Carbon vacancy in C3N4 nanotube: Electronic structure, photocatalysis mechanism and highly enhanced activity
[Display omitted] •Tubular g-C3N4 with carbon vacancy was obtained by pyrolysis under N2 atmosphere.•Carbon vacancy facilitates the adsorption of NO and O2 on the surface of g-C3N4.•Carbon vacancy accelerates the separation and transfer of photo-generated carriers.•g-C3N4 with carbon vacancy exhibit...
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| Veröffentlicht in: | Applied catalysis. B, Environmental Jg. 262; S. 118281 |
|---|---|
| Hauptverfasser: | , , , , , , , , |
| Format: | Journal Article |
| Sprache: | Englisch |
| Veröffentlicht: |
Amsterdam
Elsevier B.V
01.03.2020
Elsevier BV |
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| ISSN: | 0926-3373, 1873-3883 |
| Online-Zugang: | Volltext |
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| Abstract | [Display omitted]
•Tubular g-C3N4 with carbon vacancy was obtained by pyrolysis under N2 atmosphere.•Carbon vacancy facilitates the adsorption of NO and O2 on the surface of g-C3N4.•Carbon vacancy accelerates the separation and transfer of photo-generated carriers.•g-C3N4 with carbon vacancy exhibits improved visible photocatalytic NO oxidation.
We demonstrated that carbon vacancy modified C3N4 nanotubes can be qualified for more efficient and selective oxidation of NO to NO3− under visible light illumination than the pristine counterpart. Tubular C3N4 with carbon vacancy was fabricated by facile pyrolysis of the hydrolyzed melamine-urea mixture under N2 gas. With the particular structural merits for tubular nanostructure and the introduction of suitable carbon vacancy density, richly available surface defect sites, and accelerated separation and transfer of photo-generated charge carriers, the as-prepared carbon vacancy modified C3N4 nanotubes exhibited an excellent photocatalytic NO oxidation performance. Based on ESR measurement and DFT calculation, the electronic structure of carbon vacancy was revealed. The surface carbon vacancy in C3N4 nanotubes can greatly facilitate the adsorption of NO and O2, therefore, leading to its superior photocatalytic selectivity in conversion of NO to NO3−. The present work provides new insights into the understanding of defective semiconductor photocatalysis. |
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| AbstractList | We demonstrated that carbon vacancy modified C3N4 nanotubes can be qualified for more efficient and selective oxidation of NO to NO3− under visible light illumination than the pristine counterpart. Tubular C3N4 with carbon vacancy was fabricated by facile pyrolysis of the hydrolyzed melamine-urea mixture under N2 gas. With the particular structural merits for tubular nanostructure and the introduction of suitable carbon vacancy density, richly available surface defect sites, and accelerated separation and transfer of photo-generated charge carriers, the as-prepared carbon vacancy modified C3N4 nanotubes exhibited an excellent photocatalytic NO oxidation performance. Based on ESR measurement and DFT calculation, the electronic structure of carbon vacancy was revealed. The surface carbon vacancy in C3N4 nanotubes can greatly facilitate the adsorption of NO and O2, therefore, leading to its superior photocatalytic selectivity in conversion of NO to NO3−. The present work provides new insights into the understanding of defective semiconductor photocatalysis. [Display omitted] •Tubular g-C3N4 with carbon vacancy was obtained by pyrolysis under N2 atmosphere.•Carbon vacancy facilitates the adsorption of NO and O2 on the surface of g-C3N4.•Carbon vacancy accelerates the separation and transfer of photo-generated carriers.•g-C3N4 with carbon vacancy exhibits improved visible photocatalytic NO oxidation. We demonstrated that carbon vacancy modified C3N4 nanotubes can be qualified for more efficient and selective oxidation of NO to NO3− under visible light illumination than the pristine counterpart. Tubular C3N4 with carbon vacancy was fabricated by facile pyrolysis of the hydrolyzed melamine-urea mixture under N2 gas. With the particular structural merits for tubular nanostructure and the introduction of suitable carbon vacancy density, richly available surface defect sites, and accelerated separation and transfer of photo-generated charge carriers, the as-prepared carbon vacancy modified C3N4 nanotubes exhibited an excellent photocatalytic NO oxidation performance. Based on ESR measurement and DFT calculation, the electronic structure of carbon vacancy was revealed. The surface carbon vacancy in C3N4 nanotubes can greatly facilitate the adsorption of NO and O2, therefore, leading to its superior photocatalytic selectivity in conversion of NO to NO3−. The present work provides new insights into the understanding of defective semiconductor photocatalysis. |
| ArticleNumber | 118281 |
| Author | Fan, Jiajie Gu, Miaoli Cui, Wen Zhang, Xianming Dong, Fan Li, Yuhan Shi, Ting Cheng, Jinshui Lv, Kangle |
| Author_xml | – sequence: 1 givenname: Yuhan surname: Li fullname: Li, Yuhan organization: Engineering Research Center for Waste Oil Recovery Technology and Equipment, Ministry of Education, Chongqing Key Laboratory of Catalysis and New Environmental Materials, Chongqing Technology and Business University, Chongqing 400067, China – sequence: 2 givenname: Miaoli surname: Gu fullname: Gu, Miaoli organization: Engineering Research Center for Waste Oil Recovery Technology and Equipment, Ministry of Education, Chongqing Key Laboratory of Catalysis and New Environmental Materials, Chongqing Technology and Business University, Chongqing 400067, China – sequence: 3 givenname: Ting surname: Shi fullname: Shi, Ting organization: Hubei Key Laboratory of Catalysis and Materials Science, College of Resources and Environmental Science, South-Central University for Nationalities, Wuhan 430074, China – sequence: 4 givenname: Wen orcidid: 0000-0001-9324-4140 surname: Cui fullname: Cui, Wen organization: Engineering Research Center for Waste Oil Recovery Technology and Equipment, Ministry of Education, Chongqing Key Laboratory of Catalysis and New Environmental Materials, Chongqing Technology and Business University, Chongqing 400067, China – sequence: 5 givenname: Xianming surname: Zhang fullname: Zhang, Xianming organization: Engineering Research Center for Waste Oil Recovery Technology and Equipment, Ministry of Education, Chongqing Key Laboratory of Catalysis and New Environmental Materials, Chongqing Technology and Business University, Chongqing 400067, China – sequence: 6 givenname: Fan surname: Dong fullname: Dong, Fan email: dfctbu@126.com organization: Engineering Research Center for Waste Oil Recovery Technology and Equipment, Ministry of Education, Chongqing Key Laboratory of Catalysis and New Environmental Materials, Chongqing Technology and Business University, Chongqing 400067, China – sequence: 7 givenname: Jinshui surname: Cheng fullname: Cheng, Jinshui organization: Hubei Key Laboratory of Catalysis and Materials Science, College of Resources and Environmental Science, South-Central University for Nationalities, Wuhan 430074, China – sequence: 8 givenname: Jiajie orcidid: 0000-0002-3661-3306 surname: Fan fullname: Fan, Jiajie organization: School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, China – sequence: 9 givenname: Kangle orcidid: 0000-0001-8764-0892 surname: Lv fullname: Lv, Kangle email: lvkangle@mail.scuec.edu.cn organization: Hubei Key Laboratory of Catalysis and Materials Science, College of Resources and Environmental Science, South-Central University for Nationalities, Wuhan 430074, China |
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•Tubular g-C3N4 with carbon vacancy was obtained by pyrolysis under N2 atmosphere.•Carbon vacancy facilitates the adsorption of NO and O2 on... We demonstrated that carbon vacancy modified C3N4 nanotubes can be qualified for more efficient and selective oxidation of NO to NO3− under visible light... |
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| SubjectTerms | C3N4 nanotubes Carbon Carbon nitride Carbon vacancy Charge transfer Current carriers Electronic structure Melamine Nanotechnology Nanotubes Oxidation Photocatalysis Photocatalytic oxidation Pyrolysis Reaction mechanism Selectivity Surface defect sites Surface defects Urea Vacancies |
| Title | Carbon vacancy in C3N4 nanotube: Electronic structure, photocatalysis mechanism and highly enhanced activity |
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