Improvement of Vickers hardness measurement on SWNT/Al2O3 composites consolidated by spark plasma sintering
Dense alumina composites with different carbon nanotube content were prepared by colloidal processing and consolidated by Spark Plasma Sintering (SPS). Single-wall carbon nanotubes (SWNTs) were distributed at grain boundaries and also into agglomerates homogeneously dispersed. Carrying out Vickers h...
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| Veröffentlicht in: | Journal of the European Ceramic Society Jg. 34; H. 15; S. 3801 - 3809 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Elsevier Ltd
01.12.2014
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| ISSN: | 0955-2219, 1873-619X |
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| Abstract | Dense alumina composites with different carbon nanotube content were prepared by colloidal processing and consolidated by Spark Plasma Sintering (SPS). Single-wall carbon nanotubes (SWNTs) were distributed at grain boundaries and also into agglomerates homogeneously dispersed. Carrying out Vickers hardness tests on the cross-section surfaces instead of top (or bottom) surfaces has shown a noticeable increase in the reliability of the hardness measurements. This improvement has been mainly attributed to the different morphology of carbon nanotube agglomerates, which however does not seem to affect the Vickers hardness value. Composites with lower SWNT content maintain the Vickers hardness of monolithic alumina, whereas it significantly decreases for the rest of compositions. The decreasing trend with increasing SWNT content has been explained by the presence of higher SWNT quantities at grain boundaries. Based on the results obtained, a method for optimizing Vickers hardness tests performance on SWNT/Al2O3 composites sintered by SPS is proposed. |
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| AbstractList | Dense alumina composites with different carbon nanotube content were prepared by colloidal processing and consolidated by Spark Plasma Sintering (SPS). Single-wall carbon nanotubes (SWNTs) were distributed at grain boundaries and also into agglomerates homogeneously dispersed. Carrying out Vickers hardness tests on the cross-section surfaces instead of top (or bottom) surfaces has shown a noticeable increase in the reliability of the hardness measurements. This improvement has been mainly attributed to the different morphology of carbon nanotube agglomerates, which however does not seem to affect the Vickers hardness value. Composites with lower SWNT content maintain the Vickers hardness of monolithic alumina, whereas it significantly decreases for the rest of compositions. The decreasing trend with increasing SWNT content has been explained by the presence of higher SWNT quantities at grain boundaries. Based on the results obtained, a method for optimizing Vickers hardness tests performance on SWNT/Al2O3 composites sintered by SPS is proposed. |
| Author | Gallardo–López, A. Domínguez–Rodríguez, A. Morales–Rodríguez, A. Poyato, R. Fernández–Serrano, A. Muñoz, A. |
| Author_xml | – sequence: 1 givenname: A. surname: Morales–Rodríguez fullname: Morales–Rodríguez, A. email: amr@us.es organization: Department of Condensed Matter Physics, Universidad de Sevilla, P.O. BOX 1065, 41080 Sevilla, Spain – sequence: 2 givenname: A. surname: Gallardo–López fullname: Gallardo–López, A. organization: Department of Condensed Matter Physics, Universidad de Sevilla, P.O. BOX 1065, 41080 Sevilla, Spain – sequence: 3 givenname: A. surname: Fernández–Serrano fullname: Fernández–Serrano, A. organization: Department of Condensed Matter Physics, Universidad de Sevilla, P.O. BOX 1065, 41080 Sevilla, Spain – sequence: 4 givenname: R. surname: Poyato fullname: Poyato, R. organization: Materials Science Institute of Sevilla (CSIC–Universidad de Sevilla), Américo Vespucio 49, 41092 Sevilla, Spain – sequence: 5 givenname: A. surname: Muñoz fullname: Muñoz, A. organization: Department of Condensed Matter Physics, Universidad de Sevilla, P.O. BOX 1065, 41080 Sevilla, Spain – sequence: 6 givenname: A. surname: Domínguez–Rodríguez fullname: Domínguez–Rodríguez, A. organization: Department of Condensed Matter Physics, Universidad de Sevilla, P.O. BOX 1065, 41080 Sevilla, Spain |
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| Keywords | Carbon nanotubes Spark plasma sintering Vickers hardness Nanocomposites Alumina |
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| Title | Improvement of Vickers hardness measurement on SWNT/Al2O3 composites consolidated by spark plasma sintering |
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