Preparation and characterization of fluorophenylboronic acid-functionalized monolithic columns for high affinity capture of cis-diol containing compounds

•Three fluorophenylboronic acid-functionalized monoliths were prepared.•The monoliths exhibited untrahigh boronate affinity toward cis-diol compounds.•The boronate affinity was strongly influenced by spacer arm length.•The monolith with appropriate spacer arm length can bind with cis-diols at pH 6.0...

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Veröffentlicht in:	Journal of Chromatography A Jg. 1305; S. 123 - 130
Hauptverfasser:	Li, Qianjin, Lü, Chenchen, Liu, Zhen
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	Amsterdam Elsevier B.V 30.08.2013 Elsevier
Schlagworte:	acids Affinity Analytical chemistry Binding binding capacity Biological and medical sciences Boronate affinity Boronic Acids - chemistry Capture Chemistry Chromatographic methods and physical methods associated with chromatography chromatography Chromatography, Affinity - instrumentation Cis-diol Enrichment Exact sciences and technology Fluorine - chemistry Fluorophenylboronic acid Glycoprotein glycoproteins humans Hydrogen-Ion Concentration Investigative techniques, diagnostic techniques (general aspects) Ligands Medical sciences Microscopy, Electron, Scanning Miscellaneous. Technology molecular weight Monolithic columns monosaccharides Nucleosides Other chromatographic methods Pathology. Cytology. Biochemistry. Spectrometry. Miscellaneous investigative techniques Spacers Urine Cis-diol Fluorophenylboronic acid Boronate affinity Monolithic columns Capture Biological fluid Chemical analysis Chromatographic retention Micellar electrokinetic capillary chromatography Esterases Pyrocatechol Diphenols Chemical enrichment Surface structure Affinity adsorbent Characterization Clinical biology Nucleoside Trace analysis Human Urine Scanning electron microscopy Diol Healthy subject Enzyme Monolithic column Morphology Preparation Hydrolases Boron Organic compounds Pancreatic ribonuclease Boronic acids
ISSN:	0021-9673, 1873-3778, 1873-3778
Online-Zugang:	Volltext
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