Carbon Nanofiber Supported Transition-Metal Carbide Catalysts for the Hydrodeoxygenation of Guaiacol
Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55 bar hydrogen pressure ove...
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| Published in: | ChemCatChem Vol. 5; no. 10; pp. 2964 - 2972 |
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| Main Authors: | , , , , , |
| Format: | Journal Article |
| Language: | English |
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Weinheim
WILEY-VCH Verlag
01.10.2013
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
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| ISSN: | 1867-3880, 1867-3899 |
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| Abstract | Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55 bar hydrogen pressure over a temperature range of 300–375 °C for 4 h in dodecane, using a batch autoclave system. Combined selectivities of up to 87 and 69 % to phenol and methylated phenolics were obtained at 375 °C for W2C/CNF and Mo2C/CNF at >99 % conversion, respectively. The molybdenum carbide‐based catalyst showed a higher activity than W2C/CNF and yielded more completely deoxygenated aromatic products, such as benzene and toluene. Catalyst recycling experiments, performed with and without regeneration of the carbide phase, showed that the Mo2C/CNF catalyst was stable during reusability experiments. The most promising results were obtained with the Mo2C/CNF catalyst, as it showed a much higher activity and higher selectivity to phenolics compared to W2C/CNF.
Get off O′Me: Hydrodeoxygenation of guaiacol over W2C and Mo2C supported on carbon nanofibers was studied. These catalysts display high activities and selectivities towards phenol and cresols in comparison to previously reported CoMo/Al2O3 catalysts. Catalyst recycling experiments showed that the Mo2C/CNF catalyst is stable under reaction conditions and can be reused without further treatment (CNF=carbon nanofiber). |
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| AbstractList | Hydrodeoxygenation (HDO) studies over carbon nanofiber-supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55bar hydrogen pressure over a temperature range of 300-375°C for 4h in dodecane, using a batch autoclave system. Combined selectivities of up to 87 and 69% to phenol and methylated phenolics were obtained at 375°C for W2C/CNF and Mo2C/CNF at >99% conversion, respectively. The molybdenum carbide-based catalyst showed a higher activity than W2C/CNF and yielded more completely deoxygenated aromatic products, such as benzene and toluene. Catalyst recycling experiments, performed with and without regeneration of the carbide phase, showed that the Mo2C/CNF catalyst was stable during reusability experiments. The most promising results were obtained with the Mo2C/CNF catalyst, as it showed a much higher activity and higher selectivity to phenolics compared to W2C/CNF. [PUBLICATION ABSTRACT] Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W 2 C and Mo 2 C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55 bar hydrogen pressure over a temperature range of 300–375 °C for 4 h in dodecane, using a batch autoclave system. Combined selectivities of up to 87 and 69 % to phenol and methylated phenolics were obtained at 375 °C for W 2 C/CNF and Mo 2 C/CNF at >99 % conversion, respectively. The molybdenum carbide‐based catalyst showed a higher activity than W 2 C/CNF and yielded more completely deoxygenated aromatic products, such as benzene and toluene. Catalyst recycling experiments, performed with and without regeneration of the carbide phase, showed that the Mo 2 C/CNF catalyst was stable during reusability experiments. The most promising results were obtained with the Mo 2 C/CNF catalyst, as it showed a much higher activity and higher selectivity to phenolics compared to W 2 C/CNF. Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55 bar hydrogen pressure over a temperature range of 300–375 °C for 4 h in dodecane, using a batch autoclave system. Combined selectivities of up to 87 and 69 % to phenol and methylated phenolics were obtained at 375 °C for W2C/CNF and Mo2C/CNF at >99 % conversion, respectively. The molybdenum carbide‐based catalyst showed a higher activity than W2C/CNF and yielded more completely deoxygenated aromatic products, such as benzene and toluene. Catalyst recycling experiments, performed with and without regeneration of the carbide phase, showed that the Mo2C/CNF catalyst was stable during reusability experiments. The most promising results were obtained with the Mo2C/CNF catalyst, as it showed a much higher activity and higher selectivity to phenolics compared to W2C/CNF. Get off O′Me: Hydrodeoxygenation of guaiacol over W2C and Mo2C supported on carbon nanofibers was studied. These catalysts display high activities and selectivities towards phenol and cresols in comparison to previously reported CoMo/Al2O3 catalysts. Catalyst recycling experiments showed that the Mo2C/CNF catalyst is stable under reaction conditions and can be reused without further treatment (CNF=carbon nanofiber). Hydrodeoxygenation (HDO) studies over carbon nanofiber-supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate the potential of a catalyst for valorization of depolymerized lignin streams. Typical reactions were executed at 55 bar hydrogen pressure over a temperature range of 300–375¿°C for 4 h in dodecane, using a batch autoclave system. Combined selectivities of up to 87 and 69¿% to phenol and methylated phenolics were obtained at 375¿°C for W2C/CNF and Mo2C/CNF at >99¿% conversion, respectively. The molybdenum carbide-based catalyst showed a higher activity than W2C/CNF and yielded more completely deoxygenated aromatic products, such as benzene and toluene. Catalyst recycling experiments, performed with and without regeneration of the carbide phase, showed that the Mo2C/CNF catalyst was stable during reusability experiments. The most promising results were obtained with the Mo2C/CNF catalyst, as it showed a much higher activity and higher selectivity to phenolics compared to W2C/CNF. |
| Author | Dijkstra, Jelmer Bitter, Johannes H. Weckhuysen, Bert M. Gosselink, Robert W. Jongerius, Anna L. Bruijnincx, Pieter C. A. |
| Author_xml | – sequence: 1 givenname: Anna L. surname: Jongerius fullname: Jongerius, Anna L. organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 – sequence: 2 givenname: Robert W. surname: Gosselink fullname: Gosselink, Robert W. organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 – sequence: 3 givenname: Jelmer surname: Dijkstra fullname: Dijkstra, Jelmer organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 – sequence: 4 givenname: Johannes H. surname: Bitter fullname: Bitter, Johannes H. organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 – sequence: 5 givenname: Pieter C. A. surname: Bruijnincx fullname: Bruijnincx, Pieter C. A. organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 – sequence: 6 givenname: Bert M. surname: Weckhuysen fullname: Weckhuysen, Bert M. email: B.M.Weckhuysen@uu.nl organization: Utrecht University, Inorganic Chemistry and Catalysis, Debye Institute for Nanomaterials Science, Universiteitsweg 99, 3584 CG Utrecht (The Netherlands), Fax: (+31) 30-251-1027 |
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| Copyright | Copyright © 2013 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim Wageningen University & Research |
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A 2012, 423-424, 130. 2012; 439–440 2012; 285 2013; 3 2011; 13 2012; 17 1939; 56 2011; 17 2013; 6 1996; 75 2010; 20 2012; 134 2001 1997; 11 2000; 54 2013; 52 2010; 110 2011; 65 2010; 390 2011; 25 2010; 3 2003; 240 2009; 63 2011; 1 2000; 65 2009 2013 2013; 125 52 1996 2000; 199 2011; 4 1938; 60 2004; 108 2011; 172 2012; 106 2009; 28 2012; 50 2011; 102 2012; 413–414 2012; 2 2012; 435–436 2011; 92 2009; 100 2011; 141 2012; 4 2012; 5 2008 2008; 120 47 2012; 87 2009; 147 2011; 101 2012; 423–424 e_1_2_6_51_2 e_1_2_6_53_2 e_1_2_6_30_2 e_1_2_6_19_2 e_1_2_6_13_2 e_1_2_6_34_2 e_1_2_6_59_2 e_1_2_6_11_2 e_1_2_6_32_2 e_1_2_6_17_2 e_1_2_6_38_2 e_1_2_6_55_2 e_1_2_6_15_2 e_1_2_6_36_2 e_1_2_6_57_2 e_1_2_6_20_2 e_1_2_6_41_3 e_1_2_6_41_2 e_1_2_6_7_2 e_1_2_6_9_2 e_1_2_6_3_2 e_1_2_6_5_2 e_1_2_6_24_2 e_1_2_6_47_2 e_1_2_6_22_2 e_1_2_6_49_2 e_1_2_6_1_2 e_1_2_6_28_2 e_1_2_6_43_2 e_1_2_6_26_2 e_1_2_6_45_2 e_1_2_6_50_2 e_1_2_6_52_2 e_1_2_6_31_2 e_1_2_6_18_2 e_1_2_6_12_2 e_1_2_6_35_2 e_1_2_6_58_2 e_1_2_6_10_2 e_1_2_6_33_2 e_1_2_6_16_2 e_1_2_6_39_2 e_1_2_6_54_2 e_1_2_6_14_2 e_1_2_6_56_2 e_1_2_6_42_2 e_1_2_6_40_3 e_1_2_6_40_2 e_1_2_6_8_2 e_1_2_6_29_2 e_1_2_6_4_2 e_1_2_6_6_2 e_1_2_6_23_2 Oyama S. T. (e_1_2_6_37_2) 1996 e_1_2_6_48_2 e_1_2_6_2_2 e_1_2_6_21_2 e_1_2_6_27_2 e_1_2_6_44_2 e_1_2_6_25_2 e_1_2_6_46_2 |
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| Snippet | Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate... Hydrodeoxygenation (HDO) studies over carbon nanofiber‐supported (CNF) W 2 C and Mo 2 C catalysts were performed on guaiacol, a prototypical substrate to... Hydrodeoxygenation (HDO) studies over carbon nanofiber-supported (CNF) W2C and Mo2C catalysts were performed on guaiacol, a prototypical substrate to evaluate... |
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| SubjectTerms | aromatic chemicals carbides conversion depolymerization fast pyrolysis guaiacol hydrodeoxygenation hydrogenolysis lignin lignin model compounds molybdenum nitride catalysts organosolv lignin phenols reaction network vegetable-oils |
| Title | Carbon Nanofiber Supported Transition-Metal Carbide Catalysts for the Hydrodeoxygenation of Guaiacol |
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