Crystallization behavior of poly(ε-caprolactone)/layered double hydroxide nanocomposites

Poly(ε-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. Th...

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Published in:	Journal of applied polymer science Vol. 116; no. 5; pp. 2658 - 2667
Main Authors:	Yang, Zhe, Peng, Hongdan, Wang, Weizhi, Liu, Tianxi
Format:	Journal Article
Language:	English
Published:	Hoboken Wiley Subscription Services, Inc., A Wiley Company 05.06.2010 Wiley
Subjects:	Activation energy Applied sciences Composites Crystallization Exact sciences and technology Forms of application and semi-finished materials Hydroxides Intercalation Mathematical models Melts morphology Nanocomposites Nucleation poly(ϵ-caprolactone) Polymer industry, paints, wood Reproduction Technology of polymers Aluminium Hydroxides Experimental study Lactone polymer Modeling nanocomposites Composite material Kinetic model Melt crystallization poly(ε-caprolactone) Cobalt Hydroxides Layered double hydroxide Morphology Aliphatic polymer crystallization Nanocomposite Kinetics Polycaprolactone Activation energy
ISSN:	0021-8995, 1097-4628, 1097-4628
Online Access:	Get full text
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Abstract	Poly(ε-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami-Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization.
AbstractList	Poly(ε-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami-Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization. Poly(ϵ‐caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami–Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami–Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 Poly([Greek Lunate Epsilon]-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami-Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization. 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 Poly(Îµ-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami-Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization. Poly([Greek Lunate Epsilon]-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt crystallization kinetics of neat PCL and its LDH nanocomposites was investigated with the Ozawa, Avrami, and combined Avrami-Ozawa methods. The Ozawa method failed to describe the crystallization kinetics of the studied systems. The Avrami method was found to be useful for describing the nonisothermal crystallization behavior, but the parameters in this method do not have explicit meaning for nonisothermal crystallization. The combined Avrami-Ozawa method explained the nonisothermal crystallization behavior of PCL and its LDH nanocomposites effectively. The kinetic results and polarized optical microscopy observations indicated that the addition of LDH could affect the mechanism of nucleation and growth of the PCL matrix. The Takhor model was used to analyze the activation energies of nonisothermal crystallization. [copy 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010
Author	Wang, Weizhi Yang, Zhe Peng, Hongdan Liu, Tianxi
Author_xml	– sequence: 1 fullname: Yang, Zhe – sequence: 2 fullname: Peng, Hongdan – sequence: 3 fullname: Wang, Weizhi – sequence: 4 fullname: Liu, Tianxi
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Keywords	Aluminium Hydroxides Experimental study Lactone polymer Modeling nanocomposites Composite material Kinetic model Melt crystallization poly(ε-caprolactone) Cobalt Hydroxides Layered double hydroxide Morphology Aliphatic polymer crystallization Nanocomposite Kinetics Polycaprolactone Activation energy
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Snippet	Poly(ε-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt... Poly(ϵ‐caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt... Poly([Greek Lunate Epsilon]-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The... Poly(Îµ-caprolactone) (PCL)/layered double hydroxide (LDH) nanocomposites were prepared successfully via simple solution intercalation. The nonisothermal melt...
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SubjectTerms	Activation energy Applied sciences Composites Crystallization Exact sciences and technology Forms of application and semi-finished materials Hydroxides Intercalation Mathematical models Melts morphology Nanocomposites Nucleation poly(ϵ-caprolactone) Polymer industry, paints, wood Reproduction Technology of polymers
Title	Crystallization behavior of poly(ε-caprolactone)/layered double hydroxide nanocomposites
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