Microstructure Change of Nanosilica-Cement Composites Partially Exposed to Sulfate Attack
The deterioration of cement composites containing nanosilica partially exposed to sulfate attack was studied, and the microstructure change of the composites was analysed by a scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The results showed tha...
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| Published in: | International journal of concrete structures and materials Vol. 14; no. 3; pp. 473 - 483 |
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| Main Authors: | , , , , |
| Format: | Journal Article |
| Language: | English |
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Singapore
한국콘크리트학회
01.12.2020
Springer Singapore Springer Springer Nature B.V SpringerOpen |
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| ISSN: | 1976-0485, 2234-1315 |
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| Abstract | The deterioration of cement composites containing nanosilica partially exposed to sulfate attack was studied, and the microstructure change of the composites was analysed by a scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The results showed that nanosilica–cement composites had better sulfate resistance compared to plain cement composite under partial exposure to sulfate attack, and their sulfate resistance increased as the nanosilica content increased (in the range of 0 to 5 wt% replacing cement by weight). The main sulfate products were gypsum and ettringite within the surface and inner parts, respectively in both the immersed and evaporation portions of the nanosilica–cement composites, which was consistent with the plain cement composite. Thus, the incorporation of nanosilica did not change the distribution characteristics of the sulfate products within the composites partially exposed to sulfate attack. However, the addition of nanosilica reduced the amount of sulfate products in both the immersed and evaporation portions, and their amount decreased with the increase of nanosilica content. The evaporation portions of the composites suffered chemical sulfate attack rather than sulfate salt crystallization. Nanosilica–cement composites could be applied in real partial exposure environments containing sulfate ions. |
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| AbstractList | The deterioration of cement composites containing nanosilica partially exposed to sulfate attack was studied, and the microstructure change of the composites was analysed by a scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The results showed that nanosilica–cement composites had better sulfate resistance compared to plain cement composite under partial exposure to sulfate attack, and their sulfate resistance increased as the nanosilica content increased (in the range of 0 to 5 wt% replacing cement by weight). The main sulfate products were gypsum and ettringite within the surface and inner parts, respectively in both the immersed and evaporation portions of the nanosilica–cement composites, which was consistent with the plain cement composite. Thus, the incorporation of nanosilica did not change the distribution characteristics of the sulfate products within the composites partially exposed to sulfate attack. However, the addition of nanosilica reduced the amount of sulfate products in both the immersed and evaporation portions, and their amount decreased with the increase of nanosilica content. The evaporation portions of the composites suffered chemical sulfate attack rather than sulfate salt crystallization. Nanosilica–cement composites could be applied in real partial exposure environments containing sulfate ions. The deterioration of cement composites containing nanosilica partially exposed to sulfate attack was studied, and the microstructure change of the composites was analysed by a scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The results showed that nanosilica–cement composites had better sulfate resistance compared to plain cement composite under partial exposure to sulfate attack, and their sulfate resist-ance increased as the nanosilica content increased (in the range of 0 to 5 wt% replacing cement by weight). The main sulfate products were gypsum and ettringite within the surface and inner parts, respectively in both the immersed and evaporation portions of the nanosilica–cement composites, which was consistent with the plain cement composite. Thus, the incorporation of nanosilica did not change the distribution characteristics of the sulfate products withinthe composites partially exposed to sulfate attack. However, the addition of nanosilica reduced the amount of sulfate products in both the immersed and evaporation portions, and their amount decreased with the increase of nanosilica content. The evaporation portions of the composites suffered chemical sulfate attack rather than sulfate salt crystalliza-tion. Nanosilica–cement composites could be applied in real partial exposure environments containing sulfate ions. KCI Citation Count: 0 Abstract The deterioration of cement composites containing nanosilica partially exposed to sulfate attack was studied, and the microstructure change of the composites was analysed by a scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD). The results showed that nanosilica–cement composites had better sulfate resistance compared to plain cement composite under partial exposure to sulfate attack, and their sulfate resistance increased as the nanosilica content increased (in the range of 0 to 5 wt% replacing cement by weight). The main sulfate products were gypsum and ettringite within the surface and inner parts, respectively in both the immersed and evaporation portions of the nanosilica–cement composites, which was consistent with the plain cement composite. Thus, the incorporation of nanosilica did not change the distribution characteristics of the sulfate products within the composites partially exposed to sulfate attack. However, the addition of nanosilica reduced the amount of sulfate products in both the immersed and evaporation portions, and their amount decreased with the increase of nanosilica content. The evaporation portions of the composites suffered chemical sulfate attack rather than sulfate salt crystallization. Nanosilica–cement composites could be applied in real partial exposure environments containing sulfate ions. |
| ArticleNumber | 27 |
| Audience | Academic |
| Author | Liang Zhao Qian Huang Chenggong Zhao Dongsheng Liu Chaoqiang Wang |
| Author_xml | – sequence: 1 givenname: Qian orcidid: 0000-0003-0588-7459 surname: Huang fullname: Huang, Qian organization: School of Civil and Architectural Engineering, Yangtze Normal University – sequence: 2 givenname: Liang surname: Zhao fullname: Zhao, Liang email: zhaoliang@yznu.edu.cn organization: School of Civil and Architectural Engineering, Yangtze Normal University – sequence: 3 givenname: Chenggong surname: Zhao fullname: Zhao, Chenggong organization: School of Civil and Architectural Engineering, Yangtze Normal University – sequence: 4 givenname: Dongsheng surname: Liu fullname: Liu, Dongsheng organization: Green Intelligence Environment School, Yangtze Normal University – sequence: 5 givenname: Chaoqiang surname: Wang fullname: Wang, Chaoqiang organization: Chongqing Fuling Environment Protection Center for Shale Gas Technology & Development |
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| Cites_doi | 10.1016/j.conbuildmat.2019.05.145 10.1016/j.cemconcomp.2019.01.007 10.1016/j.conbuildmat.2011.03.036 10.1016/j.compositesb.2011.12.015 10.1016/j.cemconres.2018.01.018 10.1016/j.conbuildmat.2015.07.001 10.1016/j.conbuildmat.2019.06.219 10.1061/(ASCE)0899-1561(2003)15:4(305) 10.1016/j.jclepro.2018.08.303 10.1016/j.conbuildmat.2011.08.071 10.1016/S0008-8846(02)00914-6 10.1016/j.cemconcomp.2018.10.008 10.1016/j.conbuildmat.2014.12.074 10.1016/j.conbuildmat.2015.03.006 10.1016/j.conbuildmat.2014.10.014 10.1016/j.jnucmat.2011.09.029 10.1016/j.cemconres.2010.04.004 10.1016/j.conbuildmat.2013.07.088 10.1016/j.cemconres.2018.05.016 10.1016/j.conbuildmat.2019.01.208 10.1016/j.conbuildmat.2018.12.100 10.1007/BF02823370 10.1016/j.conbuildmat.2014.04.063 10.1016/j.cemconres.2005.04.006 10.1016/j.conbuildmat.2019.08.029 10.1016/j.conbuildmat.2012.06.044 10.1016/j.conbuildmat.2019.06.173 10.1016/j.cemconcomp.2010.10.010 |
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| SubjectTerms | Building Materials Cement cement composites Composite materials Crystallization Diffraction Engineering Ettringite Evaporation Exposure Gypsum Microstructure nanosilica partial exposure Solid Mechanics Structural Materials sulfate attack Sulfate resistance Sulfates X-rays 토목공학 |
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| Title | Microstructure Change of Nanosilica-Cement Composites Partially Exposed to Sulfate Attack |
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