ICTAC Kinetics Committee recommendations for collecting experimental thermal analysis data for kinetic computations
•Recommendations developed for collecting TG, DSC, and DTA data for successful kinetic analysis.•Focus is on preparing proper samples and selecting adequate experimental conditions.•Specific advice is offered for most common types of thermal processes, chemical and physical. The present recommendati...
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| Vydané v: | Thermochimica acta Ročník 590; s. 1 - 23 |
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| Hlavní autori: | , , , , , , , |
| Médium: | Journal Article |
| Jazyk: | English |
| Vydavateľské údaje: |
Elsevier B.V
20.08.2014
Elsevier |
| Predmet: | |
| ISSN: | 0040-6031, 1872-762X |
| On-line prístup: | Získať plný text |
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| Abstract | •Recommendations developed for collecting TG, DSC, and DTA data for successful kinetic analysis.•Focus is on preparing proper samples and selecting adequate experimental conditions.•Specific advice is offered for most common types of thermal processes, chemical and physical.
The present recommendations have been developed by the Kinetics Committee of the International Confederation for Thermal Analysis and Calorimetry (ICTAC). The recommendations offer guidance for obtaining kinetic data that are adequate to the actual kinetics of various processes, including thermal decomposition of inorganic solids; thermal and thermo-oxidative degradation of polymers and organics; reactions of solids with gases; polymerization and crosslinking; crystallization of polymers and inorganics; hazardous processes. The recommendations focus on kinetic measurements performed by means of thermal analysis methods such as thermogravimetry (TG) or thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and differential thermal analysis (DTA). The objective of these recommendations is to assist a non-expert with collecting adequate kinetic data by properly selecting the samples and measurement conditions. |
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| AbstractList | The present recommendations have been developed by the Kinetics Committee of the International Confederation for Thermal Analysis and Calorimetry (ICTAC). The recommendations offer guidance for obtaining kinetic data that are adequate to the actual kinetics of various processes, including thermal decomposition of inorganic solids; thermal and thermo-oxidative degradation of polymers and organics; reactions of solids with gases; polymerization and crosslinking; crystallization of polymers and inorganics; hazardous processes. The recommendations focus on kinetic measurements performed by means of thermal analysis methods such as thermogravimetry (TG) or thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and differential thermal analysis (DTA). The objective of these recommendations is to assist a non-expert with collecting adequate kinetic data by properly selecting the samples and measurement conditions. •Recommendations developed for collecting TG, DSC, and DTA data for successful kinetic analysis.•Focus is on preparing proper samples and selecting adequate experimental conditions.•Specific advice is offered for most common types of thermal processes, chemical and physical. The present recommendations have been developed by the Kinetics Committee of the International Confederation for Thermal Analysis and Calorimetry (ICTAC). The recommendations offer guidance for obtaining kinetic data that are adequate to the actual kinetics of various processes, including thermal decomposition of inorganic solids; thermal and thermo-oxidative degradation of polymers and organics; reactions of solids with gases; polymerization and crosslinking; crystallization of polymers and inorganics; hazardous processes. The recommendations focus on kinetic measurements performed by means of thermal analysis methods such as thermogravimetry (TG) or thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and differential thermal analysis (DTA). The objective of these recommendations is to assist a non-expert with collecting adequate kinetic data by properly selecting the samples and measurement conditions. |
| Author | Koga, Nobuyoshi Sbirrazzuoli, Nicolas Vyazovkin, Sergey Roduit, Bertrand Chrissafis, Konstantinos Di Lorenzo, Maria Laura Pijolat, Michèle Suñol, Joan Josep |
| Author_xml | – sequence: 1 givenname: Sergey orcidid: 0000-0002-6335-4215 surname: Vyazovkin fullname: Vyazovkin, Sergey email: vyazovkin@uab.edu organization: Department of Chemistry, University of Alabama at Birmingham, 901 S. 14th Street, Birmingham, AL 35294, USA – sequence: 2 givenname: Konstantinos surname: Chrissafis fullname: Chrissafis, Konstantinos organization: Solid State Physics Department, School of Physics, Aristotle University of Thessaloniki, Macedonia, Thessaloniki 541 24, Greece – sequence: 3 givenname: Maria Laura surname: Di Lorenzo fullname: Di Lorenzo, Maria Laura organization: Istituto per i Polimeri, Compositi e Biomateriali (CNR), c/o Comprensorio Olivetti, Via Campi Flegrei 34, Pozzuoli, NA 80078, Italy – sequence: 4 givenname: Nobuyoshi surname: Koga fullname: Koga, Nobuyoshi organization: Department of Science Education, Graduate School of Education, Hiroshima University, 1-1-1 Kagamiyama, Higashi-Hiroshima 739-8524, Japan – sequence: 5 givenname: Michèle surname: Pijolat fullname: Pijolat, Michèle organization: École Nationale Supérieure des Mines, Laboratoire Georges Friedel, CNRS UMR 5307, Centre SPIN, Saint-Étienne 42023, France – sequence: 6 givenname: Bertrand surname: Roduit fullname: Roduit, Bertrand organization: AKTS Inc., Advanced Kinetics and Technology Solutions, TECHNOArk 1, Siders 3960, Switzerland – sequence: 7 givenname: Nicolas surname: Sbirrazzuoli fullname: Sbirrazzuoli, Nicolas organization: Université Nice Sophia Antipolis, Laboratoire de Physique de la Matière Condensée, Equipe Fluides et Matériaux Complexes, CNRS UMR 7336, Parc Valrose Nice Cedex 2 06108, France – sequence: 8 givenname: Joan Josep surname: Suñol fullname: Suñol, Joan Josep organization: Departament de Física, Universitat de Girona, Girona, Catalonia 17071, Spain |
| BackLink | https://hal.science/hal-01056407$$DView record in HAL |
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| SubjectTerms | Chemical and Process Engineering Chemical Sciences crosslinking crystallization differential scanning calorimetry differential thermal analysis Engineering Sciences gases Glass Kinetics Liquid Material chemistry polymerization polymers Solid Temperature gradient thermal degradation thermogravimetry |
| Title | ICTAC Kinetics Committee recommendations for collecting experimental thermal analysis data for kinetic computations |
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