In situ X-ray diffraction monitoring of a mechanochemical reaction reveals a unique topology metal-organic framework
Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling...
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| Published in: | Nature communications Vol. 6; no. 1; p. 6662 |
|---|---|
| Main Authors: | , , , , , , , , , , , , , |
| Format: | Journal Article |
| Language: | English |
| Published: |
London
Nature Publishing Group UK
23.03.2015
Nature Publishing Group |
| Subjects: | |
| ISSN: | 2041-1723, 2041-1723 |
| Online Access: | Get full text |
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| Abstract | Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling is thought to create an environment supporting nonconventional reactivity and exotic intermediates, such speculations have remained without proof. Here we use
in situ
, real-time powder X-ray diffraction monitoring to discover and capture a metastable, novel-topology intermediate of a mechanochemical transformation. Monitoring the mechanochemical synthesis of an archetypal metal-organic framework ZIF-8 by
in situ
powder X-ray diffraction reveals unexpected amorphization, and on further milling recrystallization into a non-porous material via a metastable intermediate based on a previously unreported topology, herein named
katsenite
(
kat
). The discovery of this phase and topology provides direct evidence that milling transformations can involve short-lived, structurally unusual phases not yet accessed by conventional chemistry.
Ball milling chemical reactions are of interest due to their environmental credentials and potential to achieve new reactions and materials. Here, the authors isolate a metastable material with a previously unknown net topology by
in situ
monitoring of the mechanosynthesis of a metal organic framework. |
|---|---|
| AbstractList | Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling is thought to create an environment supporting nonconventional reactivity and exotic intermediates, such speculations have remained without proof. Here we use
in situ
, real-time powder X-ray diffraction monitoring to discover and capture a metastable, novel-topology intermediate of a mechanochemical transformation. Monitoring the mechanochemical synthesis of an archetypal metal-organic framework ZIF-8 by
in situ
powder X-ray diffraction reveals unexpected amorphization, and on further milling recrystallization into a non-porous material via a metastable intermediate based on a previously unreported topology, herein named
katsenite
(
kat
). The discovery of this phase and topology provides direct evidence that milling transformations can involve short-lived, structurally unusual phases not yet accessed by conventional chemistry.
Ball milling chemical reactions are of interest due to their environmental credentials and potential to achieve new reactions and materials. Here, the authors isolate a metastable material with a previously unknown net topology by
in situ
monitoring of the mechanosynthesis of a metal organic framework. Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling is thought to create an environment supporting nonconventional reactivity and exotic intermediates, such speculations have remained without proof. Here we use in situ, real-time powder X-ray diffraction monitoring to discover and capture a metastable, novel-topology intermediate of a mechanochemical transformation. Monitoring the mechanochemical synthesis of an archetypal metal-organic framework ZIF-8 by in situ powder X-ray diffraction reveals unexpected amorphization, and on further milling recrystallization into a non-porous material via a metastable intermediate based on a previously unreported topology, herein named katsenite (kat). The discovery of this phase and topology provides direct evidence that milling transformations can involve short-lived, structurally unusual phases not yet accessed by conventional chemistry. Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling is thought to create an environment supporting nonconventional reactivity and exotic intermediates, such speculations have remained without proof. Here we use in situ, real-time powder X-ray diffraction monitoring to discover and capture a metastable, novel-topology intermediate of a mechanochemical transformation. Monitoring the mechanochemical synthesis of an archetypal metal-organic framework ZIF-8 by in situ powder X-ray diffraction reveals unexpected amorphization, and on further milling recrystallization into a non-porous material via a metastable intermediate based on a previously unreported topology, herein named katsenite (kat). The discovery of this phase and topology provides direct evidence that milling transformations can involve short-lived, structurally unusual phases not yet accessed by conventional chemistry.Chemical and physical transformations by milling are attracting enormous interest for their ability to access new materials and clean reactivity, and are central to a number of core industries, from mineral processing to pharmaceutical manufacturing. While continuous mechanical stress during milling is thought to create an environment supporting nonconventional reactivity and exotic intermediates, such speculations have remained without proof. Here we use in situ, real-time powder X-ray diffraction monitoring to discover and capture a metastable, novel-topology intermediate of a mechanochemical transformation. Monitoring the mechanochemical synthesis of an archetypal metal-organic framework ZIF-8 by in situ powder X-ray diffraction reveals unexpected amorphization, and on further milling recrystallization into a non-porous material via a metastable intermediate based on a previously unreported topology, herein named katsenite (kat). The discovery of this phase and topology provides direct evidence that milling transformations can involve short-lived, structurally unusual phases not yet accessed by conventional chemistry. |
| ArticleNumber | 6662 |
| Author | Puškarić, Andreas Dinnebier, Robert E. Halasz, Ivan Pham, Minh-Hao Lazić, Predrag Magdysyuk, Oxana Katsenis, Athanassios D. Užarević, Krunoslav Kimber, Simon A. J. Julien, Patrick A. Do, Trong-On Friščić, Tomislav Štrukil, Vjekoslav Mottillo, Cristina |
| Author_xml | – sequence: 1 givenname: Athanassios D. surname: Katsenis fullname: Katsenis, Athanassios D. organization: Department of Chemistry, McGill University – sequence: 2 givenname: Andreas surname: Puškarić fullname: Puškarić, Andreas organization: Ruđer Bošković Institute – sequence: 3 givenname: Vjekoslav surname: Štrukil fullname: Štrukil, Vjekoslav organization: Department of Chemistry, McGill University, Ruđer Bošković Institute – sequence: 4 givenname: Cristina surname: Mottillo fullname: Mottillo, Cristina organization: Department of Chemistry, McGill University – sequence: 5 givenname: Patrick A. surname: Julien fullname: Julien, Patrick A. organization: Department of Chemistry, McGill University – sequence: 6 givenname: Krunoslav surname: Užarević fullname: Užarević, Krunoslav organization: Ruđer Bošković Institute – sequence: 7 givenname: Minh-Hao surname: Pham fullname: Pham, Minh-Hao organization: Department of Chemical Engineering, Université Laval – sequence: 8 givenname: Trong-On surname: Do fullname: Do, Trong-On organization: Department of Chemical Engineering, Université Laval – sequence: 9 givenname: Simon A. J. surname: Kimber fullname: Kimber, Simon A. J. organization: ESRF—The European Synchrotron – sequence: 10 givenname: Predrag surname: Lazić fullname: Lazić, Predrag organization: Ruđer Bošković Institute – sequence: 11 givenname: Oxana surname: Magdysyuk fullname: Magdysyuk, Oxana organization: Scientific Service Group X-ray Diffraction, Max Planck Institute for Solid State Research – sequence: 12 givenname: Robert E. surname: Dinnebier fullname: Dinnebier, Robert E. organization: Scientific Service Group X-ray Diffraction, Max Planck Institute for Solid State Research – sequence: 13 givenname: Ivan surname: Halasz fullname: Halasz, Ivan email: ihalasz@irb.hr organization: Ruđer Bošković Institute – sequence: 14 givenname: Tomislav surname: Friščić fullname: Friščić, Tomislav email: tomislav.friscic@mcgill.ca organization: Department of Chemistry, McGill University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25798542$$D View this record in MEDLINE/PubMed |
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| Title | In situ X-ray diffraction monitoring of a mechanochemical reaction reveals a unique topology metal-organic framework |
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