Humins from Biorefineries as Thermoreactive Macromolecular Systems
Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, ne...
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| Vydané v: | ChemSusChem Ročník 11; číslo 24; s. 4246 - 4255 |
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| Hlavní autori: | , , , |
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| Jazyk: | English |
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Germany
Wiley Subscription Services, Inc
20.12.2018
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| ISSN: | 1864-5631, 1864-564X, 1864-564X |
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| Abstract | Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass‐transition temperature (Tg>65 °C). Thus, humins can be easily processed for preparing thermoset‐like resins.
Pay attention to the humins: Thermal treatment of humins—a black and viscous coproduct from polysaccharide biorefining—is studied with a focus on tuning their structures and properties for new valorization strategies. On sufficient heating, humins form a more branched structure with a relatively high glass transition temperature, and thus they can be easily processed for preparing thermoset‐like resins. |
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| AbstractList | Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass‐transition temperature (Tg>65 °C). Thus, humins can be easily processed for preparing thermoset‐like resins.
Pay attention to the humins: Thermal treatment of humins—a black and viscous coproduct from polysaccharide biorefining—is studied with a focus on tuning their structures and properties for new valorization strategies. On sufficient heating, humins form a more branched structure with a relatively high glass transition temperature, and thus they can be easily processed for preparing thermoset‐like resins. Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass-transition temperature (Tg >65 °C). Thus, humins can be easily processed for preparing thermoset-like resins.Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass-transition temperature (Tg >65 °C). Thus, humins can be easily processed for preparing thermoset-like resins. Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass‐transition temperature (Tg>65 °C). Thus, humins can be easily processed for preparing thermoset‐like resins. Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass‐transition temperature ( T g >65 °C). Thus, humins can be easily processed for preparing thermoset‐like resins. Conversion of lignocellulosic biomass often brings about the formation of several side products. Among these, a black and viscous coproduct known as humins is formed on acidic treatment of polysaccharides. To improve the efficiency of this process from an economical and environmental perspective, new solutions for humins valorization are urgently needed. This work focuses on the comprehensive understanding of humins with special emphasis on their structure/properties relationships. Humins were subjected to different thermal treatments and characterized by means of structural, thermoanalytical, and rheological investigations. The structure and composition of humins are very diverse and depend on the thermochemical conditions. On sufficient heating, humins change into a nonreversible and more branched furanic structure with a relatively high glass-transition temperature (T >65 °C). Thus, humins can be easily processed for preparing thermoset-like resins. |
| Author | Sbirrazzuoli, Nicolas Sangregorio, Anna Guigo, Nathanael van der Waal, Jan C. |
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| Cites_doi | 10.1021/acssuschemeng.5b00473 10.1039/b812512k 10.1039/C7CC03679E 10.1016/j.cattod.2017.03.008 10.1002/cssc.201800620 10.1205/cherd05038 10.1002/cssc.201501371 10.1016/S0268-005X(00)00020-5 10.1021/ef3007454 10.3390/su10061795 10.1016/j.rser.2015.07.021 10.1021/acssuschemeng.7b03648 10.1002/cssc.201300332 10.1039/C7GC01405H 10.1016/j.jaap.2016.12.014 10.1039/C4GC01324G 10.3390/polym9080373 10.1039/C6RA24218A 10.1134/S1070427210020266 10.1021/ef2010157 10.1039/C5GC00327J 10.1002/slct.201701553 10.1021/acssuschemeng.6b02292 10.1021/cr300182k 10.1039/b518176c 10.1002/cssc.201801535 10.1039/C7GC03054A 10.1002/cssc.201801757 10.1021/acsomega.8b01274 10.1021/bk-2012-1105.ch001 10.1021/acssuschemeng.6b01834 10.1021/sc5003769 10.1007/BFb0009107 10.1002/bbb.1537 10.1002/cssc.201800778 10.1021/jp1119662 10.1039/C5GC01938A 10.1016/j.jaap.2013.07.003 10.1002/recl.19380570402 10.1016/j.conbuildmat.2016.11.019 10.1002/cssc.201300446 |
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| Title | Humins from Biorefineries as Thermoreactive Macromolecular Systems |
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