Palladium-Catalyzed Heck Cross-Coupling Reactions in Water: A Comprehensive Review

Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and i...

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Published in:	Catalysis letters Vol. 148; no. 2; pp. 489 - 511
Main Authors:	Christoffel, Fadri, Ward, Thomas R.
Format:	Journal Article
Language:	English
Published:	New York Springer US 01.02.2018 Springer Springer Nature B.V
Subjects:	Aqueous environments Aqueous solutions Biocompatibility Catalysis Catalysts Chemical reactions Chemistry Chemistry and Materials Science Cross coupling Industrial Chemistry/Chemical Engineering Nanoparticles Organic chemistry Organometallic Chemistry Palladium Palladium catalysts Perspective Physical Chemistry Substitution reactions Heck–Mizoroki reaction Aqueous catalysis Palladium Green chemistry Cross-coupling
ISSN:	1011-372X, 1572-879X
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Abstract	Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and implement bio-compatible protocols. Among different palladium cross-coupling reactions, the Heck reaction turned out to be the most challenging in an aqueous environment. This led to various original developments in catalyst design. This review summarizes the different approaches pursued to perform Heck reactions in neat water as well as aqueous mixtures. Both, homogeneous and immobilized catalysts, including nanoparticles are presented herein. Graphical Abstract
AbstractList	Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and implement bio-compatible protocols. Among different palladium cross-coupling reactions, the Heck reaction turned out to be the most challenging in an aqueous environment. This led to various original developments in catalyst design. This review summarizes the different approaches pursued to perform Heck reactions in neat water as well as aqueous mixtures. Both, homogeneous and immobilized catalysts, including nanoparticles are presented herein. Graphical Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and implement bio-compatible protocols. Among different palladium cross-coupling reactions, the Heck reaction turned out to be the most challenging in an aqueous environment. This led to various original developments in catalyst design. This review summarizes the different approaches pursued to perform Heck reactions in neat water as well as aqueous mixtures. Both, homogeneous and immobilized catalysts, including nanoparticles are presented herein. Graphical Abstract Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and implement bio-compatible protocols. Among different palladium cross-coupling reactions, the Heck reaction turned out to be the most challenging in an aqueous environment. This led to various original developments in catalyst design. This review summarizes the different approaches pursued to perform Heck reactions in neat water as well as aqueous mixtures. Both, homogeneous and immobilized catalysts, including nanoparticles are presented herein.Graphical Abstract Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these reactions to aqueous media, not only for the purpose of environmental conservation but also to expand the scope, increase the efficiency and implement bio-compatible protocols. Among different palladium cross-coupling reactions, the Heck reaction turned out to be the most challenging in an aqueous environment. This led to various original developments in catalyst design. This review summarizes the different approaches pursued to perform Heck reactions in neat water as well as aqueous mixtures. Both, homogeneous and immobilized catalysts, including nanoparticles are presented herein.
Audience	Academic
Author	Christoffel, Fadri Ward, Thomas R.
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Snippet	Palladium-catalyzed cross-coupling reactions have emerged as one of the most versatile tools in organic chemistry. Extensive efforts were made to adapt these...
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SubjectTerms	Aqueous environments Aqueous solutions Biocompatibility Catalysis Catalysts Chemical reactions Chemistry Chemistry and Materials Science Cross coupling Industrial Chemistry/Chemical Engineering Nanoparticles Organic chemistry Organometallic Chemistry Palladium Palladium catalysts Perspective Physical Chemistry Substitution reactions
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Title	Palladium-Catalyzed Heck Cross-Coupling Reactions in Water: A Comprehensive Review
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