MOF-Derived Ni1−xCox@Carbon with Tunable Nano–Microstructure as Lightweight and Highly Efficient Electromagnetic Wave Absorber

Highlights MOF-derived porous Ni 1− x Co x @Carbon composites with tuning nano-micro structure were successfully synthesized. Magnetic-dielectric synergy effect among the Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology. MOF-derived Ni@C microspheres dis...

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Published in:	Nano-micro letters Vol. 12; no. 1; p. 150
Main Authors:	Wang, Lei, Huang, Mengqiu, Yu, Xuefeng, You, Wenbin, Zhang, Jie, Liu, Xianhu, Wang, Min, Che, Renchao
Format:	Journal Article
Language:	English
Published:	Singapore Springer Singapore 01.12.2020 Springer Nature B.V
Subjects:	Absorbers Architecture Bimetals Carbon Chemical synthesis Composite materials Dielectric strength Electromagnetic radiation Energy conversion Engineering Functional materials Holography Magnetic properties Metal-organic frameworks Microspheres Microwave absorption Nanoscale Science and Technology Nanotechnology Nanotechnology and Microengineering Thermal decomposition Wave power Polarization Electromagnetic parameters Microwave absorption Magnetic coupling Metal–organic frameworks
ISSN:	2311-6706, 2150-5551, 2150-5551
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Abstract	Highlights MOF-derived porous Ni 1− x Co x @Carbon composites with tuning nano-micro structure were successfully synthesized. Magnetic-dielectric synergy effect among the Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology. MOF-derived Ni@C microspheres displayed strong microwave absorption value of − 59.5 dB. . Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni 1− x Co x @Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp 2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni 1− x Co x @Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value − 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic–dielectric synergy effect of MOF-derived Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism.
AbstractList	HighlightsMOF-derived porous Ni1−xCox@Carbon composites with tuning nano-micro structure were successfully synthesized.Magnetic-dielectric synergy effect among the Ni1−xCox@Carbon microspheres was confirmed by the off-axis electron holography technology.MOF-derived Ni@C microspheres displayed strong microwave absorption value of − 59.5 dB..Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni1−xCox@Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni1−xCox@Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value − 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic–dielectric synergy effect of MOF-derived Ni1−xCox@Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism. Highlights MOF-derived porous Ni 1− x Co x @Carbon composites with tuning nano-micro structure were successfully synthesized. Magnetic-dielectric synergy effect among the Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology. MOF-derived Ni@C microspheres displayed strong microwave absorption value of − 59.5 dB. . Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni 1− x Co x @Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp 2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni 1− x Co x @Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value − 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic–dielectric synergy effect of MOF-derived Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism. MOF-derived porous Ni1−xCox@Carbon composites with tuning nano-micro structure were successfully synthesized.Magnetic-dielectric synergy effect among the Ni1−xCox@Carbon microspheres was confirmed by the off-axis electron holography technology.MOF-derived Ni@C microspheres displayed strong microwave absorption value of − 59.5 dB.. Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni1−xCox@Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni1−xCox@Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value − 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic–dielectric synergy effect of MOF-derived Ni1−xCox@Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism. Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni1-xCox@Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni1-xCox@Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value - 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic-dielectric synergy effect of MOF-derived Ni1-xCox@Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism.Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni1-xCox@Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni1-xCox@Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value - 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic-dielectric synergy effect of MOF-derived Ni1-xCox@Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism. Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy conversion, especially in the microwave absorption (MA) field. Herein, porous Ni 1− x Co x @Carbon composites derived from metal-organic framework (MOF) were successfully synthesized via solvothermal reaction and subsequent annealing treatments. Benefiting from the coordination, carbonized bimetallic Ni-Co-MOF maintained its initial skeleton and transformed into magnetic-carbon composites with tunable nano-micro structure. During the thermal decomposition, generated magnetic particles/clusters acted as a catalyst to promote the carbon sp 2 arrangement, forming special core-shell architecture. Therefore, pure Ni@C microspheres displayed strong MA behaviors than other Ni 1− x Co x @Carbon composites. Surprisingly, magnetic-dielectric Ni@C composites possessed the strongest reflection loss value − 59.5 dB and the effective absorption frequency covered as wide as 4.7 GHz. Meanwhile, the MA capacity also can be boosted by adjusting the absorber content from 25% to 40%. Magnetic–dielectric synergy effect of MOF-derived Ni 1− x Co x @Carbon microspheres was confirmed by the off-axis electron holography technology making a thorough inquiry in the MA mechanism.
ArticleNumber	150
Author	Liu, Xianhu Che, Renchao Yu, Xuefeng Wang, Lei Zhang, Jie Wang, Min You, Wenbin Huang, Mengqiu
Author_xml	– sequence: 1 givenname: Lei surname: Wang fullname: Wang, Lei organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 2 givenname: Mengqiu surname: Huang fullname: Huang, Mengqiu organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 3 givenname: Xuefeng surname: Yu fullname: Yu, Xuefeng organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 4 givenname: Wenbin surname: You fullname: You, Wenbin organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 5 givenname: Jie surname: Zhang fullname: Zhang, Jie organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 6 givenname: Xianhu surname: Liu fullname: Liu, Xianhu organization: Key Laboratory of Materials Processing and Mold (Zhengzhou University), Ministry of Education – sequence: 7 givenname: Min surname: Wang fullname: Wang, Min organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University – sequence: 8 givenname: Renchao surname: Che fullname: Che, Renchao email: rcche@fudan.edu.cn organization: Laboratory of Advanced Materials, Department of Materials Science and Collaborative Innovation Center of Chemistry for Energy Materials (iChem), Fudan University
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Snippet	Highlights MOF-derived porous Ni 1− x Co x @Carbon composites with tuning nano-micro structure were successfully synthesized. Magnetic-dielectric synergy... Intrinsic electric-magnetic property and special nano-micro architecture of functional materials have a significant effect on its electromagnetic wave energy... HighlightsMOF-derived porous Ni1−xCox@Carbon composites with tuning nano-micro structure were successfully synthesized.Magnetic-dielectric synergy effect among... MOF-derived porous Ni1−xCox@Carbon composites with tuning nano-micro structure were successfully synthesized.Magnetic-dielectric synergy effect among the...
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SubjectTerms	Absorbers Architecture Bimetals Carbon Chemical synthesis Composite materials Dielectric strength Electromagnetic radiation Energy conversion Engineering Functional materials Holography Magnetic properties Metal-organic frameworks Microspheres Microwave absorption Nanoscale Science and Technology Nanotechnology Nanotechnology and Microengineering Thermal decomposition Wave power
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Title	MOF-Derived Ni1−xCox@Carbon with Tunable Nano–Microstructure as Lightweight and Highly Efficient Electromagnetic Wave Absorber
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