Hierarchical Co9S8 hollow microspheres as multifunctional electrocatalysts for oxygen reduction, oxygen evolution and hydrogen evolution reactions
Making efficient trifunctional non-precious metal catalysts for simultaneously catalyzing oxygen reduction reaction (ORR), oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) in same electrolyte is very important to bring energy conversion and storage systems into realities. Herein...
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| Veröffentlicht in: | Electrochimica acta Jg. 246; S. 380 - 390 |
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| Format: | Journal Article |
| Sprache: | Englisch |
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Oxford
Elsevier Ltd
20.08.2017
Elsevier BV |
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| ISSN: | 0013-4686, 1873-3859 |
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| Abstract | Making efficient trifunctional non-precious metal catalysts for simultaneously catalyzing oxygen reduction reaction (ORR), oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) in same electrolyte is very important to bring energy conversion and storage systems into realities. Herein, hierarchical Co9S8 hollow microspheres had been designed and synthesized by a facile hydrothermal reaction at 140°C (denoted as Co9S8 HMs-140). The properties and formation process of the Co9S8 HMs-140 were systematically investigated. Owing to the composition and structure features, the Co9S8 HMs-140 can be used as a trifunctional catalyst for ORR, OER and HER in the same alkaline electrolyte. The Co9S8 HMs-140 shows reasonable ORR and HER performance. Additionally, OER performance of the Co9S8 HMs-140 is superior to that of RuO2, such as a low onset potential (1.47V vs. RHE) and high stability. Furthermore, due to the bifunctional OER and HER activity of the Co9S8 HMs-140, the Co9S8 HMs-140 affords an O2 efficiency of 31 mmolh−1 and a H2 efficiency of 62mmolh−1 at 1.60V in 1M KOH solution under the given time range, exhibiting a 96% faradaic yield in the process of full water splitting to produce O2 and H2. The present work will provide a promising prospect for the development of multifunctional transition metal sulfides as effective electrocatalysts for sustainable energy systems. |
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| AbstractList | Making efficient trifunctional non-precious metal catalysts for simultaneously catalyzing oxygen reduction reaction (ORR), oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) in same electrolyte is very important to bring energy conversion and storage systems into realities. Herein, hierarchical Co9S8 hollow microspheres had been designed and synthesized by a facile hydrothermal reaction at 140°C (denoted as Co9S8 HMs-140). The properties and formation process of the Co9S8 HMs-140 were systematically investigated. Owing to the composition and structure features, the Co9S8 HMs-140 can be used as a trifunctional catalyst for ORR, OER and HER in the same alkaline electrolyte. The Co9S8 HMs-140 shows reasonable ORR and HER performance. Additionally, OER performance of the Co9S8 HMs-140 is superior to that of RuO2, such as a low onset potential (1.47V vs. RHE) and high stability. Furthermore, due to the bifunctional OER and HER activity of the Co9S8 HMs-140, the Co9S8 HMs-140 affords an O2 efficiency of 31 mmolh−1 and a H2 efficiency of 62mmolh−1 at 1.60V in 1M KOH solution under the given time range, exhibiting a 96% faradaic yield in the process of full water splitting to produce O2 and H2. The present work will provide a promising prospect for the development of multifunctional transition metal sulfides as effective electrocatalysts for sustainable energy systems. Making efficient trifunctional non-precious metal catalysts for simultaneously catalyzing oxygen reduction reaction (ORR), oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) in same electrolyte is very important to bring energy conversion and storage systems into realities. Herein, hierarchical Co9S8 hollow microspheres had been designed and synthesized by a facile hydrothermal reaction at 140 °C (denoted as Co9S8 HMs-140). The properties and formation process of the Co9S8 HMs-140 were systematically investigated. Owing to the composition and structure features, the Co9S8 HMs-140 can be used as a trifunctional catalyst for ORR, OER and HER in the same alkaline electrolyte. The Co9S8 HMs-140 shows reasonable ORR and HER performance. Additionally, OER performance of the Co9S8 HMs-140 is superior to that of RuO2, such as a low onset potential (1.47 V vs. RHE) and high stability. Furthermore, due to the bifunctional OER and HER activity of the Co9S8 HMs-140, the Co9S8 HMs-140 affords an O2 efficiency of 31mmol h-1 and a H2 efficiency of 62 mmol h-1 at 1.60 V in 1 M KOH solution under the given time range, exhibiting a 96% faradaic yield in the process of full water splitting to produce O2 and H2. The present work will provide a promising prospect for the development of multifunctional transition metal sulfides as effective electrocatalysts for sustainable energy systems. |
| Author | Zhang, Yatian Yang, Lin Han, Huijuan Bai, Zhengyu Chao, Shujun Wang, Xiaobing |
| Author_xml | – sequence: 1 givenname: Yatian surname: Zhang fullname: Zhang, Yatian organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China – sequence: 2 givenname: Shujun surname: Chao fullname: Chao, Shujun email: chaoshujun1979@163.com organization: Key Laboratory of Medical Molecular Probes, School of Basic Medical Sciences, Xinxiang Medial University, Xinxiang 453003, P.R. China – sequence: 3 givenname: Xiaobing surname: Wang fullname: Wang, Xiaobing organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China – sequence: 4 givenname: Huijuan surname: Han fullname: Han, Huijuan organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China – sequence: 5 givenname: Zhengyu surname: Bai fullname: Bai, Zhengyu organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China – sequence: 6 givenname: Lin surname: Yang fullname: Yang, Lin email: yanglin1819@163.com organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Boron Chemistry and Advanced Energy Materials, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China |
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| Keywords | Trifunctional non-precious metal catalysts oxygen evolution reaction oxygen reduction reaction transition-metal-based sulfides Co9S8 hollow microspheres hydrogen evolution reaction |
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| SubjectTerms | Catalytic oxidation Co9S8 hollow microspheres Electrocatalysts Electrolytes Energy conversion Energy storage Hydrogels hydrogen evolution reaction Hydrogen evolution reactions Hydrogen storage Metal sulfides Metals Microspheres oxygen evolution reaction Oxygen evolution reactions oxygen reduction reaction Ruthenium oxide Studies System effectiveness transition-metal-based sulfides Trifunctional non-precious metal catalysts Water splitting |
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