Microstructure characterization by X-ray tomography and EBSD of porous FeCr produced by liquid metal dealloying

Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a (FeCr)x-Ni1−x precursor, it is possible to get porous FeCr with this technique. While immersing precursors in a molten Mg bath, Ni atoms selectively mig...

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Vydané v:	Materials characterization Ročník 144; s. 166 - 172
Hlavní autori:	Mokhtari, Morgane, Le Bourlot, Christophe, Adrien, Jérome, Bonnin, Anne, Wada, Takeshi, Duchet-Rumeau, Jannick, Kato, Hidemi, Maire, Eric
Médium:	Journal Article
Jazyk:	English
Vydavateľské údaje:	United States Elsevier Inc 01.10.2018 Elsevier
Predmet:	BACKSCATTERING BCC LATTICES CHROMIUM COMPOUNDS Condensed Matter Dealloying EBSD ELECTRON DIFFRACTION FCC LATTICES Instrumentation and Detectors IRON COMPOUNDS LIQUID METALS Materials and structures in mechanics MATERIALS SCIENCE Mechanical engineering Mechanics Mechanics of materials PHASE STUDIES Physics Porous POROUS MATERIALS SOLID SOLUTIONS SOLIDS SURFACES TOMOGRAPHY X-ray tomography X-ray tomography Dealloying EBSD Porous Fe
ISSN:	1044-5803, 1873-4189
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Abstract	Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a (FeCr)x-Ni1−x precursor, it is possible to get porous FeCr with this technique. While immersing precursors in a molten Mg bath, Ni atoms selectively migrate into the Mg bath. After cooling down to room temperature, the resulting microstructure is a bi-continuous structure of FeCr and Mg (with Ni in solid solution). A final etching step removes the Mg solid-state solution phase. Precursors with different compositions were dealloyed and imaged in 3D. From X-ray tomography images, porous FeCr characteristics as solid fraction, phase size, specific surface were extracted. EBSD maps were acquired on samples before and after dealloying. We will show that precursor composition is a key parameter to control pores and grains size while dealloying parameters (time and temperature) are key parameters to control ligaments size and in fine specific surface. By controlling precursor composition and dealloying parameters it is now possible to get dealloyed nanoporous metals with desired grain and porous microstructure by liquid metal dealloying. •FeCr-Ni precursors were dealloyed in a Mg bath to give FeCr-Mg bicontinuous structure.•FeCr-Mg bicontinuous structure was immersed in HNO3 solution to get porous FeCr.•(FeCr)x-Ni1−x precursors are fully FCC phase while porous FeCr are fully BCC phase.•Composition & dealloying parameters are key parameters for controlling microstructure
AbstractList	Highlights: • FeCr-Ni precursors were dealloyed in a Mg bath to give FeCr-Mg bicontinuous structure. • FeCr-Mg bicontinuous structure was immersed in HNO{sub 3} solution to get porous FeCr. • (FeCr){sub x}-Ni{sub 1−x} precursors are fully FCC phase while porous FeCr are fully BCC phase. • Composition & dealloying parameters are key parameters for controlling microstructure - Abstract: Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a (FeCr){sub x}-Ni{sub 1−x} precursor, it is possible to get porous FeCr with this technique. While immersing precursors in a molten Mg bath, Ni atoms selectively migrate into the Mg bath. After cooling down to room temperature, the resulting microstructure is a bi-continuous structure of FeCr and Mg (with Ni in solid solution). A final etching step removes the Mg solid-state solution phase. Precursors with different compositions were dealloyed and imaged in 3D. From X-ray tomography images, porous FeCr characteristics as solid fraction, phase size, specific surface were extracted. EBSD maps were acquired on samples before and after dealloying. We will show that precursor composition is a key parameter to control pores and grains size while dealloying parameters (time and temperature) are key parameters to control ligaments size and in fine specific surface. By controlling precursor composition and dealloying parameters it is now possible to get dealloyed nanoporous metals with desired grain and porous microstructure by liquid metal dealloying. Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a (FeCr)x-Ni1−x precursor, it is possible to get porous FeCr with this technique.While immersing precursors in a molten Mg bath, Ni atoms selectively migrate into the Mg bath. After cooling down to room temperature, the resulting microstructure is a bi-continuous structure of FeCr and Mg (with Ni in solid solution). A final etching step removes the Mg solid-state solution phase. Precursors with different compositions were dealloyed and imaged in 3D. From X-ray tomography images, porous FeCr characteristics as solid fraction, phase size, specific surface were extracted. EBSD maps were acquired on samples before and after dealloying.We will show that precursor composition is a key parameter to control pores and grains size while dealloying parameters (time and temperature) are key parameters to control ligaments size and in fine specific surface. By controlling precursor composition and dealloying parameters it is now possible to get dealloyed nanoporous metals with desired grain and porous microstructure by liquid metal dealloying. Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a (FeCr)x-Ni1−x precursor, it is possible to get porous FeCr with this technique. While immersing precursors in a molten Mg bath, Ni atoms selectively migrate into the Mg bath. After cooling down to room temperature, the resulting microstructure is a bi-continuous structure of FeCr and Mg (with Ni in solid solution). A final etching step removes the Mg solid-state solution phase. Precursors with different compositions were dealloyed and imaged in 3D. From X-ray tomography images, porous FeCr characteristics as solid fraction, phase size, specific surface were extracted. EBSD maps were acquired on samples before and after dealloying. We will show that precursor composition is a key parameter to control pores and grains size while dealloying parameters (time and temperature) are key parameters to control ligaments size and in fine specific surface. By controlling precursor composition and dealloying parameters it is now possible to get dealloyed nanoporous metals with desired grain and porous microstructure by liquid metal dealloying. •FeCr-Ni precursors were dealloyed in a Mg bath to give FeCr-Mg bicontinuous structure.•FeCr-Mg bicontinuous structure was immersed in HNO3 solution to get porous FeCr.•(FeCr)x-Ni1−x precursors are fully FCC phase while porous FeCr are fully BCC phase.•Composition & dealloying parameters are key parameters for controlling microstructure
Author	Maire, Eric Bonnin, Anne Kato, Hidemi Adrien, Jérome Le Bourlot, Christophe Wada, Takeshi Duchet-Rumeau, Jannick Mokhtari, Morgane
Author_xml	– sequence: 1 givenname: Morgane orcidid: 0000-0002-2402-8927 surname: Mokhtari fullname: Mokhtari, Morgane organization: Univ Lyon, INSA Lyon, MATEIS, CNRS UMR5510, F-69621 Villeurbanne, France – sequence: 2 givenname: Christophe orcidid: 0000-0001-8088-4261 surname: Le Bourlot fullname: Le Bourlot, Christophe email: christophe.le-bourlot@insa-lyon.fr organization: Univ Lyon, INSA Lyon, MATEIS, CNRS UMR5510, F-69621 Villeurbanne, France – sequence: 3 givenname: Jérome surname: Adrien fullname: Adrien, Jérome organization: Univ Lyon, INSA Lyon, MATEIS, CNRS UMR5510, F-69621 Villeurbanne, France – sequence: 4 givenname: Anne surname: Bonnin fullname: Bonnin, Anne organization: Swiss Light Source, Paul Scherrer Institute, Villigen, Switzerland – sequence: 5 givenname: Takeshi surname: Wada fullname: Wada, Takeshi organization: Institute for Materials Research, Tohoku University, 2-1-1 Katahira, Aoba Ward, Sendai 980-8577, Japan – sequence: 6 givenname: Jannick surname: Duchet-Rumeau fullname: Duchet-Rumeau, Jannick organization: Univ Lyon, INSA Lyon, IMP, CNRS UMR5223, F-69621 Villeurbanne, France – sequence: 7 givenname: Hidemi surname: Kato fullname: Kato, Hidemi organization: Institute for Materials Research, Tohoku University, 2-1-1 Katahira, Aoba Ward, Sendai 980-8577, Japan – sequence: 8 givenname: Eric surname: Maire fullname: Maire, Eric organization: Univ Lyon, INSA Lyon, MATEIS, CNRS UMR5510, F-69621 Villeurbanne, France
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Keywords	X-ray tomography Dealloying EBSD Porous Fe
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Snippet	Liquid metal dealloying is a promising technique to get nanoporous materials which are attractive for their excellent functional properties. From a... Highlights: • FeCr-Ni precursors were dealloyed in a Mg bath to give FeCr-Mg bicontinuous structure. • FeCr-Mg bicontinuous structure was immersed in HNO{sub...
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SubjectTerms	BACKSCATTERING BCC LATTICES CHROMIUM COMPOUNDS Condensed Matter Dealloying EBSD ELECTRON DIFFRACTION FCC LATTICES Instrumentation and Detectors IRON COMPOUNDS LIQUID METALS Materials and structures in mechanics MATERIALS SCIENCE Mechanical engineering Mechanics Mechanics of materials PHASE STUDIES Physics Porous POROUS MATERIALS SOLID SOLUTIONS SOLIDS SURFACES TOMOGRAPHY X-ray tomography
Title	Microstructure characterization by X-ray tomography and EBSD of porous FeCr produced by liquid metal dealloying
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