PBDEs in environmental samples: Sampling and analysis

► The review describes commonly used analytical procedures for determining PBDE in environmental samples. ► Information on the subsequent stages of analytical procedure (e.g. sample collection, extraction, clean up, etc.) is presented. ► The special attention is paid to the newly developed and promi...

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Bibliographic Details
Published in:	Talanta (Oxford) Vol. 93; pp. 1 - 17
Main Authors:	KROL, Sylwia, ZABIEGALA, Bozena, NAMIESNIK, Jacek
Format:	Journal Article
Language:	English
Published:	Amsterdam Elsevier B.V 15.05.2012 Elsevier
Subjects:	Analytic Sample Preparation Methods Analytical chemistry Animals Applied sciences Biota Bromination Chemical Fractionation Chemistry Chromatographic methods and physical methods associated with chromatography Collection Environment Environmental samples Ethers Exact sciences and technology Extraction Gas chromatographic methods Gas chromatography Global environmental pollution Halogenated Diphenyl Ethers - analysis Halogenated Diphenyl Ethers - chemistry Halogenated Diphenyl Ethers - isolation & purification Humans Mathematical analysis microextraction Microextraction techniques Monitoring Pollution Polybrominated diphenyl ethers Quality assurance quality control Sampling Semivolatile organic compounds PCBs SPE BFR LRMS HRMS PBB SPME Semivolatile organic compounds SPE-DLLME Environmental samples IM MS USAL-DPSE-DLLME TOF PTV-LV DCM MAE SPLE Gas chromatography ASTM HF-LPM PCDD/F ICP-MS LLME QISTMS DLLME MWCNTs-SPME LLE GFF POPs SBSE APCI QFF SVOC ASE PTV SFE QuEChERS HF-LPME GC HPLC MSD HF-MMLLE QA/QC IUAPC USAE PBDEs ECD EIMS Microextraction techniques Polybrominated diphenyl ethers UPLC APPI LC CPE ECNI GPC Microanalysis Review Implementation Cloud point Quality assurance Sample preparation Limitation Hollow fiber Extraction Sampling Monitoring Organic compounds Ether Extraction process Sample Quality control Microextraction Environment Technique Detection
ISSN:	0039-9140, 1873-3573, 1873-3573
Online Access:	Get full text
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Summary:	► The review describes commonly used analytical procedures for determining PBDE in environmental samples. ► Information on the subsequent stages of analytical procedure (e.g. sample collection, extraction, clean up, etc.) is presented. ► The special attention is paid to the newly developed and promising microextraction techniques. ► Authors describe the limitations that may occur during the analysis of highly brominated congeners (e.g. BDE209). The paper reviews the subject literature concerning analytical procedures routinely sed for monitoring polybrominated diphenyl ethers (PBDE) in environmental samples. It describes and summarizes subsequent stages of analytical procedure including sample collection and preparation, extraction, clean-up and final determination. Different approaches with their advantages and limitations are presented. Special attention is drawn to the newly developed, promising extraction techniques, especially: liquid–liquid-microextraction (LLME) with its modifications, cloud point extraction (CPE) and hollow fiber microextraction. The review compares available detection techniques taking into account their usefulness for determining different PBDEs in complex matrix as well as discussing possible limitations that may occur during the analysis. The quality assurance and quality control aspect of analytical procedure is described. Finally special attention is paid to the determination of highly brominated PBDE compounds (e.g. BDE209), which requires implementation of different analytical approach.
Bibliography:	ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 ObjectType-Review-3
ISSN:	0039-9140 1873-3573 1873-3573
DOI:	10.1016/j.talanta.2012.01.048