Accurate lattice parameter measurements of stoichiometric uranium dioxide
•The lattice parameter of stoichiometric uranium dioxide has been re-evaluated.•The new value is substantially higher than the generally accepted value.•The new value has an improved precision.•Earlier published values on the lattice parameter of UO2 are carefully re-assessed.•High accuracy was obta...
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| Vydané v: | Journal of nuclear materials Ročník 459; s. 135 - 142 |
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| Hlavní autori: | , , , |
| Médium: | Journal Article |
| Jazyk: | English |
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Elsevier B.V
01.04.2015
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| ISSN: | 0022-3115, 1873-4820 |
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| Abstract | •The lattice parameter of stoichiometric uranium dioxide has been re-evaluated.•The new value is substantially higher than the generally accepted value.•The new value has an improved precision.•Earlier published values on the lattice parameter of UO2 are carefully re-assessed.•High accuracy was obtained on both stoichiometry and lattice parameter measurements.
The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO2. Attention was paid to prepare stoichiometric samples and to maintain stoichiometry throughout the analyses. The lattice parameter of UO2.000±0.001 was evaluated as being 547.127±0.008pm at 20°C, which is substantially higher than many published values for the UO2 lattice constant and has an improved precision by about one order of magnitude. The higher value of the lattice constant is mainly attributed to the avoidance of hyperstoichiometry in the present study and to a minor extent to the use of the currently accepted Cu Kα1 X-ray wavelength value. Many of the early studies used Cu Kα1 wavelength values that differ from the currently accepted value, which also contributed to an underestimation of the true lattice parameter. |
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| AbstractList | •The lattice parameter of stoichiometric uranium dioxide has been re-evaluated.•The new value is substantially higher than the generally accepted value.•The new value has an improved precision.•Earlier published values on the lattice parameter of UO2 are carefully re-assessed.•High accuracy was obtained on both stoichiometry and lattice parameter measurements.
The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO2. Attention was paid to prepare stoichiometric samples and to maintain stoichiometry throughout the analyses. The lattice parameter of UO2.000±0.001 was evaluated as being 547.127±0.008pm at 20°C, which is substantially higher than many published values for the UO2 lattice constant and has an improved precision by about one order of magnitude. The higher value of the lattice constant is mainly attributed to the avoidance of hyperstoichiometry in the present study and to a minor extent to the use of the currently accepted Cu Kα1 X-ray wavelength value. Many of the early studies used Cu Kα1 wavelength values that differ from the currently accepted value, which also contributed to an underestimation of the true lattice parameter. The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO sub(2). Attention was paid to prepare stoichiometric samples and to maintain stoichiometry throughout the analyses. The lattice parameter of UO sub(2.000+ or -0.001) was evaluated as being 547.127 + or - 0.008 pm at 20 [degrees]C, which is substantially higher than many published values for the UO sub(2) lattice constant and has an improved precision by about one order of magnitude. The higher value of the lattice constant is mainly attributed to the avoidance of hyperstoichiometry in the present study and to a minor extent to the use of the currently accepted Cu K[alpha] sub(1) X-ray wavelength value. Many of the early studies used Cu K[alpha] sub(1) wavelength values that differ from the currently accepted value, which also contributed to an underestimation of the true lattice parameter. |
| Author | Verwerft, Marc Binnemans, Koen Cardinaels, Thomas Leinders, Gregory |
| Author_xml | – sequence: 1 givenname: Gregory surname: Leinders fullname: Leinders, Gregory email: gregory.leinders@sckcen.be organization: KU Leuven, Department of Chemistry, Celestijnenlaan 200F, P.O. Box 2404, B-3001 Heverlee, Belgium – sequence: 2 givenname: Thomas surname: Cardinaels fullname: Cardinaels, Thomas organization: Belgian Nuclear Research Centre (SCK•CEN), Institute for Nuclear Materials Science, Boeretang 200, B-2400 Mol, Belgium – sequence: 3 givenname: Koen surname: Binnemans fullname: Binnemans, Koen organization: KU Leuven, Department of Chemistry, Celestijnenlaan 200F, P.O. Box 2404, B-3001 Heverlee, Belgium – sequence: 4 givenname: Marc surname: Verwerft fullname: Verwerft, Marc organization: Belgian Nuclear Research Centre (SCK•CEN), Institute for Nuclear Materials Science, Boeretang 200, B-2400 Mol, Belgium |
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| Snippet | •The lattice parameter of stoichiometric uranium dioxide has been re-evaluated.•The new value is substantially higher than the generally accepted value.•The... The paper presents and discusses lattice parameter analyses of pure, stoichiometric UO sub(2). Attention was paid to prepare stoichiometric samples and to... |
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| SubjectTerms | Avoidance Copper Lattice parameters Nonstoichiometric compounds Nuclear engineering Stoichiometry Wavelengths X-rays |
| Title | Accurate lattice parameter measurements of stoichiometric uranium dioxide |
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