobs, Pierre A. Pescarmona, Paolo P. Parres-Esclapez, Sonia Lin, Kaifeng Brooks, Neil R. Kirschhock, Christine E. A. Gobechiya, Elena Bals, Sara
Author_xml	– sequence: 1 givenname: Warunee surname: Lueangchaichaweng fullname: Lueangchaichaweng, Warunee organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 2 givenname: Neil R. surname: Brooks fullname: Brooks, Neil R. organization: Department of Chemistry, University of Leuven, Celestijnenlaan 200F, Heverlee, 3001 (Belgium) – sequence: 3 givenname: Sonia surname: Fiorilli fullname: Fiorilli, Sonia organization: DISAT, Politecnico di Torino, Corso Duca degli Abruzzi 24, Torino, 10129 (Italy) – sequence: 4 givenname: Elena surname: Gobechiya fullname: Gobechiya, Elena organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 5 givenname: Kaifeng surname: Lin fullname: Lin, Kaifeng organization: Natural Science Research Centre, Academy of Fundamental and Interdisciplinary Science, Harbin Institute of Technology box-3026, 150080 Harbin (China) – sequence: 6 givenname: Li surname: Li fullname: Li, Li organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 7 givenname: Sonia surname: Parres-Esclapez fullname: Parres-Esclapez, Sonia organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 8 givenname: Elsa surname: Javon fullname: Javon, Elsa organization: EMAT, University of Antwerp, Groenenborgerlaan 171, 2020 Antwerp (Belgium) – sequence: 9 givenname: Sara surname: Bals fullname: Bals, Sara organization: EMAT, University of Antwerp, Groenenborgerlaan 171, 2020 Antwerp (Belgium) – sequence: 10 givenname: Gustaaf surname: Van Tendeloo fullname: Van Tendeloo, Gustaaf organization: EMAT, University of Antwerp, Groenenborgerlaan 171, 2020 Antwerp (Belgium) – sequence: 11 givenname: Johan A. surname: Martens fullname: Martens, Johan A. organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 12 givenname: Christine E. A. surname: Kirschhock fullname: Kirschhock, Christine E. A. organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 13 givenname: Pierre A. surname: Jacobs fullname: Jacobs, Pierre A. organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium) – sequence: 14 givenname: Paolo P. surname: Pescarmona fullname: Pescarmona, Paolo P. email: paolo.pescarmona@biw.kuleuven.be organization: Centre for Surface Chemistry and Catalysis, University of Leuven, Kasteelpark Arenberg 23, Heverlee, 3001 (Belgium)
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Copyright	Copyright © 2014 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. Copyright © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
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Keywords	gallium oxide epoxidation heterogeneous catalysis nanorods hydrogen peroxide
Language	English
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Notes	Prodex ArticleID:ANIE201308384 ERC - No. 24691; No. 335078 This work was supported by START1, Methusalem, Prodex, IAP-PAI, and the ERC (grant number 24691-COUNTATOMS and grant number 335078-COLOURATOM) projects. The authors acknowledge Dr. K. Houthoofd, G. Vanbutsele, Dr. C. Klaysom, Prof. J. W. Seo, Dr. T. Korányi, and Prof. K. Binnemans for their support in the characterizations, and Dr. C. Özdilek for useful scientific discussions. Methusalem IAP-PAI istex:C2D7C264D44005C65DC00CABB3FD88B2EB6B9262 ark:/67375/WNG-51VWBCRP-V START1 This work was supported by START1, Methusalem, Prodex, IAP‐PAI, and the ERC (grant number 24691—COUNTATOMS and grant number 335078—COLOURATOM) projects. The authors acknowledge Dr. K. Houthoofd, G. Vanbutsele, Dr. C. Klaysom, Prof. J. W. Seo, Dr. T. Korányi, and Prof. K. Binnemans for their support in the characterizations, and Dr. C. Özdilek for useful scientific discussions. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23
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Snippet	Gallium oxide nanorods with unprecedented small dimensions (20–80 nm length and 3–5 nm width) were prepared using a novel, template‐free synthesis method. This... Gallium oxide nanorods with unprecedented small dimensions (20-80 nm length and 3-5 nm width) were prepared using a novel, template-free synthesis method. This... Gallium oxide nanorods with unprecedented small dimensions (20-80nm length and 3-5nm width) were prepared using a novel, template-free synthesis method. This...
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SubjectTerms	Alkenes Catalysts Epoxidation Gallium gallium oxide Gallium oxides heterogeneous catalysis Hydrogen peroxide Nanorods Nanostructure Physicochemical properties R&D Research & development Specific surface Synthesis
Title	Gallium Oxide Nanorods: Novel, Template-Free Synthesis and High Catalytic Activity in Epoxidation Reactions
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