Thermal stability study of transition metal perovskite sulfides

Transition metal perovskite chalcogenides, a class of materials with rich tunability in functionalities, are gaining increased attention as candidate materials for renewable energy applications. Perovskite oxides are considered excellent n-type thermoelectric materials. Compared to oxide counterpart...

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Published in:	Journal of materials research Vol. 33; no. 24; pp. 4135 - 4143
Main Authors:	Niu, Shanyuan, Milam-Guerrero, JoAnna, Zhou, Yucheng, Ye, Kevin, Zhao, Boyang, Melot, Brent C., Ravichandran, Jayakanth
Format:	Journal Article
Language:	English
Published:	New York, USA Cambridge University Press 28.12.2018 Springer International Publishing Springer Nature B.V
Subjects:	Applied and Technical Physics Biomaterials Chalcogenides Cold Differential scanning calorimetry Heat conductivity Heat treating Heat treatment High temperature Inorganic Chemistry Invited Paper Iodine Materials Engineering Materials research Materials Science Materials selection Nanotechnology Organic chemistry Oxidation Perovskites Phase transitions Physical properties Raman spectroscopy Single crystals Stability analysis Studies Sulfur Thermal conductivity Thermal stability Thermodynamic properties Thermoelectric materials Thermogravimetric analysis Transition metals X-ray diffraction X-ray spectroscopy United States > US Massachusetts calorimetry S crystal growth
ISSN:	0884-2914, 2044-5326
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Abstract	Transition metal perovskite chalcogenides, a class of materials with rich tunability in functionalities, are gaining increased attention as candidate materials for renewable energy applications. Perovskite oxides are considered excellent n-type thermoelectric materials. Compared to oxide counterparts, we expect the chalcogenides to possess more favorable thermoelectric properties such as lower lattice thermal conductivity and smaller band gap, making them promising material candidates for high temperature thermoelectrics. Thus, it is necessary to study the thermal properties of these materials in detail, especially thermal stability, to evaluate their potential. In this work, we report the synthesis and thermal stability study of five compounds, α-SrZrS3, β-SrZrS3, BaZrS3, Ba2ZrS4, and Ba3Zr2S7. These materials cover several structural types including distorted perovskite, needle-like, and Ruddlesden–Popper phases. Differential scanning calorimeter and thermogravimetric analysis measurements were performed up to 1200 °C in air. Structural and chemical characterizations such as X-ray diffraction, Raman spectroscopy, and energy dispersive analytical X-ray spectroscopy were performed on all the samples before and after the heat treatment to understand the oxidation process. Our studies show that perovskite chalcogenides possess excellent thermal stability in air at least up to 550 °C.
AbstractList	Transition metal perovskite chalcogenides, a class of materials with rich tunability in functionalities, are gaining increased attention as candidate materials for renewable energy applications. Perovskite oxides are considered excellent n-type thermoelectric materials. Compared to oxide counterparts, we expect the chalcogenides to possess more favorable thermoelectric properties such as lower lattice thermal conductivity and smaller band gap, making them promising material candidates for high temperature thermoelectrics. Thus, it is necessary to study the thermal properties of these materials in detail, especially thermal stability, to evaluate their potential. In this work, we report the synthesis and thermal stability study of five compounds, α-SrZrS3, β-SrZrS3, BaZrS3, Ba2ZrS4, and Ba3Zr2S7. These materials cover several structural types including distorted perovskite, needle-like, and Ruddlesden–Popper phases. Differential scanning calorimeter and thermogravimetric analysis measurements were performed up to 1200 °C in air. Structural and chemical characterizations such as X-ray diffraction, Raman spectroscopy, and energy dispersive analytical X-ray spectroscopy were performed on all the samples before and after the heat treatment to understand the oxidation process. Our studies show that perovskite chalcogenides possess excellent thermal stability in air at least up to 550 °C. Transition metal perovskite chalcogenides, a class of materials with rich tunability in functionalities, are gaining increased attention as candidate materials for renewable energy applications. Perovskite oxides are considered excellent n-type thermoelectric materials. Compared to oxide counterparts, we expect the chalcogenides to possess more favorable thermoelectric properties such as lower lattice thermal conductivity and smaller band gap, making them promising material candidates for high temperature thermoelectrics. Thus, it is necessary to study the thermal properties of these materials in detail, especially thermal stability, to evaluate their potential. In this work, we report the synthesis and thermal stability study of five compounds, α-SrZrS 3 , β-SrZrS 3 , BaZrS 3 , Ba 2 ZrS 4 , and Ba 3 Zr 2 S 7 . These materials cover several structural types including distorted perovskite, needle-like, and Ruddlesden–Popper phases. Differential scanning calorimeter and thermogravimetric analysis measurements were performed up to 1200 °C in air. Structural and chemical characterizations such as X-ray diffraction, Raman spectroscopy, and energy dispersive analytical X-ray spectroscopy were performed on all the samples before and after the heat treatment to understand the oxidation process. Our studies show that perovskite chalcogenides possess excellent thermal stability in air at least up to 550 °C.
Author	Melot, Brent C. Zhao, Boyang Zhou, Yucheng Milam-Guerrero, JoAnna Niu, Shanyuan Ravichandran, Jayakanth Ye, Kevin
Author_xml	– sequence: 1 givenname: Shanyuan orcidid: 0000-0002-0559-3461 surname: Niu fullname: Niu, Shanyuan organization: Mork Family Department of Chemical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089, USA – sequence: 2 givenname: JoAnna surname: Milam-Guerrero fullname: Milam-Guerrero, JoAnna organization: †Department of Chemistry, University of Southern California, Los Angeles, California 90089, USA – sequence: 3 givenname: Yucheng surname: Zhou fullname: Zhou, Yucheng organization: Mork Family Department of Chemical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089, USA – sequence: 4 givenname: Kevin surname: Ye fullname: Ye, Kevin organization: Mork Family Department of Chemical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089, USA – sequence: 5 givenname: Boyang surname: Zhao fullname: Zhao, Boyang organization: Mork Family Department of Chemical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089, USA – sequence: 6 givenname: Brent C. surname: Melot fullname: Melot, Brent C. organization: †Department of Chemistry, University of Southern California, Los Angeles, California 90089, USA – sequence: 7 givenname: Jayakanth orcidid: 0000-0001-5030-9143 surname: Ravichandran fullname: Ravichandran, Jayakanth email: jayakanr@usc.edu organization: ‡Mork Family Department of Chemical Engineering and Materials Science, University of Southern California, Los Angeles, California 90089, USA; and Ming Hsieh Department of Electrical Engineering, University of Southern California, Los Angeles, California 90089, USA
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Snippet	Transition metal perovskite chalcogenides, a class of materials with rich tunability in functionalities, are gaining increased attention as candidate materials...
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SubjectTerms	Applied and Technical Physics Biomaterials Chalcogenides Cold Differential scanning calorimetry Heat conductivity Heat treating Heat treatment High temperature Inorganic Chemistry Invited Paper Iodine Materials Engineering Materials research Materials Science Materials selection Nanotechnology Organic chemistry Oxidation Perovskites Phase transitions Physical properties Raman spectroscopy Single crystals Stability analysis Studies Sulfur Thermal conductivity Thermal stability Thermodynamic properties Thermoelectric materials Thermogravimetric analysis Transition metals X-ray diffraction X-ray spectroscopy
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Title	Thermal stability study of transition metal perovskite sulfides
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Volume	33
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