Reduction of dislocation densities in single crystal CVD diamond by confinement in the lateral sector

The use of diamond as a semiconductor material in power electronics applications is held back by the presence of vertical threading dislocations that are believed to deteriorate device performance. Reducing their occurrence in single crystal diamond is therefore crucial. Recently we found that thick...

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Vydané v:Diamond and related materials Ročník 83; s. 162 - 169
Hlavní autori: Boussadi, A., Tallaire, A., Kasu, M., Barjon, J., Achard, J.
Médium: Journal Article
Jazyk:English
Vydavateľské údaje: Amsterdam Elsevier B.V 01.03.2018
Elsevier BV
Elsevier
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ISSN:0925-9635, 1879-0062
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Abstract The use of diamond as a semiconductor material in power electronics applications is held back by the presence of vertical threading dislocations that are believed to deteriorate device performance. Reducing their occurrence in single crystal diamond is therefore crucial. Recently we found that thick CVD diamond grown on the inclined plane of a pyramidal-shape substrate can lead to dislocation bending from a [001] to a [110] direction (Tallaire et al., 2013a [1]). In this work we further explore this strategy for the growth of thick crystals with low dislocation density. It is shown that the boundary angle between inclined lateral and top faces plays a critical role in preserving bent dislocations during the entire growth run. Indeed under well-chosen growth conditions, a boundary angle of at least 45° ensures that dislocations never intercept the top face and are confined in a lateral sector. We eventually show clear evidence of dislocation density reduction in the crystal using this approach. [Display omitted] •Growth of thick (100)-oriented single crystal CVD diamond with low dislocation density on (100) pyramidal shape substrate.•Evolution of pyramidal shape as function of boron and nitrogen impurities concentration in the gas phase and power/pressure values.•Evolution of growth sector boundary angle and control of direction propagation of dislocation.•Confinement of dislocations in lateral sectors during CVD diamond growth.
AbstractList The use of diamond as a semiconductor material in power electronics applications is held back by the presence of vertical threading dislocations that are believed to deteriorate device performance. Reducing their occurrence in single crystal diamond is therefore crucial. Recently we found that thick CVD diamond grown on the inclined plane of a pyramidal-shape substrate can lead to dislocation bending from a [001] to a [110] direction (Tallaire et al., 2013a [1]). In this work we further explore this strategy for the growth of thick crystals with low dislocation density. It is shown that the boundary angle between inclined lateral and top faces plays a critical role in preserving bent dislocations during the entire growth run. Indeed under well-chosen growth conditions, a boundary angle of at least 45° ensures that dislocations never intercept the top face and are confined in a lateral sector. We eventually show clear evidence of dislocation density reduction in the crystal using this approach.
The use of diamond as a semiconductor material in power electronics applications is held back by the presence of vertical threading dislocations that are believed to deteriorate device performance. Reducing their occurrence in single crystal diamond is therefore crucial. Recently we found that thick CVD diamond grown on the inclined plane of a pyramidal-shape substrate can lead to dislocation bending from a [001] to a [110] direction (Tallaire et al., 2013a [1]). In this work we further explore this strategy for the growth of thick crystals with low dislocation density. It is shown that the boundary angle between inclined lateral and top faces plays a critical role in preserving bent dislocations during the entire growth run. Indeed under well-chosen growth conditions, a boundary angle of at least 45° ensures that dislocations never intercept the top face and are confined in a lateral sector. We eventually show clear evidence of dislocation density reduction in the crystal using this approach. [Display omitted] •Growth of thick (100)-oriented single crystal CVD diamond with low dislocation density on (100) pyramidal shape substrate.•Evolution of pyramidal shape as function of boron and nitrogen impurities concentration in the gas phase and power/pressure values.•Evolution of growth sector boundary angle and control of direction propagation of dislocation.•Confinement of dislocations in lateral sectors during CVD diamond growth.
Author Tallaire, A.
Kasu, M.
Barjon, J.
Achard, J.
Boussadi, A.
Author_xml – sequence: 1
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  orcidid: 0000-0001-5430-5772
  surname: Boussadi
  fullname: Boussadi, A.
  email: amine.boussadi@gmail.com
  organization: Laboratoire des Sciences des Procédés et des Matériaux (LSPM), Université Paris 13, Sorbonne Paris Cité, CNRS, Villetaneuse 93430, France
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  surname: Tallaire
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  fullname: Kasu, M.
  organization: Graduate School of Electrical and Electronic Engineering, Saga University, Saga 840-8502, Japan
– sequence: 4
  givenname: J.
  surname: Barjon
  fullname: Barjon, J.
  organization: Groupe d'Etude de la Matière Condensée (GEMaC), Université Versailles St. Quentin en Yvelines, CNRS, Université Paris Saclay, 78035 Versailles, France
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  givenname: J.
  surname: Achard
  fullname: Achard, J.
  email: jocelyn.achard@lspm.cnrs.fr
  organization: Laboratoire des Sciences des Procédés et des Matériaux (LSPM), Université Paris 13, Sorbonne Paris Cité, CNRS, Villetaneuse 93430, France
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Keywords Confinement
Threading dislocation
Plasma assisted CVD
Growth sector boundary
Single crystal diamond
Extended defect
Pyramidal shape substrate
Language English
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Snippet The use of diamond as a semiconductor material in power electronics applications is held back by the presence of vertical threading dislocations that are...
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SubjectTerms Chemical and Process Engineering
Chemical vapor deposition
Confinement
Crystals
Diamonds
Dislocation density
Engineering Sciences
Extended defect
Growth sector boundary
Physics
Plasma assisted CVD
Plasma physics
Pyramidal shape substrate
Reduction
Semiconductor materials
Single crystal diamond
Single crystals
Substrates
Threading dislocation
Threading dislocations
Title Reduction of dislocation densities in single crystal CVD diamond by confinement in the lateral sector
URI https://dx.doi.org/10.1016/j.diamond.2018.02.010
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