An improved underivatized, cost-effective, validated method for six short-chain fatty organic acids by high-performance liquid chromatography
•A rapid low-cost underivatized HPLC-PDA method was optimized for organic acids.•The method was validated for accuracy, linearity, and repeatability.•The optimized method can be applied to aqueous samples with complex matrices. A fast analytical method for a High-Performance Liquid Chromatograph cou...
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| Vydáno v: | Journal of Chromatography Open Ročník 7; číslo C; s. 100193 |
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| Hlavní autoři: | , , , , |
| Médium: | Journal Article |
| Jazyk: | angličtina |
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Elsevier B.V
01.05.2025
Elsevier |
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| ISSN: | 2772-3917, 2772-3917 |
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| Abstract | •A rapid low-cost underivatized HPLC-PDA method was optimized for organic acids.•The method was validated for accuracy, linearity, and repeatability.•The optimized method can be applied to aqueous samples with complex matrices.
A fast analytical method for a High-Performance Liquid Chromatograph coupled with a Photodiode Array detector (HPLC-PDA) for quantifying six short-chain fatty acids: formic, acetic, propionic, butyric, isovaleric, and valeric acids is optimized and validated. The improved method is compared to existing literature, does not require derivatization, and produces rapid results with relatively low chromatographic cost. Elution modes, mobile phase, pH, and column temperature are optimized to improve peak separation and shorten analysis time without derivatization. The optimized method is characterized by a gradient elution mode with flow rates ranging from 1 to 2.5 mL min −1 and a short analysis time (7.6 mins). The limits of detection for all six acids (LOD) ranged from 0.0003 to 0.068 mM, while the limits of quantification (LOQ) ranged from 0.001 to 0.226 mM. The improved method showed acceptable sensitivity, precision, and dynamic range. Validation and quantification were tested using fermentation broth samples. This optimized method is characterized by lower detection limits and a 50 % shorter analysis time and is applicable to aqueous samples with complex matrices.
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| AbstractList | •A rapid low-cost underivatized HPLC-PDA method was optimized for organic acids.•The method was validated for accuracy, linearity, and repeatability.•The optimized method can be applied to aqueous samples with complex matrices.
A fast analytical method for a High-Performance Liquid Chromatograph coupled with a Photodiode Array detector (HPLC-PDA) for quantifying six short-chain fatty acids: formic, acetic, propionic, butyric, isovaleric, and valeric acids is optimized and validated. The improved method is compared to existing literature, does not require derivatization, and produces rapid results with relatively low chromatographic cost. Elution modes, mobile phase, pH, and column temperature are optimized to improve peak separation and shorten analysis time without derivatization. The optimized method is characterized by a gradient elution mode with flow rates ranging from 1 to 2.5 mL min −1 and a short analysis time (7.6 mins). The limits of detection for all six acids (LOD) ranged from 0.0003 to 0.068 mM, while the limits of quantification (LOQ) ranged from 0.001 to 0.226 mM. The improved method showed acceptable sensitivity, precision, and dynamic range. Validation and quantification were tested using fermentation broth samples. This optimized method is characterized by lower detection limits and a 50 % shorter analysis time and is applicable to aqueous samples with complex matrices.
[Display omitted] A fast analytical method for a High-Performance Liquid Chromatograph coupled with a Photodiode Array detector (HPLC-PDA) for quantifying six short-chain fatty acids: formic, acetic, propionic, butyric, isovaleric, and valeric acids is optimized and validated. The improved method is compared to existing literature, does not require derivatization, and produces rapid results with relatively low chromatographic cost. Elution modes, mobile phase, pH, and column temperature are optimized to improve peak separation and shorten analysis time without derivatization. The optimized method is characterized by a gradient elution mode with flow rates ranging from 1 to 2.5 mL min −1 and a short analysis time (7.6 mins). The limits of detection for all six acids (LOD) ranged from 0.0003 to 0.068 mM, while the limits of quantification (LOQ) ranged from 0.001 to 0.226 mM. The improved method showed acceptable sensitivity, precision, and dynamic range. Validation and quantification were tested using fermentation broth samples. This optimized method is characterized by lower detection limits and a 50 % shorter analysis time and is applicable to aqueous samples with complex matrices. |
| ArticleNumber | 100193 |
| Author | Olonimoyo, Esther A. Lansing, Stephanie Asa-Awuku, Akua A. Duncan, Candice M. Amradi, Naresh Kumar |
| Author_xml | – sequence: 1 givenname: Esther A. surname: Olonimoyo fullname: Olonimoyo, Esther A. email: estherao@umd.edu organization: Department of Chemistry and Biochemistry, University of Maryland, College Park, College Park, MD 20742 USA – sequence: 2 givenname: Naresh Kumar surname: Amradi fullname: Amradi, Naresh Kumar email: nareshka@umd.edu organization: Department of Environmental Science and Technology, University of Maryland, College Park, College Park, MD 20742 USA – sequence: 3 givenname: Stephanie surname: Lansing fullname: Lansing, Stephanie email: slansing@umd.edu organization: Department of Environmental Science and Technology, University of Maryland, College Park, College Park, MD 20742 USA – sequence: 4 givenname: Akua A. orcidid: 0000-0002-0354-8368 surname: Asa-Awuku fullname: Asa-Awuku, Akua A. email: asaawuku@umd.edu organization: Department of Chemistry and Biochemistry, University of Maryland, College Park, College Park, MD 20742 USA – sequence: 5 givenname: Candice M. orcidid: 0000-0003-2814-8034 surname: Duncan fullname: Duncan, Candice M. email: cduncan1@umd.edu organization: Department of Environmental Science and Technology, University of Maryland, College Park, College Park, MD 20742 USA |
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| Issue | C |
| Keywords | Liquid chromatography Method optimization Validation, Photodiode Array Detector Volatile fatty acids |
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| Snippet | •A rapid low-cost underivatized HPLC-PDA method was optimized for organic acids.•The method was validated for accuracy, linearity, and repeatability.•The... A fast analytical method for a High-Performance Liquid Chromatograph coupled with a Photodiode Array detector (HPLC-PDA) for quantifying six short-chain fatty... |
| SourceID | doaj osti crossref elsevier |
| SourceType | Open Website Open Access Repository Enrichment Source Index Database Publisher |
| StartPage | 100193 |
| SubjectTerms | Liquid chromatography Method optimization Validation, Photodiode Array Detector Volatile fatty acids |
| Title | An improved underivatized, cost-effective, validated method for six short-chain fatty organic acids by high-performance liquid chromatography |
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