Fast synthesis of TiNi by mechanical alloying and its hydrogenation properties
Mechanical alloying is widely used for the synthesis of hydrogen storage materials. However, amorphization and contamination triggered by long-time milling are serious drawbacks for obtaining efficient hydrogen storage. In this work, short-time ball milling synthesis is explored for a representative...
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| Veröffentlicht in: | International Journal of Hydrogen Energy Jg. 44; H. 21; S. 10770 - 10776 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Elsevier Ltd
23.04.2019
Elsevier BV Elsevier |
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| ISSN: | 0360-3199, 1879-3487 |
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| Abstract | Mechanical alloying is widely used for the synthesis of hydrogen storage materials. However, amorphization and contamination triggered by long-time milling are serious drawbacks for obtaining efficient hydrogen storage. In this work, short-time ball milling synthesis is explored for a representative hydride forming compound: TiNi. Through structural, morphological and chemical characterizations, we evidence that formation of TiNi is complete in only 20 min with minor Fe contamination (0.2 wt%). Cross-sectional analysis of powder stuck on milling balls reveals that alloy formation occurs through the interdiffusion between thin layers of co-laminated pure elements. Hydrogenation thermodynamics and kinetics of short-time mechanically alloyed TiNi are similar to those of coarse-grained compounds obtained by classical high-temperature melting. Mechanical alloying is a suitable method for fast and energy-efficient synthesis of intermetallic compounds such as TiNi.
•TiNi phase synthesized in only 20 min of mechanical alloying.•TiNi formation mechanism visualized by scanning electron microscopy.•Mechanically alloyed TiNi has a high hydrogen capacity and fast absorption kinetics.•Mechanical alloying is an energy-efficient method for TiNi synthesis. |
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| AbstractList | Mechanical alloying is widely used for the synthesis of hydrogen storage materials. However, amorphization and contamination triggered by long-time milling are serious drawbacks for obtaining efficient hydrogen storage. In this work, short-time ball milling synthesis is explored for a representative hydride forming compound: TiNi. Through structural, morphological and chemical characterizations, we evidence that formation of TiNi is complete in only 20 min with minor Fe contamination (0.2 wt%). Cross-sectional analysis of powder stuck on milling balls reveals that alloy formation occurs through the interdiffusion between thin layers of co-laminated pure elements. Hydrogenation thermodynamics and kinetics of short-time mechanically alloyed TiNi are similar to those of coarse-grained compounds obtained by classical high-temperature melting. Mechanical alloying is a suitable method for fast and energy-efficient synthesis of intermetallic compounds such as TiNi. Mechanical alloying is widely used for the synthesis of hydrogen storage materials. However, amorphization and contamination triggered by long-time milling are serious drawbacks for obtaining efficient hydrogen storage. In this work, short-time ball milling synthesis is explored for a representative hydride forming compound: TiNi. Through structural, morphological and chemical characterizations, we evidence that formation of TiNi is complete in only 20 min with minor Fe contamination (0.2 wt%). Cross-sectional analysis of powder stuck on milling balls reveals that alloy formation occurs through the interdiffusion between thin layers of co-laminated pure elements. Hydrogenation thermodynamics and kinetics of short-time mechanically alloyed TiNi are similar to those of coarse-grained compounds obtained by classical high-temperature melting. Mechanical alloying is a suitable method for fast and energy-efficient synthesis of intermetallic compounds such as TiNi. •TiNi phase synthesized in only 20 min of mechanical alloying.•TiNi formation mechanism visualized by scanning electron microscopy.•Mechanically alloyed TiNi has a high hydrogen capacity and fast absorption kinetics.•Mechanical alloying is an energy-efficient method for TiNi synthesis. |
| Author | Cuevas, Fermin Nobuki, Tohru Joubert, Jean-Marc Crivello, Jean-Claude |
| Author_xml | – sequence: 1 givenname: Tohru surname: Nobuki fullname: Nobuki, Tohru email: nobuki@hiro.kindai.ac.jp organization: Université Paris Est, ICMPE (UMR 7182), CNRS, UPEC, F-94320 Thiais, France – sequence: 2 givenname: Jean-Claude surname: Crivello fullname: Crivello, Jean-Claude organization: Université Paris Est, ICMPE (UMR 7182), CNRS, UPEC, F-94320 Thiais, France – sequence: 3 givenname: Fermin orcidid: 0000-0002-9055-5880 surname: Cuevas fullname: Cuevas, Fermin organization: Université Paris Est, ICMPE (UMR 7182), CNRS, UPEC, F-94320 Thiais, France – sequence: 4 givenname: Jean-Marc surname: Joubert fullname: Joubert, Jean-Marc organization: Université Paris Est, ICMPE (UMR 7182), CNRS, UPEC, F-94320 Thiais, France |
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| Cites_doi | 10.1016/0925-8388(95)02054-3 10.1002/1527-2648(200111)3:11<837::AID-ADEM837>3.0.CO;2-0 10.1038/scientificamerican0576-40 10.1016/S0925-8388(01)00929-X 10.1039/f19797500561 10.1016/0925-8388(93)90582-8 10.1007/s10853-006-0312-4 10.1088/0953-8984/1/14/003 10.1016/S0925-8388(96)02985-4 10.1016/j.jallcom.2004.07.026 10.1016/j.ijhydene.2008.07.056 10.1016/S0925-8388(01)01508-0 10.1016/j.pmatsci.2012.10.001 10.1016/j.pmatsci.2012.07.001 10.1016/j.jpowsour.2015.01.135 10.1016/j.ijhydene.2009.07.017 10.1016/j.matchemphys.2013.05.021 10.1016/0921-4526(93)90108-I 10.1016/j.msea.2009.04.015 10.2464/jilm.38.165 10.1016/j.jpowsour.2014.04.114 10.1016/S0966-9795(98)00070-3 10.1016/j.electacta.2008.11.024 10.1016/S0079-6425(99)00010-9 10.1016/j.ensm.2016.11.008 10.1016/j.actamat.2018.06.011 10.1016/j.ijhydene.2011.03.092 |
| ContentType | Journal Article |
| Contributor | CUEVAS, Fermin Institut de Chimie et des Matériaux Paris-Est (ICMPE) ; Institut de Chimie du CNRS (INC)-Université Paris-Est Créteil Val-de-Marne - Paris 12 (UPEC UP12)-Centre National de la Recherche Scientifique (CNRS) Institut de Chimie et des Matériaux Paris-Est (ICMPE) ; Institut de Chimie - CNRS Chimie (INC-CNRS)-Université Paris-Est Créteil Val-de-Marne - Paris 12 (UPEC UP12)-Centre National de la Recherche Scientifique (CNRS) Kindai University |
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| Copyright | 2019 The Author(s) Distributed under a Creative Commons Attribution 4.0 International License |
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| Issue | 21 |
| Keywords | Mechanical alloying Hydrogen storage TiNi |
| Language | English |
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| Title | Fast synthesis of TiNi by mechanical alloying and its hydrogenation properties |
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