Hydrothermal synthesis of a concentrated and stable dispersion of TiO2 nanoparticles

► Two-step, low temperature hydrothermal method. ► Deagglomeration and stabilization of 6nm nanoseeds via hydrothermal treatment. ► Stable dispersion of anatase TiO2 nanoparticles with a zeta potential of −51mV and content of 10wt.%. ► Attractive as coating solution for the deposition of different m...

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Vydáno v:	Chemical engineering journal (Lausanne, Switzerland : 1996) Ročník 223; s. 135 - 144
Hlavní autoři:	Souvereyns, B., Elen, K., De Dobbelaere, C., Kelchtermans, A., Peys, N., D’Haen, J., Mertens, M., Mullens, S., Van den Rul, H., Meynen, V., Cool, P., Hardy, A., Van Bael, M.K.
Médium:	Journal Article
Jazyk:	angličtina
Vydáno:	Elsevier B.V 01.05.2013
Témata:	Agglomeration Anatase Aqueous dispersion chemical engineering Crystal structure Dispersions hot water treatment Hydrothermal dispersion Hydrothermal treatment Nanoparticles Raman spectroscopy Stability Synthesis temperature TiO2 Titanium dioxide transmission electron microscopy viscosity X-ray diffraction zeta potential Hydrothermal dispersion Anatase Aqueous dispersion TiO2
ISSN:	1385-8947, 1873-3212
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Abstract	► Two-step, low temperature hydrothermal method. ► Deagglomeration and stabilization of 6nm nanoseeds via hydrothermal treatment. ► Stable dispersion of anatase TiO2 nanoparticles with a zeta potential of −51mV and content of 10wt.%. ► Attractive as coating solution for the deposition of different morphologies of TiO2. A low temperature method for the preparation of an aqueous dispersion of 10wt.% of TiO2 nanoparticles with prolonged stability is presented. This stable, aqueous dispersion is obtained by a two-step, hydrothermal synthesis method using a maximum temperature of 130°C. The hydrothermal treatment of pre-synthesized crystalline nanoparticles results in a colloidal dispersion with minimal particle agglomeration due to the combination of surface modification, pH adjustment and optimized hydrothermal conditions. The presented procedure can be regarded as an alternative and improved method for the dispersion of TiO2 pre-synthesized nanoparticles in an aqueous medium. The stability (sedimentation and particle agglomeration) of the dispersion is investigated by means of zeta potential measurements, evaluation of viscosity in function of time and interaction potential calculations. Transmission Electron Microscopy, X-ray Diffraction and Raman Spectroscopy are used to characterize the structural and chemical features of the TiO2 nanoparticles. The crystalline nanoparticles in dispersion have dimensions<10nm and contain 80% anatase and 20% brookite, according to quantitative XRD analysis. Additionally, the hydrothermal treatment not only stabilized the particles but also increased the crystallinity of the particles in dispersion as a supplemental advantage. Experiments show that this dispersion can be used in combination with various deposition techniques to obtain films with different morphologies.
AbstractList	A low temperature method for the preparation of an aqueous dispersion of 10wt.% of TiO₂ nanoparticles with prolonged stability is presented. This stable, aqueous dispersion is obtained by a two-step, hydrothermal synthesis method using a maximum temperature of 130°C. The hydrothermal treatment of pre-synthesized crystalline nanoparticles results in a colloidal dispersion with minimal particle agglomeration due to the combination of surface modification, pH adjustment and optimized hydrothermal conditions. The presented procedure can be regarded as an alternative and improved method for the dispersion of TiO₂ pre-synthesized nanoparticles in an aqueous medium. The stability (sedimentation and particle agglomeration) of the dispersion is investigated by means of zeta potential measurements, evaluation of viscosity in function of time and interaction potential calculations. Transmission Electron Microscopy, X-ray Diffraction and Raman Spectroscopy are used to characterize the structural and chemical features of the TiO₂ nanoparticles. The crystalline nanoparticles in dispersion have dimensions<10nm and contain 80% anatase and 20% brookite, according to quantitative XRD analysis. Additionally, the hydrothermal treatment not only stabilized the particles but also increased the crystallinity of the particles in dispersion as a supplemental advantage. Experiments show that this dispersion can be used in combination with various deposition techniques to obtain films with different morphologies. ► Two-step, low temperature hydrothermal method. ► Deagglomeration and stabilization of 6nm nanoseeds via hydrothermal treatment. ► Stable dispersion of anatase TiO2 nanoparticles with a zeta potential of −51mV and content of 10wt.%. ► Attractive as coating solution for the deposition of different morphologies of TiO2. A low temperature method for the preparation of an aqueous dispersion of 10wt.% of TiO2 nanoparticles with prolonged stability is presented. This stable, aqueous dispersion is obtained by a two-step, hydrothermal synthesis method using a maximum temperature of 130°C. The hydrothermal treatment of pre-synthesized crystalline nanoparticles results in a colloidal dispersion with minimal particle agglomeration due to the combination of surface modification, pH adjustment and optimized hydrothermal conditions. The presented procedure can be regarded as an alternative and improved method for the dispersion of TiO2 pre-synthesized nanoparticles in an aqueous medium. The stability (sedimentation and particle agglomeration) of the dispersion is investigated by means of zeta potential measurements, evaluation of viscosity in function of time and interaction potential calculations. Transmission Electron Microscopy, X-ray Diffraction and Raman Spectroscopy are used to characterize the structural and chemical features of the TiO2 nanoparticles. The crystalline nanoparticles in dispersion have dimensions<10nm and contain 80% anatase and 20% brookite, according to quantitative XRD analysis. Additionally, the hydrothermal treatment not only stabilized the particles but also increased the crystallinity of the particles in dispersion as a supplemental advantage. Experiments show that this dispersion can be used in combination with various deposition techniques to obtain films with different morphologies. A low temperature method for the preparation of an aqueous dispersion of 10 wt.% of TiO2 nanoparticles with prolonged stability is presented. This stable, aqueous dispersion is obtained by a two-step, hydrothermal synthesis method using a maximum temperature of 130 degree C. The hydrothermal treatment of pre-synthesized crystalline nanoparticles results in a colloidal dispersion with minimal particle agglomeration due to the combination of surface modification, pH adjustment and optimized hydrothermal conditions. The presented procedure can be regarded as an alternative and improved method for the dispersion of TiO2 pre-synthesized nanoparticles in an aqueous medium. The stability (sedimentation and particle agglomeration) of the dispersion is investigated by means of zeta potential measurements, evaluation of viscosity in function of time and interaction potential calculations. Transmission Electron Microscopy, X-ray Diffraction and Raman Spectroscopy are used to characterize the structural and chemical features of the TiO2 nanoparticles. The crystalline nanoparticles in dispersion have dimensions <10 nm and contain 80% anatase and 20% brookite, according to quantitative XRD analysis. Additionally, the hydrothermal treatment not only stabilized the particles but also increased the crystallinity of the particles in dispersion as a supplemental advantage. Experiments show that this dispersion can be used in combination with various deposition techniques to obtain films with different morphologies.
Author	Kelchtermans, A. Elen, K. Cool, P. De Dobbelaere, C. Meynen, V. Souvereyns, B. D’Haen, J. Peys, N. Hardy, A. Van Bael, M.K. Mullens, S. Van den Rul, H. Mertens, M.
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Cites_doi	10.1016/j.jeurceramsoc.2007.02.206 10.1021/cm990180f 10.1016/j.apcata.2007.02.010 10.1557/JMR.1998.0363 10.1002/pen.10373 10.1006/jcis.1996.0444 10.1016/S0040-6090(01)01509-7 10.1021/es802628n 10.1021/cm00052a010 10.1002/jrs.1250260110 10.1016/j.jcis.2010.04.045 10.1016/j.jeurceramsoc.2008.02.017 10.1021/la048898j 10.1016/0001-8686(94)00233-3 10.1002/adma.200802603 10.1006/jcat.2001.3316 10.1016/S0167-577X(00)00320-7 10.1016/j.jcis.2005.09.044 10.1007/s12598-017-0990-x 10.1016/j.jcis.2006.07.003 10.1021/cr00035a013 10.1111/j.1151-2916.2003.tb03608.x 10.1021/es060847g 10.1016/S0001-8686(97)00003-1 10.1016/S0022-0248(02)01938-3 10.1016/j.crci.2009.09.012 10.1016/j.jcis.2006.12.010 10.1016/S0040-6090(00)00862-2 10.1111/j.1151-2916.2000.tb01394.x 10.1089/ees.2007.24.85 10.1021/jp000499j 10.1016/j.surfcoat.2009.09.041 10.1021/es980923i 10.1111/j.1151-2916.1997.tb03245.x 10.1111/j.1151-2916.1999.tb01855.x 10.1016/S0928-4931(01)00274-0 10.1007/s10971-007-1645-4 10.1038/238037a0 10.1016/S0955-2219(02)00194-2 10.1016/j.jeurceramsoc.2011.01.026 10.1038/353737a0 10.1039/tf9666201638 10.1016/0921-5093(95)09785-6 10.1002/pip.481 10.1016/0927-7757(95)03353-X 10.1007/s10971-006-0123-8 10.1023/B:JSST.0000047984.60654.a1 10.3866/PKU.WHXB20050301 10.1080/01932691003756738 10.1111/j.1151-2916.1992.tb04426.x
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References	Cheng, Ma, Zhao, Qi (b0085) 1995; 7 Hu, Tsai, Huang (b0270) 2003; 23 Li, Hou, Xu, Wu, Sun (b0100) 2005; 21 Zhang, Yu, Li, Yang, Wang, Chen (b0170) 2008; 37 Jolivet, Cassaignon, Chanéac, Chiche, Tronc (b0290) 2008; 46 French, Jacobson, Kim, Isley, Penn, Baveye (b0140) 2009; 43 Gupta, Jain, Mittal, Mathur, Sikarwar (b0010) 2007; 309 Xia, Whitesides (b0310) 1998; 28 Vicent, Sanchez, Santacruz, Moreno (b0150) 2011; 31 Linsebigler, Lu, Yates (b0025) 1995; 95 Zhang, Banfield (b0105) 2000; 104 Kim, Kwak (b0040) 2007; 323 Richard A. Nyquist, C.L.P., M. Anne Leugers, Handbook of infrared and Raman spectra of inorganic compounds and organic salts, 4-volume set, volume 2: infrared and Raman spectral atlas of inorganic compounds and organic salts, Raman spectra, 1997. U. Aschauer, Hamaker 2.1: a colloidal stability toolkit (version 2.1) [computer software] Riman (b0175) 1993 Cullity, Stock (b0215) 2001 Wu, Lin, Zhao, Hidaka, Serpone (b0005) 1999; 33 Abramoff, Magelhaes, Ram (b0220) 2004; 11 Bergstrom, Schilling, Aksay (b0245) 1992; 75 Truijen, Van Bael, Van den Rul, D’Haen, Mullens (b0075) 2006; 41 Hotza, Greil (b0315) 1995; 202 Moret, Zallen, Vijay, Desu (b0275) 2000; 366 Jolivet, Cassaignon, Chanéac, Chiche, Durupthy, Portehault (b0295) 2010; 13 Späth, Sommeling, Van Roosmalen, Smit, Van der Burg, Mahieu, Bakker, Kroon (b0195) 2003; 11 Deiss, Anizan, Hadigui, Wecker (b0200) 1996; 106 Hogg, Healy, Fuerstenau (b0240) 1966; 62 Koelsch, Cassaignon, Guillemoles, Jolivet (b0055) 2002; 403–404 Laboratoire de technologie des poudres, Ecole polytechnique fédérale de Lausanne, Switserland, Princeton University, USA, Retrieved May 2010 Yang, Mei, Ferreira (b0185) 2003; 86 . Guzman, Finnegan, Banfield (b0155) 2006; 40 Jolivet (b0285) 2000 Fazio, Guzman, Colomer, Salomoni, Moreno (b0145) 2008; 28 Bowen, Jenner (b0235) 1995; 56 Kartini, Meredith, Diniz da Costa, Lu (b0210) 2004; 31 Aschauer, Burgos-Montes, Moreno, Bowen (b0225) 2010; 32 G. Baldi, M. Bitossi, and A. Barzanti, Method For the Preparation of Aqueous Dispersions of TiO = Beusen, Van Bael, Van den Rul, D’Haen, Mullens (b0090) 2007; 27 Fujishima, Honda (b0020) 1972 Barbé, Arendse, Comte, Jirousek, Lenzmann, Shklover, Graetzel (b0030) 1997; 80 Israelachvili (b0230) 1991 Zhang, Chan, Porter, Guo (b0280) 1998; 13 Yang, Mei, Ferreira (b0080) 2001; 15 Hoogeveen, Stuart, Fleer (b0160) 1996; 182 Zachariah, Baiju, Shukla, Deepa, James, Warrier (b0065) 2008; 112 Veronovski, Andreozzi, La Mesa, Sfiligoj-Smole (b0135) 2010; 204 in the form of Nanoparticles, and Dispersions Obtainable With This Method, US patent 20080317959, (25.12.08). Wang, Ying (b0070) 1999; 11 Bergström (b0250) 1997; 70 Pbca Zhang, Banfield (b0110) 2007; 11 Hall, Underhill, Torkelson (b0305) 1998; 38 Yang, Mei, Ferreira (b0180) 2000; 83 Chen, Huang, Cheng, Caruso (b0050) 2009; 21 Kim, Park, Jeong, Park (b0095) 1999; 82 G.A. Tompsett, G.A. Bowmaker, R.P. Cooney, J.B. Metson, K.A. Rodgers, J.M. Seakins, The Raman spectrum of brookite, TiO Sharma, Whittingham (b0190) 2001; 48 Liu, Zhou, Bai, Li, Zhang, Zheng, Zhu, Cai (b0015) 2009; 89 O’ Regan, Graetzel (b0035) 1991; 353 French, Jacobson, Kim, Isley, Penn, Baveye (b0120) 2009; 43 Chen, Lee, Yeng, Chiu (b0115) 2003; 247 Li, Lv, Fan, Ma, Li, Wan, Zhao (b0130) 2010; 348 Wahi, Liu, Falkner, Colvin (b0255) 2006; 302 8) J. Raman Spectrosc. 36 (1195) 57 Giammar, Maus, Xie (b0045) 2007; 24 Li, Tripp (b0165) 2004; 20 Yaremko, Tkachenko, Bellmann, Pich (b0125) 2006; 296 Ohno, Sarukawa, Tokieda, Matsumura (b0060) 2001; 203 French (10.1016/j.cej.2013.02.047_b0140) 2009; 43 Cullity (10.1016/j.cej.2013.02.047_b0215) 2001 O’ Regan (10.1016/j.cej.2013.02.047_b0035) 1991; 353 Beusen (10.1016/j.cej.2013.02.047_b0090) 2007; 27 Moret (10.1016/j.cej.2013.02.047_b0275) 2000; 366 Kim (10.1016/j.cej.2013.02.047_b0040) 2007; 323 Hoogeveen (10.1016/j.cej.2013.02.047_b0160) 1996; 182 Aschauer (10.1016/j.cej.2013.02.047_b0225) 2010; 32 Bowen (10.1016/j.cej.2013.02.047_b0235) 1995; 56 Jolivet (10.1016/j.cej.2013.02.047_b0290) 2008; 46 10.1016/j.cej.2013.02.047_b0205 Yang (10.1016/j.cej.2013.02.047_b0185) 2003; 86 Kartini (10.1016/j.cej.2013.02.047_b0210) 2004; 31 Bergström (10.1016/j.cej.2013.02.047_b0250) 1997; 70 Li (10.1016/j.cej.2013.02.047_b0100) 2005; 21 Hotza (10.1016/j.cej.2013.02.047_b0315) 1995; 202 Yang (10.1016/j.cej.2013.02.047_b0080) 2001; 15 Wahi (10.1016/j.cej.2013.02.047_b0255) 2006; 302 Kim (10.1016/j.cej.2013.02.047_b0095) 1999; 82 Hall (10.1016/j.cej.2013.02.047_b0305) 1998; 38 Späth (10.1016/j.cej.2013.02.047_b0195) 2003; 11 Abramoff (10.1016/j.cej.2013.02.047_b0220) 2004; 11 Zhang (10.1016/j.cej.2013.02.047_b0110) 2007; 11 Wu (10.1016/j.cej.2013.02.047_b0005) 1999; 33 Ohno (10.1016/j.cej.2013.02.047_b0060) 2001; 203 Chen (10.1016/j.cej.2013.02.047_b0115) 2003; 247 Koelsch (10.1016/j.cej.2013.02.047_b0055) 2002; 403–404 Giammar (10.1016/j.cej.2013.02.047_b0045) 2007; 24 Xia (10.1016/j.cej.2013.02.047_b0310) 1998; 28 Li (10.1016/j.cej.2013.02.047_b0165) 2004; 20 10.1016/j.cej.2013.02.047_b0265 Jolivet (10.1016/j.cej.2013.02.047_b0285) 2000 Li (10.1016/j.cej.2013.02.047_b0130) 2010; 348 10.1016/j.cej.2013.02.047_b0300 Jolivet (10.1016/j.cej.2013.02.047_b0295) 2010; 13 Sharma (10.1016/j.cej.2013.02.047_b0190) 2001; 48 Zhang (10.1016/j.cej.2013.02.047_b0280) 1998; 13 Barbé (10.1016/j.cej.2013.02.047_b0030) 1997; 80 Truijen (10.1016/j.cej.2013.02.047_b0075) 2006; 41 Zachariah (10.1016/j.cej.2013.02.047_b0065) 2008; 112 Wang (10.1016/j.cej.2013.02.047_b0070) 1999; 11 Vicent (10.1016/j.cej.2013.02.047_b0150) 2011; 31 Gupta (10.1016/j.cej.2013.02.047_b0010) 2007; 309 Yang (10.1016/j.cej.2013.02.047_b0180) 2000; 83 10.1016/j.cej.2013.02.047_b0260 Chen (10.1016/j.cej.2013.02.047_b0050) 2009; 21 Israelachvili (10.1016/j.cej.2013.02.047_b0230) 1991 Bergstrom (10.1016/j.cej.2013.02.047_b0245) 1992; 75 Fujishima (10.1016/j.cej.2013.02.047_b0020) 1972 Deiss (10.1016/j.cej.2013.02.047_b0200) 1996; 106 Hu (10.1016/j.cej.2013.02.047_b0270) 2003; 23 Linsebigler (10.1016/j.cej.2013.02.047_b0025) 1995; 95 Zhang (10.1016/j.cej.2013.02.047_b0105) 2000; 104 Veronovski (10.1016/j.cej.2013.02.047_b0135) 2010; 204 Zhang (10.1016/j.cej.2013.02.047_b0170) 2008; 37 Riman (10.1016/j.cej.2013.02.047_b0175) 1993 Yaremko (10.1016/j.cej.2013.02.047_b0125) 2006; 296 Guzman (10.1016/j.cej.2013.02.047_b0155) 2006; 40 Hogg (10.1016/j.cej.2013.02.047_b0240) 1966; 62 Liu (10.1016/j.cej.2013.02.047_b0015) 2009; 89 French (10.1016/j.cej.2013.02.047_b0120) 2009; 43 Fazio (10.1016/j.cej.2013.02.047_b0145) 2008; 28 Cheng (10.1016/j.cej.2013.02.047_b0085) 1995; 7
References_xml	– reference: Laboratoire de technologie des poudres, Ecole polytechnique fédérale de Lausanne, Switserland, Princeton University, USA, Retrieved May 2010 < – volume: 43 start-page: 1354 year: 2009 ident: b0120 article-title: Influence of ionic strength, pH, and cation valence on aggregation kinetics of titanium dioxide nanoparticles publication-title: Environ. Sci. Technol. – volume: 182 start-page: 133 year: 1996 end-page: 145 ident: b0160 article-title: Polyelectrolyte adsorption on oxides: I. Kinetics and adsorbed amounts publication-title: J. Colloid Interface Sci. – volume: 20 start-page: 10526 year: 2004 end-page: 10533 ident: b0165 article-title: Interaction of sodium polyacrylate adsorbed on TiO publication-title: Langmuir – reference: (Pbca, – volume: 13 start-page: 2602 year: 1998 end-page: 2609 ident: b0280 article-title: Micro-Raman Spectroscopy characterization of nanosized TiO publication-title: J. Mater. Res. – volume: 21 start-page: 229 year: 2005 end-page: 233 ident: b0100 article-title: Preparation and characterization of silica-modified titanium dioxide nanoparticles by co-precipitation method publication-title: Acta Phys.-Chim. Sin. – volume: 86 start-page: 2055 year: 2003 end-page: 2058 ident: b0185 article-title: Hydrothermal synthesis of submicrometer a-alumina from seeded tetraethylammonium hydroxide-peptized aluminum hydroxide publication-title: J. Amer. Ceram. Soc. – volume: 403–404 start-page: 312 year: 2002 end-page: 319 ident: b0055 article-title: Comparison of optical and electrochemical properties of anatase and brookite TiO publication-title: Thin Solid Films – volume: 302 start-page: 530 year: 2006 end-page: 536 ident: b0255 article-title: Solvothermal synthesis and characterization of anatase TiO publication-title: J. Colloid Interface Sci. – volume: 70 start-page: 125 year: 1997 end-page: 169 ident: b0250 article-title: Hamaker constants for inorganic materials publication-title: Adv. Colloid Interface Sci. – volume: 11 start-page: 3113 year: 1999 end-page: 3120 ident: b0070 article-title: Sol−Gel synthesis and hydrothermal processing of anatase and rutile titania nanocrystals publication-title: Chem. Mat. – volume: 7 start-page: 663 year: 1995 end-page: 671 ident: b0085 article-title: Hydrothermal preparation of uniform nanosize rutile and anatase particles publication-title: Chem. Mat. – volume: 202 start-page: 206 year: 1995 end-page: 217 ident: b0315 article-title: Review: aqueous tape casting of ceramic powders publication-title: Mater. Sci. Eng., A – volume: 247 start-page: 363 year: 2003 end-page: 370 ident: b0115 article-title: The effect of calcination temperature on the crystallinity of TiO publication-title: J. Cryst. Growth – year: 1993 ident: b0175 article-title: High performance ceramics: surface chemistry in processing technology – reference: G.A. Tompsett, G.A. Bowmaker, R.P. Cooney, J.B. Metson, K.A. Rodgers, J.M. Seakins, The Raman spectrum of brookite, TiO – reference: G. Baldi, M. Bitossi, and A. Barzanti, Method For the Preparation of Aqueous Dispersions of TiO – volume: 89 start-page: 142 year: 2009 end-page: 148 ident: b0015 article-title: Efficient photochemical water splitting and organic pollutant degradation by highly ordered TiO publication-title: Appl. Catal. B-Environ. – volume: 95 start-page: 735 year: 1995 end-page: 758 ident: b0025 article-title: Photocatalysis on TiO publication-title: Chem. Rev. – volume: 348 start-page: 342 year: 2010 end-page: 347 ident: b0130 article-title: Effect of the agglomeration of TiO publication-title: J. Colloid Interface Sci. – volume: 75 start-page: 3305 year: 1992 end-page: 3314 ident: b0245 article-title: Consolidation behavior of flocculated alumina suspensions publication-title: J. Amer. Ceram. Soc. – volume: 82 start-page: 927 year: 1999 end-page: 932 ident: b0095 article-title: Homogeneous precipitation of TiO publication-title: J. Amer. Cer. Soc. – volume: 24 start-page: 85 year: 2007 end-page: 95 ident: b0045 article-title: Effects of particle size and crystalline phase on lead adsorption to titanium dioxide nanoparticles publication-title: Environ. Eng. Sci. – volume: 23 start-page: 691 year: 2003 end-page: 696 ident: b0270 article-title: Effect of brookite phase in the anatase–rutile transition in titania nanoparticles publication-title: J. Eur. Ceram. Soc. – volume: 80 start-page: 3157 year: 1997 end-page: 3171 ident: b0030 article-title: Nanocrystalline titanium oxide electrodes for photovoltaic applications publication-title: J. Amer. Ceram. Soc. – volume: 366 start-page: 8 year: 2000 end-page: 10 ident: b0275 article-title: Brookite-rich titania films made by pulsed laser deposition publication-title: Thin Solid Films – volume: 13 start-page: 40 year: 2010 end-page: 51 ident: b0295 article-title: Design of metal oxide nanoparticles: control of size, shape, crystalline structure and functionalization by aqueous chemistry publication-title: C. R. Chim. – volume: 31 start-page: 185 year: 2004 end-page: 189 ident: b0210 article-title: A novel route to the synthesis of mesoporous titania with full anatase nanocrystalline publication-title: J. Sol–gel Sci. Technol. – volume: 21 start-page: 2206 year: 2009 end-page: 2210 ident: b0050 article-title: Mesoporous anatase TiO publication-title: Adv. Mater. – volume: 104 start-page: 3481 year: 2000 end-page: 3487 ident: b0105 article-title: Understanding polymorphic phase transformation behavior during growth of nanocrystalline aggregates: insights from TiO publication-title: J. Phys. Chem. B – volume: 204 start-page: 1445 year: 2010 end-page: 1451 ident: b0135 article-title: Stable TiO publication-title: Surf. Coat. Technol. – volume: 56 start-page: 201 year: 1995 end-page: 243 ident: b0235 article-title: Theoretical descriptions of membrane filtration of colloids and fine particles: an assessment and review publication-title: Adv. Colloid Interface Sci. – volume: 48 start-page: 319 year: 2001 end-page: 323 ident: b0190 article-title: The role of tetraethyl ammonium hydroxide on the phase determination and electrical properties of gamma-MnOOH synthesized by hydrothermal publication-title: Mater. Lett. – volume: 37 start-page: 326 year: 2008 end-page: 329 ident: b0170 article-title: The effecting factors of super-dispersion TiO publication-title: Rare Metal Mat. Eng. – volume: 62 start-page: 1638 year: 1966 end-page: 1651 ident: b0240 article-title: Mutual coagulation of colloidal dispersions publication-title: Transact. Faraday Soc. – volume: 11 start-page: 2621 year: 2007 end-page: 2629 ident: b0110 article-title: Polymorphic transformations and particle coarsening in nanocrystalline titania ceramic powders and membranes publication-title: J. Phys. Chem. C – volume: 296 start-page: 565 year: 2006 end-page: 571 ident: b0125 article-title: Redispergation of TiO publication-title: J. Colloid Interface Sci. – volume: 28 start-page: 2171 year: 2008 end-page: 2176 ident: b0145 article-title: Colloidal stability of nanosized titania aqueous suspensions publication-title: J. Eur. Ceram. Soc. – volume: 31 start-page: 1413 year: 2011 end-page: 1419 ident: b0150 article-title: Dispersion of TiO publication-title: J. Eur. Cer. Soc. – year: 1991 ident: b0230 article-title: Intermolecular and Surface Forces – volume: 41 start-page: 43 year: 2006 end-page: 48 ident: b0075 article-title: Synthesis of thin dense titania films via aqueous solution–gel method publication-title: J. Sol–gel Sci. Technol. – volume: 38 year: 1998 ident: b0305 article-title: Spin coating of thin and ultrathin polymer films publication-title: Polym. Eng. Sci. – volume: 323 start-page: 110 year: 2007 end-page: 118 ident: b0040 article-title: The hydrothermal synthesis of mesoporous TiO publication-title: Appl. Catal. A-Gen. – volume: 15 start-page: 183 year: 2001 end-page: 185 ident: b0080 article-title: Hydrothermal synthesis of TiO publication-title: Mater. Sci. Engin. C – volume: 28 start-page: 153 year: 1998 end-page: 184 ident: b0310 article-title: Soft lithography publication-title: Annu. Rev. Mater. Res. – reference: = – volume: 309 start-page: 464 year: 2007 end-page: 469 ident: b0010 article-title: Photochemical degradation of the hazardous dye Safranin-T using TiO publication-title: J. Colloid Interface Sci. – year: 2000 ident: b0285 article-title: Metal Oxide Chemistry and Synthesis: from solution to solid state – reference: U. Aschauer, Hamaker 2.1: a colloidal stability toolkit (version 2.1) [computer software] – reference: in the form of Nanoparticles, and Dispersions Obtainable With This Method, US patent 20080317959, (25.12.08). – volume: 33 start-page: 1379 year: 1999 end-page: 1387 ident: b0005 article-title: TiO publication-title: Environ. Sci. Technol. – year: 2001 ident: b0215 article-title: Elements of X-ray Diffraction – volume: 40 start-page: 7688 year: 2006 end-page: 7693 ident: b0155 article-title: Influence of surface potential on aggregation and transport of titania nanoparticles publication-title: Environ. Sci. Technol. – volume: 11 start-page: 207 year: 2003 end-page: 220 ident: b0195 article-title: Reproducible manufacturing of dye sensitized solar cells on a semi-automated baseline publication-title: Prog. Photovoltaics Res. Appl. – start-page: 37 year: 1972 ident: b0020 article-title: Electrochemical photolysis of water at a semiconductor electrode publication-title: Nature – volume: 83 start-page: 1361 year: 2000 end-page: 1368 ident: b0180 article-title: Hydrothermal synthesis of nanosized titania powder: influence of peptization and peptizing agents on the crystalline phases and phase transitions publication-title: J. Amer. Ceram. Soc. – reference: >. – volume: 112 start-page: 11345 year: 2008 end-page: 11356 ident: b0065 article-title: Synergistic effect in photocatalysis as observed for mixed-phase nanocrystalline titania processed via sol−gel solvent mixing and calcination publication-title: J. Phys. Chem. – volume: 43 start-page: 1354 year: 2009 end-page: 1359 ident: b0140 article-title: Influence of ionic strength, pH, and cation valence on aggregation kinetics of titanium dioxide nanoparticles publication-title: Environ. Sci. Technol. – volume: 46 start-page: 299 year: 2008 end-page: 305 ident: b0290 article-title: Design of oxide nanoparticles by aqueous chemistry publication-title: J. Sol–gel Sci. Technol. – volume: 353 start-page: 737 year: 1991 end-page: 740 ident: b0035 article-title: A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO publication-title: Nature – volume: 106 start-page: 59 year: 1996 end-page: 62 ident: b0200 article-title: Steric stability of TiO publication-title: Colloids Surf. A – volume: 32 start-page: 470 year: 2010 ident: b0225 article-title: Hamaker 2: A toolkit for the calculation of particle interactions and suspension stability and its application to mullite synthesis by colloidal methods publication-title: J. Dispersion Sci. Technol. – volume: 11 start-page: 36 year: 2004 end-page: 42 ident: b0220 article-title: Image processing with Image J publication-title: Biophotonics Int. – reference: Richard A. Nyquist, C.L.P., M. Anne Leugers, Handbook of infrared and Raman spectra of inorganic compounds and organic salts, 4-volume set, volume 2: infrared and Raman spectral atlas of inorganic compounds and organic salts, Raman spectra, 1997. – volume: 27 start-page: 4529 year: 2007 end-page: 4535 ident: b0090 article-title: Preparation of a nanoporous nanocrystalline TiO publication-title: J. Eur. Ceram. Soc. – reference: 8) J. Raman Spectrosc. 36 (1195) 57 – volume: 203 start-page: 82 year: 2001 end-page: 86 ident: b0060 article-title: Morphology of a TiO publication-title: J. Catal. – volume: 27 start-page: 4529 year: 2007 ident: 10.1016/j.cej.2013.02.047_b0090 article-title: Preparation of a nanoporous nanocrystalline TiO2 layer by deposition of hydrothermally synthesized nanoparticles publication-title: J. Eur. Ceram. Soc. doi: 10.1016/j.jeurceramsoc.2007.02.206 – volume: 11 start-page: 3113 issue: 11 year: 1999 ident: 10.1016/j.cej.2013.02.047_b0070 article-title: Sol−Gel synthesis and hydrothermal processing of anatase and rutile titania nanocrystals publication-title: Chem. Mat. doi: 10.1021/cm990180f – volume: 323 start-page: 110 year: 2007 ident: 10.1016/j.cej.2013.02.047_b0040 article-title: The hydrothermal synthesis of mesoporous TiO2 with high crystallinity, thermal stability, large surface area, and enhanced photocatalytic activity publication-title: Appl. Catal. A-Gen. doi: 10.1016/j.apcata.2007.02.010 – volume: 13 start-page: 2602 issue: 9 year: 1998 ident: 10.1016/j.cej.2013.02.047_b0280 article-title: Micro-Raman Spectroscopy characterization of nanosized TiO2 powders prepared by vapor hydrolysis publication-title: J. Mater. Res. doi: 10.1557/JMR.1998.0363 – volume: 38 issue: 12 year: 1998 ident: 10.1016/j.cej.2013.02.047_b0305 article-title: Spin coating of thin and ultrathin polymer films publication-title: Polym. Eng. Sci. doi: 10.1002/pen.10373 – volume: 182 start-page: 133 issue: 1 year: 1996 ident: 10.1016/j.cej.2013.02.047_b0160 article-title: Polyelectrolyte adsorption on oxides: I. Kinetics and adsorbed amounts publication-title: J. Colloid Interface Sci. doi: 10.1006/jcis.1996.0444 – volume: 403–404 start-page: 312 year: 2002 ident: 10.1016/j.cej.2013.02.047_b0055 article-title: Comparison of optical and electrochemical properties of anatase and brookite TiO2 synthesized by the sol–gel method publication-title: Thin Solid Films doi: 10.1016/S0040-6090(01)01509-7 – volume: 43 start-page: 1354 year: 2009 ident: 10.1016/j.cej.2013.02.047_b0120 article-title: Influence of ionic strength, pH, and cation valence on aggregation kinetics of titanium dioxide nanoparticles publication-title: Environ. Sci. Technol. doi: 10.1021/es802628n – volume: 7 start-page: 663 issue: 4 year: 1995 ident: 10.1016/j.cej.2013.02.047_b0085 article-title: Hydrothermal preparation of uniform nanosize rutile and anatase particles publication-title: Chem. Mat. doi: 10.1021/cm00052a010 – ident: 10.1016/j.cej.2013.02.047_b0265 doi: 10.1002/jrs.1250260110 – volume: 348 start-page: 342 year: 2010 ident: 10.1016/j.cej.2013.02.047_b0130 article-title: Effect of the agglomeration of TiO2 nanoparticles on their photocatalytic performance in the aqueous phase publication-title: J. Colloid Interface Sci. doi: 10.1016/j.jcis.2010.04.045 – volume: 28 start-page: 2171 year: 2008 ident: 10.1016/j.cej.2013.02.047_b0145 article-title: Colloidal stability of nanosized titania aqueous suspensions publication-title: J. Eur. Ceram. Soc. doi: 10.1016/j.jeurceramsoc.2008.02.017 – volume: 20 start-page: 10526 issue: 24 year: 2004 ident: 10.1016/j.cej.2013.02.047_b0165 article-title: Interaction of sodium polyacrylate adsorbed on TiO2 with cationic and anionic surfactants publication-title: Langmuir doi: 10.1021/la048898j – year: 2000 ident: 10.1016/j.cej.2013.02.047_b0285 – volume: 56 start-page: 201 year: 1995 ident: 10.1016/j.cej.2013.02.047_b0235 article-title: Theoretical descriptions of membrane filtration of colloids and fine particles: an assessment and review publication-title: Adv. Colloid Interface Sci. doi: 10.1016/0001-8686(94)00233-3 – volume: 21 start-page: 2206 year: 2009 ident: 10.1016/j.cej.2013.02.047_b0050 article-title: Mesoporous anatase TiO2 beads with high surface areas and controllable pore sizes: a superior candidate for high-performance dye-sensitized solar Cells publication-title: Adv. Mater. doi: 10.1002/adma.200802603 – volume: 203 start-page: 82 year: 2001 ident: 10.1016/j.cej.2013.02.047_b0060 article-title: Morphology of a TiO2 photoctalyst (Degussa, P-25) consisting of a anatase and rutile crystalline phases publication-title: J. Catal. doi: 10.1006/jcat.2001.3316 – volume: 48 start-page: 319 year: 2001 ident: 10.1016/j.cej.2013.02.047_b0190 article-title: The role of tetraethyl ammonium hydroxide on the phase determination and electrical properties of gamma-MnOOH synthesized by hydrothermal publication-title: Mater. Lett. doi: 10.1016/S0167-577X(00)00320-7 – volume: 296 start-page: 565 issue: 2 year: 2006 ident: 10.1016/j.cej.2013.02.047_b0125 article-title: Redispergation of TiO2 particles in aqueous solutions publication-title: J. Colloid Interface Sci. doi: 10.1016/j.jcis.2005.09.044 – volume: 37 start-page: 326 year: 2008 ident: 10.1016/j.cej.2013.02.047_b0170 article-title: The effecting factors of super-dispersion TiO2 nanoparticles prepared by sol–emulsion–gel method publication-title: Rare Metal Mat. Eng. doi: 10.1007/s12598-017-0990-x – volume: 302 start-page: 530 year: 2006 ident: 10.1016/j.cej.2013.02.047_b0255 article-title: Solvothermal synthesis and characterization of anatase TiO2 nanocrystals with ultrahigh surface area publication-title: J. Colloid Interface Sci. doi: 10.1016/j.jcis.2006.07.003 – volume: 95 start-page: 735 year: 1995 ident: 10.1016/j.cej.2013.02.047_b0025 article-title: Photocatalysis on TiOn Surfaces: principles, mechanisms, and selected results publication-title: Chem. Rev. doi: 10.1021/cr00035a013 – volume: 86 start-page: 2055 year: 2003 ident: 10.1016/j.cej.2013.02.047_b0185 article-title: Hydrothermal synthesis of submicrometer a-alumina from seeded tetraethylammonium hydroxide-peptized aluminum hydroxide publication-title: J. Amer. Ceram. Soc. doi: 10.1111/j.1151-2916.2003.tb03608.x – volume: 40 start-page: 7688 year: 2006 ident: 10.1016/j.cej.2013.02.047_b0155 article-title: Influence of surface potential on aggregation and transport of titania nanoparticles publication-title: Environ. Sci. Technol. doi: 10.1021/es060847g – volume: 70 start-page: 125 year: 1997 ident: 10.1016/j.cej.2013.02.047_b0250 article-title: Hamaker constants for inorganic materials publication-title: Adv. Colloid Interface Sci. doi: 10.1016/S0001-8686(97)00003-1 – volume: 247 start-page: 363 issue: 3–4 year: 2003 ident: 10.1016/j.cej.2013.02.047_b0115 article-title: The effect of calcination temperature on the crystallinity of TiO2 nanopowders publication-title: J. Cryst. Growth doi: 10.1016/S0022-0248(02)01938-3 – volume: 89 start-page: 142 issue: 1–2 year: 2009 ident: 10.1016/j.cej.2013.02.047_b0015 article-title: Efficient photochemical water splitting and organic pollutant degradation by highly ordered TiO2 nanopore arrays publication-title: Appl. Catal. B-Environ. – volume: 28 start-page: 153 year: 1998 ident: 10.1016/j.cej.2013.02.047_b0310 article-title: Soft lithography publication-title: Annu. Rev. Mater. Res. – volume: 13 start-page: 40 year: 2010 ident: 10.1016/j.cej.2013.02.047_b0295 article-title: Design of metal oxide nanoparticles: control of size, shape, crystalline structure and functionalization by aqueous chemistry publication-title: C. R. Chim. doi: 10.1016/j.crci.2009.09.012 – year: 1993 ident: 10.1016/j.cej.2013.02.047_b0175 article-title: High performance ceramics: surface chemistry in processing technology – year: 2001 ident: 10.1016/j.cej.2013.02.047_b0215 – volume: 309 start-page: 464 issue: 2 year: 2007 ident: 10.1016/j.cej.2013.02.047_b0010 article-title: Photochemical degradation of the hazardous dye Safranin-T using TiO2 catalyst publication-title: J. Colloid Interface Sci. doi: 10.1016/j.jcis.2006.12.010 – volume: 366 start-page: 8 year: 2000 ident: 10.1016/j.cej.2013.02.047_b0275 article-title: Brookite-rich titania films made by pulsed laser deposition publication-title: Thin Solid Films doi: 10.1016/S0040-6090(00)00862-2 – volume: 11 start-page: 36 issue: 7 year: 2004 ident: 10.1016/j.cej.2013.02.047_b0220 article-title: Image processing with Image J publication-title: Biophotonics Int. – volume: 83 start-page: 1361 issue: 6 year: 2000 ident: 10.1016/j.cej.2013.02.047_b0180 article-title: Hydrothermal synthesis of nanosized titania powder: influence of peptization and peptizing agents on the crystalline phases and phase transitions publication-title: J. Amer. Ceram. Soc. doi: 10.1111/j.1151-2916.2000.tb01394.x – ident: 10.1016/j.cej.2013.02.047_b0205 – volume: 24 start-page: 85 issue: 1 year: 2007 ident: 10.1016/j.cej.2013.02.047_b0045 article-title: Effects of particle size and crystalline phase on lead adsorption to titanium dioxide nanoparticles publication-title: Environ. Eng. Sci. doi: 10.1089/ees.2007.24.85 – volume: 104 start-page: 3481 year: 2000 ident: 10.1016/j.cej.2013.02.047_b0105 article-title: Understanding polymorphic phase transformation behavior during growth of nanocrystalline aggregates: insights from TiO2 publication-title: J. Phys. Chem. B doi: 10.1021/jp000499j – volume: 204 start-page: 1445 year: 2010 ident: 10.1016/j.cej.2013.02.047_b0135 article-title: Stable TiO2 dispersions for nanocoating preparation publication-title: Surf. Coat. Technol. doi: 10.1016/j.surfcoat.2009.09.041 – volume: 33 start-page: 1379 issue: 9 year: 1999 ident: 10.1016/j.cej.2013.02.047_b0005 article-title: TiO2-assisted photodegradation of dyes. 9. Photooxidation of a squarylium cyanine dye in aqueous dispersions under visible light irradiation publication-title: Environ. Sci. Technol. doi: 10.1021/es980923i – volume: 80 start-page: 3157 issue: 12 year: 1997 ident: 10.1016/j.cej.2013.02.047_b0030 article-title: Nanocrystalline titanium oxide electrodes for photovoltaic applications publication-title: J. Amer. Ceram. Soc. doi: 10.1111/j.1151-2916.1997.tb03245.x – volume: 82 start-page: 927 issue: 4 year: 1999 ident: 10.1016/j.cej.2013.02.047_b0095 article-title: Homogeneous precipitation of TiO2 ultrafine powders from aqueous TiOCl2 solution publication-title: J. Amer. Cer. Soc. doi: 10.1111/j.1151-2916.1999.tb01855.x – year: 1991 ident: 10.1016/j.cej.2013.02.047_b0230 – volume: 112 start-page: 11345 issue: 30 year: 2008 ident: 10.1016/j.cej.2013.02.047_b0065 article-title: Synergistic effect in photocatalysis as observed for mixed-phase nanocrystalline titania processed via sol−gel solvent mixing and calcination publication-title: J. Phys. Chem. – volume: 15 start-page: 183 year: 2001 ident: 10.1016/j.cej.2013.02.047_b0080 article-title: Hydrothermal synthesis of TiO2 nanopowders from tetraalkylammonium hydroxide peptized sols publication-title: Mater. Sci. Engin. C doi: 10.1016/S0928-4931(01)00274-0 – volume: 46 start-page: 299 year: 2008 ident: 10.1016/j.cej.2013.02.047_b0290 article-title: Design of oxide nanoparticles by aqueous chemistry publication-title: J. Sol–gel Sci. Technol. doi: 10.1007/s10971-007-1645-4 – start-page: 37 year: 1972 ident: 10.1016/j.cej.2013.02.047_b0020 article-title: Electrochemical photolysis of water at a semiconductor electrode publication-title: Nature doi: 10.1038/238037a0 – volume: 23 start-page: 691 year: 2003 ident: 10.1016/j.cej.2013.02.047_b0270 article-title: Effect of brookite phase in the anatase–rutile transition in titania nanoparticles publication-title: J. Eur. Ceram. Soc. doi: 10.1016/S0955-2219(02)00194-2 – volume: 31 start-page: 1413 year: 2011 ident: 10.1016/j.cej.2013.02.047_b0150 article-title: Dispersion of TiO2 nanopowders to obtain homogeneous nanostructured granules by spray-drying publication-title: J. Eur. Cer. Soc. doi: 10.1016/j.jeurceramsoc.2011.01.026 – ident: 10.1016/j.cej.2013.02.047_b0260 – ident: 10.1016/j.cej.2013.02.047_b0300 – volume: 353 start-page: 737 year: 1991 ident: 10.1016/j.cej.2013.02.047_b0035 article-title: A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO2 films publication-title: Nature doi: 10.1038/353737a0 – volume: 62 start-page: 1638 year: 1966 ident: 10.1016/j.cej.2013.02.047_b0240 article-title: Mutual coagulation of colloidal dispersions publication-title: Transact. Faraday Soc. doi: 10.1039/tf9666201638 – volume: 43 start-page: 1354 issue: 5 year: 2009 ident: 10.1016/j.cej.2013.02.047_b0140 article-title: Influence of ionic strength, pH, and cation valence on aggregation kinetics of titanium dioxide nanoparticles publication-title: Environ. Sci. Technol. doi: 10.1021/es802628n – volume: 202 start-page: 206 year: 1995 ident: 10.1016/j.cej.2013.02.047_b0315 article-title: Review: aqueous tape casting of ceramic powders publication-title: Mater. Sci. Eng., A doi: 10.1016/0921-5093(95)09785-6 – volume: 11 start-page: 207 year: 2003 ident: 10.1016/j.cej.2013.02.047_b0195 article-title: Reproducible manufacturing of dye sensitized solar cells on a semi-automated baseline publication-title: Prog. Photovoltaics Res. Appl. doi: 10.1002/pip.481 – volume: 11 start-page: 2621 year: 2007 ident: 10.1016/j.cej.2013.02.047_b0110 article-title: Polymorphic transformations and particle coarsening in nanocrystalline titania ceramic powders and membranes publication-title: J. Phys. Chem. C – volume: 106 start-page: 59 year: 1996 ident: 10.1016/j.cej.2013.02.047_b0200 article-title: Steric stability of TiO2 nanoparticles in aqueous dispersions publication-title: Colloids Surf. A doi: 10.1016/0927-7757(95)03353-X – volume: 41 start-page: 43 year: 2006 ident: 10.1016/j.cej.2013.02.047_b0075 article-title: Synthesis of thin dense titania films via aqueous solution–gel method publication-title: J. Sol–gel Sci. Technol. doi: 10.1007/s10971-006-0123-8 – volume: 31 start-page: 185 year: 2004 ident: 10.1016/j.cej.2013.02.047_b0210 article-title: A novel route to the synthesis of mesoporous titania with full anatase nanocrystalline publication-title: J. Sol–gel Sci. Technol. doi: 10.1023/B:JSST.0000047984.60654.a1 – volume: 21 start-page: 229 issue: 3 year: 2005 ident: 10.1016/j.cej.2013.02.047_b0100 article-title: Preparation and characterization of silica-modified titanium dioxide nanoparticles by co-precipitation method publication-title: Acta Phys.-Chim. Sin. doi: 10.3866/PKU.WHXB20050301 – volume: 32 start-page: 470 issue: 4 year: 2010 ident: 10.1016/j.cej.2013.02.047_b0225 article-title: Hamaker 2: A toolkit for the calculation of particle interactions and suspension stability and its application to mullite synthesis by colloidal methods publication-title: J. Dispersion Sci. Technol. doi: 10.1080/01932691003756738 – volume: 75 start-page: 3305 year: 1992 ident: 10.1016/j.cej.2013.02.047_b0245 article-title: Consolidation behavior of flocculated alumina suspensions publication-title: J. Amer. Ceram. Soc. doi: 10.1111/j.1151-2916.1992.tb04426.x
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Snippet	► Two-step, low temperature hydrothermal method. ► Deagglomeration and stabilization of 6nm nanoseeds via hydrothermal treatment. ► Stable dispersion of... A low temperature method for the preparation of an aqueous dispersion of 10wt.% of TiO₂ nanoparticles with prolonged stability is presented. This stable,... A low temperature method for the preparation of an aqueous dispersion of 10 wt.% of TiO2 nanoparticles with prolonged stability is presented. This stable,...
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SubjectTerms	Agglomeration Anatase Aqueous dispersion chemical engineering Crystal structure Dispersions hot water treatment Hydrothermal dispersion Hydrothermal treatment Nanoparticles Raman spectroscopy Stability Synthesis temperature TiO2 Titanium dioxide transmission electron microscopy viscosity X-ray diffraction zeta potential
Title	Hydrothermal synthesis of a concentrated and stable dispersion of TiO2 nanoparticles
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