Reflections on the Spatial Performance of Atom Probe Tomography in the Analysis of Atomic Neighborhoods

Atom probe tomography (APT) is often introduced as providing “atomic-scale” mapping of the composition of materials and as such is often exploited to analyze atomic neighborhoods within a material. Yet quantifying the actual spatial performance of the technique in a general case remains challenging,...

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Veröffentlicht in:	Microscopy and microanalysis Jg. 28; H. 4; S. 1116 - 1126
Hauptverfasser:	Gault, Baptiste, Klaes, Benjamin, Morgado, Felipe F., Freysoldt, Christoph, Li, Yue, De Geuser, Frederic, Stephenson, Leigh T., Vurpillot, François
Format:	Journal Article
Sprache:	Englisch
Veröffentlicht:	New York, USA Cambridge University Press 01.08.2022 Oxford University Press
Schlagworte:	Atoms & subatomic particles Condensed Matter Datasets Development and Computation Evaporation Field ion microscopy High entropy alloys Materials Science Metals Microscopy Neighborhoods Physics Simulation Solid solutions Spatial discrimination Spatial resolution Tomography compositionally complex alloys nearest neighbors field evaporation image simulations
ISSN:	1431-9276, 1435-8115, 1435-8115
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Abstract	Atom probe tomography (APT) is often introduced as providing “atomic-scale” mapping of the composition of materials and as such is often exploited to analyze atomic neighborhoods within a material. Yet quantifying the actual spatial performance of the technique in a general case remains challenging, as it depends on the material system being investigated as well as on the specimen's geometry. Here, by using comparisons with field-ion microscopy experiments, field-ion imaging and field evaporation simulations, we provide the basis for a critical reflection on the spatial performance of APT in the analysis of pure metals, low alloyed systems and concentrated solid solutions (i.e., akin to high-entropy alloys). The spatial resolution imposes strong limitations on the possible interpretation of measured atomic neighborhoods, and directional neighborhood analyses restricted to the depth are expected to be more robust. We hope this work gets the community to reflect on its practices, in the same way, it got us to reflect on our work.
AbstractList	Atom probe tomography (APT) is often introduced as providing "atomic-scale" mapping of the composition of materials and as such is often exploited to analyze atomic neighborhoods within a material. Yet quantifying the actual spatial performance of the technique in a general case remains challenging, as it depends on the material system being investigated as well as on the specimen's geometry. Here, by using comparisons with field-ion microscopy experiments, field-ion imaging and field evaporation simulations, we provide the basis for a critical reflection on the spatial performance of APT in the analysis of pure metals, low alloyed systems and concentrated solid solutions (i.e., akin to high-entropy alloys). The spatial resolution imposes strong limitations on the possible interpretation of measured atomic neighborhoods, and directional neighborhood analyses restricted to the depth are expected to be more robust. We hope this work gets the community to reflect on its practices, in the same way, it got us to reflect on our work. Atom probe tomography (APT) is often introduced as providing “atomic-scale” mapping of the composition of materials and as such is often exploited to analyze atomic neighborhoods within a material. Yet quantifying the actual spatial performance of the technique in a general case remains challenging, as it depends on the material system being investigated as well as on the specimen's geometry. Here, by using comparisons with field-ion microscopy experiments, field-ion imaging and field evaporation simulations, we provide the basis for a critical reflection on the spatial performance of APT in the analysis of pure metals, low alloyed systems and concentrated solid solutions (i.e., akin to high-entropy alloys). The spatial resolution imposes strong limitations on the possible interpretation of measured atomic neighborhoods, and directional neighborhood analyses restricted to the depth are expected to be more robust. We hope this work gets the community to reflect on its practices, in the same way, it got us to reflect on our work.Atom probe tomography (APT) is often introduced as providing “atomic-scale” mapping of the composition of materials and as such is often exploited to analyze atomic neighborhoods within a material. Yet quantifying the actual spatial performance of the technique in a general case remains challenging, as it depends on the material system being investigated as well as on the specimen's geometry. Here, by using comparisons with field-ion microscopy experiments, field-ion imaging and field evaporation simulations, we provide the basis for a critical reflection on the spatial performance of APT in the analysis of pure metals, low alloyed systems and concentrated solid solutions (i.e., akin to high-entropy alloys). The spatial resolution imposes strong limitations on the possible interpretation of measured atomic neighborhoods, and directional neighborhood analyses restricted to the depth are expected to be more robust. We hope this work gets the community to reflect on its practices, in the same way, it got us to reflect on our work.
Author	Vurpillot, François De Geuser, Frederic Gault, Baptiste Klaes, Benjamin Freysoldt, Christoph Li, Yue Morgado, Felipe F. Stephenson, Leigh T.
Author_xml	– sequence: 1 givenname: Baptiste orcidid: 0000-0002-4934-0458 surname: Gault fullname: Gault, Baptiste email: b.gault@mpie.de organization: 1Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, Düsseldorf 40237, Germany – sequence: 2 givenname: Benjamin orcidid: 0000-0002-9295-0489 surname: Klaes fullname: Klaes, Benjamin organization: 3Groupe Physique des Matériaux, Université de Rouen, Saint Etienne du Rouvray, Normandie 76800, France – sequence: 3 givenname: Felipe F. surname: Morgado fullname: Morgado, Felipe F. organization: 1Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, Düsseldorf 40237, Germany – sequence: 4 givenname: Christoph orcidid: 0000-0002-7896-3478 surname: Freysoldt fullname: Freysoldt, Christoph organization: 1Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, Düsseldorf 40237, Germany – sequence: 5 givenname: Yue surname: Li fullname: Li, Yue organization: 1Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, Düsseldorf 40237, Germany – sequence: 6 givenname: Frederic surname: De Geuser fullname: De Geuser, Frederic organization: 4Université Grenoble Alpes, CNRS, Grenoble INP, SIMAP, Grenoble 38000, France – sequence: 7 givenname: Leigh T. orcidid: 0000-0002-7852-2509 surname: Stephenson fullname: Stephenson, Leigh T. organization: 1Max-Planck-Institut für Eisenforschung, Max-Planck-Str. 1, Düsseldorf 40237, Germany – sequence: 8 givenname: François surname: Vurpillot fullname: Vurpillot, François organization: 3Groupe Physique des Matériaux, Université de Rouen, Saint Etienne du Rouvray, Normandie 76800, France
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Keywords	compositionally complex alloys nearest neighbors field evaporation image simulations
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Snippet	Atom probe tomography (APT) is often introduced as providing “atomic-scale” mapping of the composition of materials and as such is often exploited to analyze... Atom probe tomography (APT) is often introduced as providing "atomic-scale" mapping of the composition of materials and as such is often exploited to analyze...
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SubjectTerms	Atoms & subatomic particles Condensed Matter Datasets Development and Computation Evaporation Field ion microscopy High entropy alloys Materials Science Metals Microscopy Neighborhoods Physics Simulation Solid solutions Spatial discrimination Spatial resolution Tomography
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Title	Reflections on the Spatial Performance of Atom Probe Tomography in the Analysis of Atomic Neighborhoods
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