Sustainable Development of High‐performance Poly(ester‐imine) Biobased Thermosets
The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐perfor...
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| Veröffentlicht in: | Advanced science Jg. 12; H. 26; S. e2503483 - n/a |
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John Wiley & Sons, Inc
01.07.2025
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| Abstract | The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm−3) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications.
Schiff‐based epoxy monomers derived from renewable natural resources are used to design robust structures by cross–linking with bio‐anhydrides. The resulting eco‐friendly, high‐performance thermosets feature two cleavable bonds, offering versatility for various applications. These materials exhibit properties suitable for a wide range of needs, from flexible to rigid structures, ensuring adaptability in demanding environments. |
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| AbstractList | The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm−3) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications. Schiff‐based epoxy monomers derived from renewable natural resources are used to design robust structures by cross–linking with bio‐anhydrides. The resulting eco‐friendly, high‐performance thermosets feature two cleavable bonds, offering versatility for various applications. These materials exhibit properties suitable for a wide range of needs, from flexible to rigid structures, ensuring adaptability in demanding environments. The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco-friendly and high-performance poly(ester-imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross-linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester-imine) thermosets with high performances that exceed those reported in previous studies. The thermo-mechanical investigations show that the novel-designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame-retardant properties without the addition of supplementary additives. Their low-density values (1.05‒1.36 g cm ) and the very low WA% ≈0.09-1.15 % after 24 h make them well-suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester-imine) materials as promising sustainable candidates for a wide range of high-end applications. Abstract The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm−3) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications. The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco-friendly and high-performance poly(ester-imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross-linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester-imine) thermosets with high performances that exceed those reported in previous studies. The thermo-mechanical investigations show that the novel-designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame-retardant properties without the addition of supplementary additives. Their low-density values (1.05‒1.36 g cm-3) and the very low WA% ≈0.09-1.15 % after 24 h make them well-suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester-imine) materials as promising sustainable candidates for a wide range of high-end applications.The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco-friendly and high-performance poly(ester-imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross-linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester-imine) thermosets with high performances that exceed those reported in previous studies. The thermo-mechanical investigations show that the novel-designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame-retardant properties without the addition of supplementary additives. Their low-density values (1.05‒1.36 g cm-3) and the very low WA% ≈0.09-1.15 % after 24 h make them well-suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester-imine) materials as promising sustainable candidates for a wide range of high-end applications. The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm −3 ) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications. The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm−3) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications. Schiff‐based epoxy monomers derived from renewable natural resources are used to design robust structures by cross–linking with bio‐anhydrides. The resulting eco‐friendly, high‐performance thermosets feature two cleavable bonds, offering versatility for various applications. These materials exhibit properties suitable for a wide range of needs, from flexible to rigid structures, ensuring adaptability in demanding environments. The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context, the development of environmentally friendly alternatives becomes crucial. This study investigates the synthesis of eco‐friendly and high‐performance poly(ester‐imine) thermosets by sustainable approaches. Starting with vanillin or syringaldehyde, the synthesis involves the introduction of imine linkages within the epoxy monomer's structure. A new strategy is used through the cross–linking of the designed epoxy monomers using anhydrides, without initiators. This approach conducts to novel poly(ester‐imine) thermosets with high performances that exceed those reported in previous studies. The thermo‐mechanical investigations show that the novel‐designed thermosets have performant properties with storage moduli at room temperature ranging between 0.3‒1.74 GPa and glass transition values between 90 and 170 °C. The Limit Oxygen Index (LOI) in the range of 24‒36%, confirms the excellent flame‐retardant properties without the addition of supplementary additives. Their low‐density values (1.05‒1.36 g cm−3) and the very low WA% ≈0.09–1.15 % after 24 h make them well‐suited for a range of uses where weight and hydrophobicity considerations are critical. The obtained results place these poly(ester‐imine) materials as promising sustainable candidates for a wide range of high‐end applications. |
| Author | Swanson, David D. Cibotaru, Sandu Mija, Alice Dinu, Roxana |
| AuthorAffiliation | 2 Air Force Office of Scientific Research (AFOSR) European Office of Aerospace Research and Development (EOARD) 86 Blenheim Crescent, Ruislip HA4 7HD UK 1 Université Côte d'Azur ICN France |
| AuthorAffiliation_xml | – name: 1 Université Côte d'Azur ICN France – name: 2 Air Force Office of Scientific Research (AFOSR) European Office of Aerospace Research and Development (EOARD) 86 Blenheim Crescent, Ruislip HA4 7HD UK |
| Author_xml | – sequence: 1 givenname: Roxana surname: Dinu fullname: Dinu, Roxana organization: ICN – sequence: 2 givenname: Sandu surname: Cibotaru fullname: Cibotaru, Sandu organization: ICN – sequence: 3 givenname: David D. surname: Swanson fullname: Swanson, David D. organization: Air Force Office of Scientific Research (AFOSR) European Office of Aerospace Research and Development (EOARD) – sequence: 4 givenname: Alice orcidid: 0000-0001-5208-5956 surname: Mija fullname: Mija, Alice email: Alice.Mija@univ-cotedazur.fr organization: ICN |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/40279547$$D View this record in MEDLINE/PubMed |
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| Keywords | Schiff bases high‐performance biobased thermosets novel poly(ester‐imine) |
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| Snippet | The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this context,... Abstract The massive production of materials based on petroleum derivatives and often toxic compounds generates significant environmental pollution. In this... |
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| SubjectTerms | Aldehydes biobased thermosets Bisphenol A Curing Fossil fuels Fourier transforms high‐performance Lignin Mechanical properties novel poly(ester‐imine) Oxidation Renewable resources Schiff bases Sustainable materials |
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| Title | Sustainable Development of High‐performance Poly(ester‐imine) Biobased Thermosets |
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